纳米氧化钇稳定氧化锆对Ni-20Cr复合镀层性能的影响

IF 2.9 Q2 ELECTROCHEMISTRY Journal of Electrochemical Science and Engineering Pub Date : 2022-08-16 DOI:10.5599/jese.1319
Sukhjinderjit Singh, K. Goyal, R. Bhatia
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引用次数: 4

摘要

本研究采用高速氧燃料喷涂工艺,在Ni-20Cr粉末中增强5 wt.%和10 wt.%钇稳定氧化锆(YSZ)纳米颗粒,并将其沉积在锅炉管钢上。研究了YSZ增强对合金显微硬度、表面粗糙度和孔隙率的影响。当YSZ含量为10 wt.%时,涂层的硬度最高,硬度随孔隙率的减小而增大。利用场发射扫描电镜(FE-SEM)和能谱仪(EDS)对涂层的微观结构和元素进行了表征。用x射线衍射仪鉴定了涂层的成分。结果表明,含10 wt.% YSZ增强纳米复合镀层的复合镀层显微硬度最高,为1008 ~ 1055 hv。在涂层过程中,纳米YSZ颗粒分散在微米级Ni-20Cr颗粒之间的间隙中,提供了比常规Ni-20Cr更好的涂层基质。在Ni-20Cr中添加10 wt.%的YSZ纳米粒子,在力学性能和微观组织性能方面表现出较好的效果。
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Effect of nano yttria-stabilized zirconia on properties of Ni-20Cr composite coatings
In the present work, 5 wt.% and 10 wt.% yttria-stabilized zirconia (YSZ) nanoparticles were reinforced in Ni-20Cr powder and deposited on boiler tube steel using a high-velocity oxy-fuel spraying process. The effect of YSZ reinforcement on microhardness, surface roughness and porosity was investigated. The hardness was the highest for nanocomposite coating reinforced with 10 wt.% YSZ and hardness was found to increase with a decrease in porosity. The coating microstructure and elements were characterized using field emission scanning electron microscopy (FE-SEM) with an energy dispersive spectroscope (EDS). The constituents of the coating were identified using X-ray diffractometer. It was found that the composite coating with 10 wt.% YSZ reinforced nanocomposite coating has the highest microhardness, in the range of 1008-1055 hv. During the coating process, nano YSZ particles were dispersed in the gaps between the micrometric Ni-20Cr particles, providing a better coating matrix than conventional Ni-20Cr. The Ni-20Cr with 10 wt.% of YSZ nanoparticles showed better results in terms of mechanical and microstructural properties during the investigation.
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来源期刊
CiteScore
3.60
自引率
27.30%
发文量
90
审稿时长
6 weeks
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