含氟有机/无机复合颗粒的制备与表征

Rui Weng, Chong-Hui Wang, Lianmeng Zhang, Shui-Ping Wang
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引用次数: 0

摘要

氟化有机/无机复合颗粒是由氨基硅烷(N- β -氨基乙基)- γ -氨基丙基三甲氧基硅烷或N-(β -氨基乙基)- γ -氨基丙基甲基二甲氧基硅烷与全氟辛基磺酸氟化合物复配而成。通过FTIR、1hnmr、TG/DTA、master粒度分析和接触角对产物的结构和性能进行表征,合成产物具有良好的热阻性,其粒径在微米级,表面水接触角为116°。
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Preparation and Characterization of Fluorinated Organic/Inorganic Composite Particles
Fluorinated organic/inorganic composite pariticles is synthesized by compounding aminosilane (N-beta-aminoethyl)-gamma-aminopropyl trimethoxy silane or N-(beta-aminoethyl)- gamma-aminopropyl methyldimethoxy silane and perfluorinated octyl sulfonic acid fluoride. The structure and properties of products are characterized by FTIR , 1 HNMR, TG/DTA, Mastersizer analysis and contact angle, the synthesized product shows good thermal resistance, and its particle size is in the micrometer- level, surface water contact angle is 116deg.
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