脉冲镀参数对镍镀层电接触性能的影响

S. Benhenda, N. Benjemâa, M. Bourir
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引用次数: 7

摘要

研究了铜及铜合金脉冲镀镍涂层作为Au/Ni/Cu镀层底层或外保护涂层的应用。为了确定沉积参数对电沉积Ni薄膜的微观结构和电接触性能的影响,研究了沉积参数的变化。对这些样品进行了粗糙度和硬度测量以及扫描电镜研究。在高暂停脉冲比、25 ~ 75 Hz脉冲电镀频率和低电流密度条件下,镀层光滑致密。在0.1 ~ 10 n范围内,测量了在接近模式和插入模式下沉积样品的接触电阻R/sub c/随载荷F/sub c/的变化。结果表明,初始接触电阻R/sub c/=KF/sub c//sup -n/,其中n与镀层的硬度和形貌有关。此外,在日常循环气氛中老化的样品在测试过程中显示接触电阻增加,但欧姆行为普遍存在,并由电流-电压特性验证。最后,微动研究表明,脉冲反向条件提高了接触电阻的稳定性。
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Effect of pulse plating parameters on electrical contact behaviour of nickel coatings
Pulse plated nickel coatings on copper and copper alloys were investigated in view of their use as underlayer in Au/Ni/Cu or as external protective coatings. Deposition parameters were varied in order to determine their influence on the microstructure and consequently on the electrical contact properties of the electrodeposited Ni films. Roughness and hardness measurements as well as SEM studies were performed on these samples. Smooth and dense coatings were obtained for high pause-to-pulse ratio, 25-75 Hz pulse-plating frequencies and low current density. The contact resistances R/sub c/ of the as-deposited samples in approach and insert mode were measured versus load F/sub c/ in the range 0.1-10 N. It was found that initial contact resistance follows the power law R/sub c/=KF/sub c//sup -n/ where n is hardness and coating topography dependent. Moreover, aging samples in daily cyclic atmosphere shows an increase in contact resistance during the test, but ohmic behaviour prevails as verified by the current-voltage characteristics. Finally, the mechanical behaviour investigated by a fretting study shows that the pulse reverse condition improves contact resistance stability.
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