喷雾干燥制备热塑性淀粉/二氧化钛/石墨烯纳米复合材料用于水果覆盖的作用和性能评价

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摘要

在这项研究中,二氧化钛纳米粒子(TiO2)和石墨烯被加入到从木薯(Manihot esculenta Crantz)中获得的热塑性淀粉(TPS)基质中,目的是生产一种覆盖水果的材料,旨在延长食品的保质期。采用溶剂分散法制备高分子纳米复合材料,然后采用喷雾干燥法制备粉体。采用傅里叶变换红外光谱(FTIR)、x射线衍射(XRD)、流动性指数(MFI)、动态光散射(DLS)、ζ电位(PZ)和紫外吸收光谱(UV-vis)对ncp进行了表征。研究结果表明,纳米复合材料制备的聚合物悬浮液具有吸收UV-A和UV-B辐射效率高、溶液稳定性好等特点,具有应用于苹果和番石榴涂层的潜力。此外,水果涂层测试证明,开发的溶液改善了视觉特性,并显着延缓了被分析水果的降解过程,证明有效地延长了食品的寿命,减少了过高的损失和浪费,对经济和环境产生了积极的影响。
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Evaluation of the action and properties of thermoplastic starch / titanium dioxide / graphene nanocomposites obtained through spray drying for fruit covering
In this study, nanoparticles of titanium dioxide (TiO2) and graphene were incorporated into a matrix of thermoplastic starch (TPS) obtained from cassava (Manihot esculenta Crantz) with the objective of producing a material for covering fruit, aiming to last the shelf life of food. The polymeric nanocomposites (NCPs) were obtained by the solvent dispersion method and, subsequently, the spray drying technique was used to obtain the material in powder form. The NCPs were characterized by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), fluidity index (MFI), dynamic light scattering (DLS), zeta potential (PZ) and UV absorption spectroscopy ultraviolet and visible (UV-vis). The main results showed that the polymeric suspension obtained from the pulverized nanocomposites presented characteristics for potential use in coating apples and guava, such as high efficiency in absorbing UV-A and UV-B radiation and high stability of the formed solutions. Furthermore, the fruit coating test proved that the developed solution improved the visual characteristics and significantly delayed the degradation process of the analyzed fruits, proving to be effective in offering greater longevity to the food, reducing exorbitant losses and waste that strongly impact positively the economy and the environment.
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