海参长链脂肪化合物的分离与鉴定

V. Nyigo, H. Malebo, F. Mabiki, R. Mdegela
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引用次数: 3

摘要

利用层析技术对海合子根皮和叶片的二氯甲烷提取物进行纯化,分离到赤藓酸盐C和1-八烷醇两种化合物。主要利用一维和二维1H和13C核磁共振数据,并将现有核磁共振数据与文献数据进行比较,建立化学结构。用质谱数据通过分子离子峰进行确认。已知这两种化合物均从其他植物中分离得到,但均为首次从该植物中分离得到。
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Isolation and identification of long -chain aliphatic compounds from Synadenium glaucescens
Purification of dichloromethane extract from root barks and leaves of Synadenium glaucescens extracts through chromatographic techniques resulted into the isolation of two compounds, namely erythrinacinate C and 1-octacosanol. Chemical structures were established mainly using both one and two dimensional 1H and 13C NMR data and by comparison of the current NMR data with those from literature. Mass spectrophotometry data were used for confirmation through molecular ion peak. Both compounds are known to have been isolated from other plant species but are being reported from this plant species for the first time.
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