The influence of pre-heating the restoration and luting agent on the flexural strength of indirect ceramic and composite restorations

João Paulo Mendes Tribst, Lilis Etoeharnowo, Maril Tadros, A. Feilzer, Arie Werner, C. Kleverlaan, A. D. Dal Piva
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Abstract

Abstract Background This study investigated the impact of luting procedure and restoration thicknesses on the flexural strength of CAD/CAM restorations. Traditional luting agents have been questioned in favor of pre-heated resin composites or flowable composites. Materials and Methods 400 disc-shaped restorations (lithium disilicate [IPS e.max CAD] or resin composite [Tetric CAD, Ivoclar]) were cemented onto dentin analog discs using different procedures (n = 20): dual-curing resin cement (Panavia V5), light-curing resin cement (Panavia Veneer LC), pre-heated resin composite (Clearfil™ AP-X) with or without pre-heated restoration, and high-filled flowable composite (Clearfil Majesty™ Flow). The biaxial flexural strength was calculated. Results There were significant effects of material, thickness, and luting procedure on flexural strength (p < 0.001). Resin composite specimens exhibited lower flexural strength (90 MPa) compared to lithium disilicate specimens (571 MPa), with thicker restorations (338 MPa) being stronger than thinner ones (323 MPa). Light-curing cement showed the highest strength (408.8 MPa)A, followed by dual-curing cement (362 MPa)B, pre-heated cement with pre-heated composite (318 MPa)C, pre-heated composite (304 MPa)C, and flowable resin composite (259 MPa)D. The light-curing cement yielded similar results to the pre-heated resin composite associated or not with the pre-heated crown for the thicker lithium disilicate specimens, whereas for the thinner lithium disilicate specimens all luting procedures performed similarly. Thin resin composite discs showed higher flexural strength when luted with light-curing cement, whereas the luting procedure had less influence for the thicker restorations. Conclusion Luting procedures impact the flexural strength of CAD/CAM lithium disilicate and resin composite restorations. Pre-heated resin composite, with or without pre-heated restoration, can replace dual-curing cement. Nevertheless, light-curing cement is superior for resin composite and 1.5 mm lithium disilicate restorations. Key-messages Different luting procedures significantly impact the flexural strength of CAD/CAM lithium disilicate and resin composite restorations, with light-curing cement demonstrating superior performance for specific thicknesses. Pre-heated resin composites, either with or without pre-heated restorations, offer a viable alternative to conventional dual-curing cement for bonding indirect restorations, presenting potential clinical advantages. Restoration thickness plays a crucial role in the mechanical response of restorations, with thinner resin composite restorations benefiting from dual- or light-curing, while thicker ones are less sensitive to luting procedure variations.
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预热修复体和衬垫剂对间接陶瓷和复合材料修复体抗弯强度的影响
摘要 背景 本研究调查了上胶程序和修复体厚度对 CAD/CAM 修复体抗弯强度的影响。传统的粘结剂已受到质疑,而预热树脂复合材料或可流动复合材料则更受青睐。材料和方法 使用不同的程序(n = 20)将 400 个盘状修复体(二硅酸锂[IPS e.max CAD]或树脂复合材料[Tetric CAD, Ivoclar])粘结到牙本质模拟盘上:双固化树脂粘结剂(Panavia V5)、光固化树脂粘结剂(Panavia Veneer LC)、带或不带预热修复体的预热树脂复合材料(Clearfil™ AP-X)以及高填充可流动复合材料(Clearfil Majesty™ Flow)。计算了双轴抗弯强度。结果 材料、厚度和上胶程序对抗弯强度有明显影响(p < 0.001)。树脂复合材料试样的抗弯强度(90 兆帕)低于二硅酸锂试样(571 兆帕),较厚的修复体(338 兆帕)强于较薄的修复体(323 兆帕)。光固化水门汀的强度最高(408.8 兆帕)A,其次是双固化水门汀(362 兆帕)B、带预热复合材料的预热水门汀(318 兆帕)C、预热复合材料(304 兆帕)C 和可流动树脂复合材料(259 兆帕)D。对于较厚的二硅酸锂试样,光固化水泥与预热树脂复合材料的结果相似,而对于较薄的二硅酸锂试样,所有砌合程序的结果都相似。当使用光固化粘接剂粘结时,薄树脂复合片显示出更高的抗弯强度,而粘结程序对厚修复体的影响较小。结论 光固化程序会影响 CAD/CAM 二硅酸锂和树脂复合材料修复体的抗折强度。预热或不预热的树脂复合修复体可以替代双固化水门汀。尽管如此,光固化水门汀对于树脂复合材料和1.5毫米二硅酸锂修复体还是更有优势。关键信息 不同的粘结程序对 CAD/CAM 二硅酸锂和树脂复合材料修复体的抗弯强度有很大影响,光固化粘结剂在特定厚度的修复体中表现出更优越的性能。预热或不预热修复体的预热树脂复合材料为粘结间接修复体提供了传统双固化粘结剂的可行替代方案,具有潜在的临床优势。修复体的厚度对修复体的机械反应起着至关重要的作用,较薄的树脂复合材料修复体可从双固化或光固化中获益,而较厚的修复体则对粘结程序的变化不太敏感。
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Root-filling materials for endodontic surgery: biological and clinical aspects. Silane and acid etch cross contamination of dentin and composite reduced µ-tensile bond strength. Recipient of Biomaterial Investigations in Dentistry's Young Author Award 2023. Reliability and agreement of root length measurements during orthodontic treatment in images from different CBCT machines using multiplanar reconstruction. The sealing ability of different endodontic biomaterials as an intra-orifice barrier: evaluation with high-performance liquid chromatography.
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