Optimization and verification of hot tensile deformation parameters of Ti-47.5Al-2.5V-1.0Cr-0.2Zr alloy based on processing map theory

IF 4.8 2区 材料科学 Q2 CHEMISTRY, PHYSICAL Intermetallics Pub Date : 2025-05-01 Epub Date: 2025-02-04 DOI:10.1016/j.intermet.2025.108692
Xuejian Lin, Hongjun Huang, Xiaoguang Yuan, Bowen Zheng, Xiaojiao Zuo, Ge Zhou, Kai Du
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Abstract

The high temperature tensile experiment of Ti-47.5Al-2.5V-1.0Cr-0.2Zr alloy was completed at 750–900 °C and strain rate of 10−5–10−3 s−1. The processing map corresponding to the tensile process was established, and both optimal and instability zones were identified. The microstructure of different zones of processing map were observed in detail, and the justness of processing map was proved. The results show that the strain rate sensitivity index and energy dissipation rate increase with change of deformation conditions from low temperature/high stretching rate to high temperature/low stretching rate. The parameters of thermal tensile instability zone are: 750–795 °C/10−4–4 × 10−4s−1 and 750–778 °C/10−4–10−5s−1. The optimal hot deformation parameters are as follows: the temperature is 880–900 °C and the strain rate is 2.5 × 10−4–10−5s−1. The obvious cracks and holes appear in the deformation structure corresponding to the instability zone, which are preferentially generated at the lamellar interface. The ratio of recrystallized structure corresponding to the optimal deformation parameter zone is higher than that in the instability zone, and the plastic deformation ability is greatly improved. The deformation characteristics of the instability zone are the dislocation pile-up, which is caused by the hindrance of the lamellar boundary and lamellar structure to the dislocation movement, and the substructure formed by the entanglement of the high-density dislocation regions in the lamellar structure. At the same time, there are also twins with a certain angle between the lamellar structure. The characteristics of deformation structure corresponding to the optimal deformation parameter region are dislocation, twin and recrystallization. The dislocation density in the recrystallized structure decreases, which can slow down the stress concentration inside the deformed structure, and the probability of instability such as cracks inside the alloy decreases.
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基于加工图理论的Ti-47.5Al-2.5V-1.0Cr-0.2Zr合金热拉伸变形参数优化与验证
Ti-47.5Al-2.5V-1.0Cr-0.2Zr合金在750 ~ 900℃,应变速率为10−5 ~ 10−3 s−1的条件下完成高温拉伸实验。建立了与拉伸工艺相对应的工艺图,确定了最优区和不稳定区。对加工图不同区域的微观结构进行了详细观察,证明了加工图的正确性。结果表明:从低温/高拉伸速率到高温/低拉伸速率,应变率敏感性指数和能量耗散率随变形条件的变化而增大;热拉伸失稳区参数为:750 ~ 795℃/10−4-4 × 10−4s−1和750 ~ 778℃/10−4-10−5s−1。最佳热变形参数为:温度为880 ~ 900℃,应变速率为2.5 × 10−4 ~ 10−5s−1。与失稳区相对应的变形结构中出现了明显的裂纹和孔洞,这些裂纹和孔洞优先在片层界面处产生。最佳变形参数区对应的再结晶组织比例高于失稳区,塑性变形能力大大提高。失稳区的变形特征是由于层状边界和层状结构对位错运动的阻碍造成的位错堆积,以及高密度位错区域在层状结构中纠缠形成的亚结构。同时,还存在着具有一定夹角的孪晶片层结构。最佳变形参数区对应的变形组织特征为位错、孪晶和再结晶。再结晶组织中的位错密度降低,可以减缓变形组织内部的应力集中,降低合金内部出现裂纹等不稳定的概率。
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来源期刊
Intermetallics
Intermetallics 工程技术-材料科学:综合
CiteScore
7.80
自引率
9.10%
发文量
291
审稿时长
37 days
期刊介绍: This journal is a platform for publishing innovative research and overviews for advancing our understanding of the structure, property, and functionality of complex metallic alloys, including intermetallics, metallic glasses, and high entropy alloys. The journal reports the science and engineering of metallic materials in the following aspects: Theories and experiments which address the relationship between property and structure in all length scales. Physical modeling and numerical simulations which provide a comprehensive understanding of experimental observations. Stimulated methodologies to characterize the structure and chemistry of materials that correlate the properties. Technological applications resulting from the understanding of property-structure relationship in materials. Novel and cutting-edge results warranting rapid communication. The journal also publishes special issues on selected topics and overviews by invitation only.
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