Potential of strain-integrated gas infusion (SIGI) casting on post-heat treatment kinetics of AZ91 magnesium alloy

IF 13.8 1区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING Journal of Magnesium and Alloys Pub Date : 2025-02-01 Epub Date: 2025-02-03 DOI:10.1016/j.jma.2025.01.016
V. Tiwari , S.K. Panigrahi
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Abstract

Heat treatments play a crucial role in enhancing the mechanical properties of AZ91 Mg alloy by dissolving coarse phases during solution treatment and promoting precipitation during aging. However, non-uniform microstructures and coarse secondary phases in conventional casting methods hinder the effectiveness of these treatments, leading to reduced ductility, inconsistent properties, and prolonged durations. To overcome these challenges, this study introduces the Strain Integrated Gas-Infusion (SIGI) casting process that integrates strain and gas infusion in the semi-solid state. The impact of the SIGI process on the solution treatment and aging kinetics of AZ91 Mg alloy is explored. The SIGI process refines α-Mg and β-Mg17Al12 phases, significantly enhancing mechanical properties. Experimental and quantitative analyses reveal that the SIGI process accelerates solute atom dissolution, reducing solution treatment times by half, and promotes faster nucleation and growth of precipitates during aging, shortening aging times by one-third. These improvements result in substantial gains in ultimate tensile strength (∼40–50%) and ductility (∼20–30%) after age hardening compared to conventional casting. The mechanisms driving these changes, including enhanced nucleation rates, reduced diffusion distances, and microstructural refinement, are discussed. These findings demonstrate the potential of the SIGI casting process to advance magnesium alloy performance for engineering applications.

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应变集成气体注入铸造对AZ91镁合金热处理后动力学的影响
热处理对AZ91镁合金力学性能的提高起着至关重要的作用,在固溶过程中,热处理能溶解粗相,在时效过程中,热处理能促进析出。然而,常规铸造方法中不均匀的组织和粗糙的二次相阻碍了这些处理的有效性,导致延展性降低、性能不一致和持续时间延长。为了克服这些挑战,本研究引入了应变集成气体注入(SIGI)铸造工艺,该工艺在半固态下集成了应变和气体注入。探讨了SIGI工艺对AZ91镁合金固溶处理和时效动力学的影响。SIGI工艺细化了α-Mg和β-Mg17Al12相,显著提高了力学性能。实验和定量分析表明,SIGI工艺加速了溶质原子的溶解,使固溶处理次数减少了一半,并促进了时效过程中析出相的更快形核和生长,使时效时间缩短了三分之一。与传统铸件相比,这些改进可显著提高时效硬化后的极限抗拉强度(~ 40 - 50%)和延展性(~ 20 - 30%)。讨论了驱动这些变化的机制,包括增强的成核速率,减少的扩散距离和微观结构的细化。这些发现证明了SIGI铸造工艺在提高镁合金工程应用性能方面的潜力。
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来源期刊
Journal of Magnesium and Alloys
Journal of Magnesium and Alloys Engineering-Mechanics of Materials
CiteScore
20.20
自引率
14.80%
发文量
52
审稿时长
59 days
期刊介绍: The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.
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