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The impact of holding time variation on the effectiveness of DSSC TiO2 transparent with dye Ipomoea aquatica Forsk 研究了保温时间的变化对水草染料DSSC TiO2透明膜效能的影响
Pub Date : 2022-10-12 DOI: 10.53402/ajmse.v1i1.188
T. Y. Septiawan
In dye-sensitized solar cells, the working electrode is frequently made of the semiconductor TiO2 (DSSC). TiO2 is utilized in two different forms: transparent paste and nano powder. In this study, TiO2 and a transparent sort of paste were used to fabricate DSSCs with success. To fabricate the DSSC, transparent TiO2 paste 18 NR-T was placed in the furnace Carbonite 1100 heating process with three different holding times. 10 minutes, 20 minutes, and 30 minutes at 500 °C were the different holding times employed. Ipomoea aquatica Forsk is the source of natural colouring. Keithley 2620A and UV-Vis Spectrophotometer Lambda 25 were used for the I-V test and the absorbance test, respectively, for DSSC characterization. According to the characterization results, the efficiency was 5.5 x 10-2 per cent. At the same time, the absorbance test found absorption peaks in the wavelength ranges of 400–440 nm and 640–680 nm for each watercolour dye.
在染料敏化太阳能电池中,工作电极通常由半导体TiO2 (DSSC)制成。二氧化钛以两种不同的形式被利用:透明膏状和纳米粉末状。在这项研究中,二氧化钛和一种透明的浆料成功地制备了DSSCs。为了制备DSSC,将透明TiO2浆料18nr - t置于Carbonite 1100炉中加热,并进行三次不同的保温时间。在500℃下,保温时间分别为10分钟、20分钟和30分钟。水木是天然色素的来源。分别使用Keithley 2620A和UV-Vis分光光度计Lambda 25进行I-V测试和吸光度测试,以表征DSSC。根据表征结果,效率为5.5 x 10- 2%。同时,吸光度测试发现每种水彩染料的吸收峰在400-440 nm和640-680 nm的波长范围内。
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引用次数: 0
Parallel circuit resistance in motor: A simulation study 电机并联电阻的仿真研究
Pub Date : 2022-07-09 DOI: 10.53402/ajmse.v1i1.73
X. Run, Z. Chen
The phenomenon that occurs while a motor is under load disqualifies the applicant. In the interim, it may measure the maximal motor property during production. Consequently, the phenomena of numerous circuits is investigated in order to identify a simulation of electrical state that can anticipate the maximum currency and torque, which is a procedure that must be completed prior to design. We observe that the simulation matches the reference quite well. Multiple circuit circumstances with t=6s, U=12V result in the greatest stall force based on rotation to modify time and voltage. Then, the sequence is t=8s, U=10V; t=10s, U=8V; and t=12s, U=6V. In terms of torque, t=6s, U=12V, t=8s, U=10V, t=6s, U=12V, and t=12s, U=6V are the values. When the voltage falls, the resistance falls, and ultimately the spinning slows.
电机在负载下发生的现象使申请人丧失资格。在此期间,它可以测量生产过程中的最大运动性能。因此,研究了许多电路的现象,以确定可以预测最大货币和扭矩的电气状态的模拟,这是一个必须在设计之前完成的过程。我们观察到,模拟结果与参考文献吻合得很好。t=6s, U=12V的多种电路情况下,基于旋转修改时间和电压的失速力最大。则顺序为t=8s, U=10V;t = 10 s U = 8 v;t=12s, U=6V。转矩的取值为t=6s, U=12V, t=8s, U=10V, t=6s, U=12V, t=12s, U=6V。当电压下降时,电阻下降,最终旋转速度减慢。
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引用次数: 0
Evaluation of injection molded gas and water atomized 316l stainless steel powder properties 316l不锈钢注塑气、水雾化粉末性能评价
Pub Date : 2022-07-07 DOI: 10.53402/ajmse.v1i1.74
M. A. Omar, I. Subuki
This research investigates the features crucial to injection molding via the rheological behavior, injection molding, debinding, and sintering process of water and gas atomised 316L stainless steel powder utilizing a newly developed locally based binder system containing palm stearin. The critical powder loading for injection molding was 65vol% for gas atomisation and 62vol% for water atomisation. Due to the minimal interparticle friction and high packing density, the gas-atomised powder proved easier to shape. In contrast, the water-atomised powder has a high viscosity of the injection molding feedstock, a high interparticle friction, and a low packing density, all of which impede injection molding. The debinding of the binder was accomplished utilizing solvent and thermal methods. After debinding, samples were sintered in a high-temperature vacuum furnace at 1360 degrees Celsius. Results reveal that water-atomised powder can be sintered to 95% of its theoretical density, whereas gas-atomised powder can be sintered to near full density.
本研究利用一种新开发的含有棕榈硬脂的本地粘合剂系统,通过流变行为、注射成型、脱脂和水和气雾化316L不锈钢粉末的烧结过程,研究了注射成型的关键特征。注射成型的临界粉末负荷为气体雾化的65vol%和水雾化的62vol%。由于颗粒间摩擦最小,堆积密度高,气体雾化粉末被证明更容易成型。相反,水雾化粉末具有注塑原料的高粘度、高颗粒间摩擦和低堆积密度,所有这些都阻碍了注塑成型。采用溶剂法和热法对粘结剂进行了脱粘。脱粘后,样品在1360℃的高温真空炉中烧结。结果表明,水雾化粉末可以烧结到理论密度的95%,而气体雾化粉末可以烧结到接近全密度。
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引用次数: 0
Synthesis, characterisation of schiff bases generated from salicylaldehyde with certain amino acids using a new established technique 水杨醛与特定氨基酸合成席夫碱的新工艺及表征
Pub Date : 2022-07-04 DOI: 10.53402/ajmse.v1i1.75
A. Wady, M. B. Hussein, M. M. Mohammed
Amino acids are compounds that consist of an amine group, a carboxylic acid group, and a variable side chain. These molecules are very significant in biochemistry. Amino acids with uncharged amino groups can also undergo Schiff base production at physiological PH levels, presenting an additional possible pathway for metal complexes. In this investigation, four novel Schiff-base amino acid compounds were identified: 5Chlorosalcialdehyde-glycine (H2L1), 5-Chlorosalycialdehyde-alanine (H2L2), 5-Nitrosalycialdehyde-glycine (H2L3), and 5Nitrosalycialdehyde-alanine (H2L4) (H2L4). Condensation reaction product of substituted salicylaldehyde. With a few amino acids, glycine and -alanine, using an alternate technique. The innovation is the addition of 10-2mole sodium hydroxide as a novel catalyst to the traditional process of synthesizing Schiff bases. Elements (C.H.N) and spectroscopic techniques (IR, 1H, and 13C NMR) were used to describe the four Schiff bases. These techniques were successfully used to characterize the prepared Schiff bases
氨基酸是由一个胺基、一个羧基和一个可变侧链组成的化合物。这些分子在生物化学中非常重要。不带电荷的氨基酸也可以在生理PH水平下产生希夫碱,这为金属配合物提供了另一种可能的途径。在这项研究中,鉴定了四种新的希夫碱氨基酸化合物:5氯水杨醛-甘氨酸(H2L1)、5氯水杨醛-丙氨酸(H2L2)、5硝基水杨醛-甘氨酸(H2L3)和5硝基水杨醛-丙氨酸(H2L4) (H2L4)。取代水杨醛缩合反应产物。用一些氨基酸,甘氨酸和丙氨酸,用另一种技术。创新之处是在传统的希夫碱合成工艺中加入10-2mol氢氧化钠作为新型催化剂。采用元素(C.H.N)和光谱技术(IR、1H和13C NMR)对四种希夫碱进行了表征。这些技术成功地用于表征所制备的希夫碱
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引用次数: 0
Carbon dioxide emissions and wetland soil physicochemical properties in Oguta Lake, Imo State, Nigeria 尼日利亚伊莫州奥古塔湖二氧化碳排放与湿地土壤理化性质
Pub Date : 2022-07-01 DOI: 10.53402/ajmse.v1i1.76
A. W. Verla, J. Olumba, E. N. Verla
Wetlands contribute around 5 percent of the world's carbon dioxide (CO2) emissions via respiration, which is believed to be controlled by soil conditions. The objective of this study is to establish a link between the physicochemical parameters of marsh soil and CO2 respiration at Oguta lake point one. Standard procedures were used to assess the soil parameters, and an AZ 77535 CO2 gas analyzer was held at arm's length to determine the CO2 concentration at the sample location. The mean values for pH (5.03), temperature (28.16 oC), electrical conductivity (108.56 uS/cm), moisture content (17.83 percent), and organic matter were 5.03, 28.16, 108.56, 108.56, and 17.83, respectively (1.35 percent). The mean weekly [CO2] concentrations (564 13.5 to 580.72.2 13.03 ppm) were greater than the global average (370 ppm) and all locations surrounding the lake, including the control site (425 2.5 to 438.2 2.0 ppm). Positive relationships were identified between [CO2] and R2 values of (0.262), (0.370), (0.304), (0.294), and (0.056), respectively. This demonstrates that CO2 respiration is regulated by soil characteristics. A rise in soil characteristics corresponded to an increase in CO2 concentration. These findings contribute to our understanding of how soil characteristics might be adjusted to reduce soil respired CO2 and, consequently, wetland contributions to global warming.
湿地通过呼吸作用排放的二氧化碳约占世界二氧化碳排放量的5%,而这被认为是由土壤条件控制的。本研究的目的是建立沼泽土壤的理化参数与奥古塔湖1点CO2呼吸之间的联系。使用标准程序评估土壤参数,并将AZ 77535 CO2气体分析仪保持一臂距离以确定样品位置的CO2浓度。pH(5.03)、温度(28.16 oC)、电导率(108.56 uS/cm)、含水量(17.83%)和有机质的平均值分别为5.03、28.16、108.56、108.56和17.83(1.35%)。周平均[CO2]浓度(564 13.5 ~ 580.72.2 13.03 ppm)高于全球平均值(370 ppm)和湖周围所有地点,包括对照地点(425 2.5 ~ 438.2 2.0 ppm)。[CO2]与R2分别为(0.262)、(0.370)、(0.304)、(0.294)和(0.056),呈正相关。这表明CO2呼吸受土壤特性的调节。土壤特征的增加与二氧化碳浓度的增加相对应。这些发现有助于我们理解如何调整土壤特征以减少土壤呼吸的二氧化碳,从而减少湿地对全球变暖的贡献。
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引用次数: 1
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Asian Journal of Material Science and Engineering
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