Pub Date : 2022-02-03DOI: 10.5772/intechopen.102387
T. Aizawa, T. Shiratori, T. Yoshino, Yohei Suzuki, T. Komatsu
The high-density plasma nitriding at 673 K and 623 K was employed to make 10% of nitrogen supersaturation on AISI316 base austenitic stainless steels. The processing parameters and nitrogen-hydrogen gas flow ratio were optimized to increase the yield of N2+ ion and NH-radical for efficient nitriding. The nitrided AISI316 specimens were prepared for multidimensional analysis to describe the fundamental features of low-temperature plasma nitriding. First, macroscopic evaluation revealed that nitrogen supersaturation induced the γ-lattice expansion and the higher nitrogen content than 4% of mass in depth. The mesoscopic analysis describes the holding temperature and initial grain-size effects on the microstructure changes. Plastic straining, grain-size refinement, and nitrogen zone-boundary diffusion processes advance with nitrogen supersaturation to drive the inner nitriding behavior. The microscopic analysis explains the microstructure refinement, the two-phase structuring, and the microstructure modification. Through this multi-dimensional analysis, the essential characteristics of the low-temperature plasma nitriding of 316 austenitic stainless steels were precisely understood to extend the engineering treatise on the bulk nitrogen stainless steels for surface modification and treatment of stainless steels by nitriding. This plasma nitriding was applied to strengthen and harden the AISI316 wire surfaces toward its application on surgery wires.
{"title":"Nitrogen Supersaturation of AISI316 Base Stainless Steels at 673 K and 623 K for Hardening and Microstructure Control","authors":"T. Aizawa, T. Shiratori, T. Yoshino, Yohei Suzuki, T. Komatsu","doi":"10.5772/intechopen.102387","DOIUrl":"https://doi.org/10.5772/intechopen.102387","url":null,"abstract":"The high-density plasma nitriding at 673 K and 623 K was employed to make 10% of nitrogen supersaturation on AISI316 base austenitic stainless steels. The processing parameters and nitrogen-hydrogen gas flow ratio were optimized to increase the yield of N2+ ion and NH-radical for efficient nitriding. The nitrided AISI316 specimens were prepared for multidimensional analysis to describe the fundamental features of low-temperature plasma nitriding. First, macroscopic evaluation revealed that nitrogen supersaturation induced the γ-lattice expansion and the higher nitrogen content than 4% of mass in depth. The mesoscopic analysis describes the holding temperature and initial grain-size effects on the microstructure changes. Plastic straining, grain-size refinement, and nitrogen zone-boundary diffusion processes advance with nitrogen supersaturation to drive the inner nitriding behavior. The microscopic analysis explains the microstructure refinement, the two-phase structuring, and the microstructure modification. Through this multi-dimensional analysis, the essential characteristics of the low-temperature plasma nitriding of 316 austenitic stainless steels were precisely understood to extend the engineering treatise on the bulk nitrogen stainless steels for surface modification and treatment of stainless steels by nitriding. This plasma nitriding was applied to strengthen and harden the AISI316 wire surfaces toward its application on surgery wires.","PeriodicalId":218102,"journal":{"name":"Stainless Steels [Working Title]","volume":"117 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-02-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"127629348","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2022-01-05DOI: 10.5772/intechopen.101782
Selma Attabi, A. Himour, L. Laouar, A. Motallebzadeh
316L is a type of austenitic stainless steel that offers a good combination of mechanical properties, corrosion resistance, and biocompatibility. In some industrial applications, it is necessary to proceed to finish treatments to extend the lifetime of the mechanical parts. In the present chapter, ball burnishing treatment is applied to improve the surface integrity of 316L since the performance behavior of parts is directly dependant on the surface properties of the used material. Both surface topography and surface microhardness of 316L after subjection to ball burnishing are studied. The number of burnishing passes is varied by up to five to investigate its effect on the results. Optical profilometer and atomic force microscopy (AFM) were used to analyze the surface roughness and surface topography texture while measurements of microhardness Vickers were proceeded to investigate the changes in surface hardening.
{"title":"Surface Integrity of Ball Burnished 316L Stainless Steel","authors":"Selma Attabi, A. Himour, L. Laouar, A. Motallebzadeh","doi":"10.5772/intechopen.101782","DOIUrl":"https://doi.org/10.5772/intechopen.101782","url":null,"abstract":"316L is a type of austenitic stainless steel that offers a good combination of mechanical properties, corrosion resistance, and biocompatibility. In some industrial applications, it is necessary to proceed to finish treatments to extend the lifetime of the mechanical parts. In the present chapter, ball burnishing treatment is applied to improve the surface integrity of 316L since the performance behavior of parts is directly dependant on the surface properties of the used material. Both surface topography and surface microhardness of 316L after subjection to ball burnishing are studied. The number of burnishing passes is varied by up to five to investigate its effect on the results. Optical profilometer and atomic force microscopy (AFM) were used to analyze the surface roughness and surface topography texture while measurements of microhardness Vickers were proceeded to investigate the changes in surface hardening.","PeriodicalId":218102,"journal":{"name":"Stainless Steels [Working Title]","volume":"354 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-01-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"115926725","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2022-01-05DOI: 10.5772/intechopen.101430
Temitope Olumide Olugbade
Stainless steels are widely recognized and find applications in many engineering industries and companies due to their excellent properties including high resistance to corrosion as a result of their minimum 10.5% chromium content, exceptional strength and durability, temperature resistance, high recyclability, and easy formability. In the present book chapter, the basic concepts of stainless steel including its applications, classifications, and corrosion properties will first be discussed. Thereafter, their corrosion behaviour will then be explained. The various methods by which the corrosion resistance behaviour can be significantly improved including surface treatments such as coatings/electrodepositions, alloying, mechanical treatment, and others will be discussed in detail.
{"title":"Corrosion Resistance, Evaluation Methods, and Surface Treatments of Stainless Steels","authors":"Temitope Olumide Olugbade","doi":"10.5772/intechopen.101430","DOIUrl":"https://doi.org/10.5772/intechopen.101430","url":null,"abstract":"Stainless steels are widely recognized and find applications in many engineering industries and companies due to their excellent properties including high resistance to corrosion as a result of their minimum 10.5% chromium content, exceptional strength and durability, temperature resistance, high recyclability, and easy formability. In the present book chapter, the basic concepts of stainless steel including its applications, classifications, and corrosion properties will first be discussed. Thereafter, their corrosion behaviour will then be explained. The various methods by which the corrosion resistance behaviour can be significantly improved including surface treatments such as coatings/electrodepositions, alloying, mechanical treatment, and others will be discussed in detail.","PeriodicalId":218102,"journal":{"name":"Stainless Steels [Working Title]","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-01-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"124104277","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-12-12DOI: 10.5772/intechopen.101388
I. Dey, Pallabi Manna, M. Yadav, Nisith Kumar Tewary, Jayanta Kumar Saha, Swarup Kumar Ghosh
In the present research, the effects of various alloying elements and microstructural constituents on the mechanical properties and corrosion behaviour have been studied for four different rebars. The microstructures of stainless steel and plain rebar primarily reveal equiaxed ferrite grains and ferrite-pearlite microstructures, respectively, with no evidence of transition zone, whereas tempered martensite at the outer rim, followed by a narrow bainitic transition zone with an internal core of ferrite-pearlite, has been observed for the thermomechanically treated (TMT) rebars. The hardness profiles obtained from this study display maximum hardness at the periphery, which decreases gradually towards the centre, thereby providing the classical U-shaped hardness profile for TMT rebars. The tensile test results confirm that stainless steel rebar exhibits the highest combination of strength (≈755 MPa) and ductility (≈27%). It has been witnessed that in Tafel plots, the corrosion rate increases for all the experimental rebars in 1% HCl solution, which is well expected because the acid solutions generally possess a higher corrosive environment than seawater (3.5% NaCl) due to their acidic nature and lower pH values. However, all the experimental results obtained from Tafel and Nyquist plots correlate well for both 1% HCl and 3.5% NaCl solutions.
{"title":"Study on the Perspective of Mechanical Properties and Corrosion Behaviour of Stainless Steel, Plain and TMT Rebars","authors":"I. Dey, Pallabi Manna, M. Yadav, Nisith Kumar Tewary, Jayanta Kumar Saha, Swarup Kumar Ghosh","doi":"10.5772/intechopen.101388","DOIUrl":"https://doi.org/10.5772/intechopen.101388","url":null,"abstract":"In the present research, the effects of various alloying elements and microstructural constituents on the mechanical properties and corrosion behaviour have been studied for four different rebars. The microstructures of stainless steel and plain rebar primarily reveal equiaxed ferrite grains and ferrite-pearlite microstructures, respectively, with no evidence of transition zone, whereas tempered martensite at the outer rim, followed by a narrow bainitic transition zone with an internal core of ferrite-pearlite, has been observed for the thermomechanically treated (TMT) rebars. The hardness profiles obtained from this study display maximum hardness at the periphery, which decreases gradually towards the centre, thereby providing the classical U-shaped hardness profile for TMT rebars. The tensile test results confirm that stainless steel rebar exhibits the highest combination of strength (≈755 MPa) and ductility (≈27%). It has been witnessed that in Tafel plots, the corrosion rate increases for all the experimental rebars in 1% HCl solution, which is well expected because the acid solutions generally possess a higher corrosive environment than seawater (3.5% NaCl) due to their acidic nature and lower pH values. However, all the experimental results obtained from Tafel and Nyquist plots correlate well for both 1% HCl and 3.5% NaCl solutions.","PeriodicalId":218102,"journal":{"name":"Stainless Steels [Working Title]","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-12-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128591060","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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