{"title":"Calorimetry","authors":"F. Winnefeld, A. Schöler, B. Lothenbach","doi":"10.1201/b19074-2","DOIUrl":"https://doi.org/10.1201/b19074-2","url":null,"abstract":"","PeriodicalId":365485,"journal":{"name":"A Practical Guide to Microstructural Analysis of Cementitious Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2018-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"123298710","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"High-resolution solid-state nuclear magnetic resonance spectroscopy of portland cement-based systems","authors":"Jørgen Skibsted","doi":"10.1201/b19074-6","DOIUrl":"https://doi.org/10.1201/b19074-6","url":null,"abstract":"","PeriodicalId":365485,"journal":{"name":"A Practical Guide to Microstructural Analysis of Cementitious Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2018-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"114223041","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Arnaud C. A. Muller, Jonathan Mitchell, Peter J. McDonald
As advanced teaching and training in the development of cementitious materials increase, the need has emerged for an up-to-date practical guide to the field suitable for graduate students and junior and general practitioners. This edited volume provides the cement science community with a state-of-the-art overview of analytical techniques used in cement chemistry to study the hydration and microstructure of cements. Each chapter focuses on a specific technique, not only describing the basic principles behind the technique, but also providing essential, practical details on its application to the study of cement hydration. Each chapter sets out present best practice, and draws attention to the limitations and potential experimental pitfalls of the technique. Databases that supply examples and that support the analysis and interpretation of the experimental results strengthen a very valuable ready reference.
{"title":"Proton nuclear magnetic resonance relaxometry","authors":"Arnaud C. A. Muller, Jonathan Mitchell, Peter J. McDonald","doi":"10.1201/B19074-7","DOIUrl":"https://doi.org/10.1201/B19074-7","url":null,"abstract":"As advanced teaching and training in the development of cementitious materials increase, the need has emerged for an up-to-date practical guide to the field suitable for graduate students and junior and general practitioners. \u0000This edited volume provides the cement science community with a state-of-the-art overview of analytical techniques used in cement chemistry to study the hydration and microstructure of cements. Each chapter focuses on a specific technique, not only describing the basic principles behind the technique, but also providing essential, practical details on its application to the study of cement hydration. Each chapter sets out present best practice, and draws attention to the limitations and potential experimental pitfalls of the technique. Databases that supply examples and that support the analysis and interpretation of the experimental results strengthen a very valuable ready reference.","PeriodicalId":365485,"journal":{"name":"A Practical Guide to Microstructural Analysis of Cementitious Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2018-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"114252842","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The determination of pore size following the technique of mercury intrusion is based on the behavior of “nonwetting” liquids in capillary. A liquid coming in contact with a solid porous material and behaving as a non wetting agent (namely if the contact angle of the liquid with that solid material exceeds 90°) cannot be spontaneously absorbed by the pores of the solid itself, because of surface tension. However, this resistance to penetration can be won by applying an external pressure. Required pressure depends on the pore size. The relation between the pore size and the applied pressure, assuming the pore is cylindrical, is expressed as:
{"title":"Mercury intrusion porosimetry","authors":"","doi":"10.1201/b19074-9","DOIUrl":"https://doi.org/10.1201/b19074-9","url":null,"abstract":"The determination of pore size following the technique of mercury intrusion is based on the behavior of “nonwetting” liquids in capillary. A liquid coming in contact with a solid porous material and behaving as a non wetting agent (namely if the contact angle of the liquid with that solid material exceeds 90°) cannot be spontaneously absorbed by the pores of the solid itself, because of surface tension. However, this resistance to penetration can be won by applying an external pressure. Required pressure depends on the pore size. The relation between the pore size and the applied pressure, assuming the pore is cylindrical, is expressed as:","PeriodicalId":365485,"journal":{"name":"A Practical Guide to Microstructural Analysis of Cementitious Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2018-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"117081614","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Characterisation of development of cement hydration using chemical shrinkage METTE GEIKER","authors":"","doi":"10.1201/b19074-3","DOIUrl":"https://doi.org/10.1201/b19074-3","url":null,"abstract":"","PeriodicalId":365485,"journal":{"name":"A Practical Guide to Microstructural Analysis of Cementitious Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2018-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"127466817","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
M. Palacios, Hadi Kazemi-Kamyab, S. Mantellato, P. Bowen
{"title":"Laser diffraction and gas adsorption techniques","authors":"M. Palacios, Hadi Kazemi-Kamyab, S. Mantellato, P. Bowen","doi":"10.1201/B19074-10","DOIUrl":"https://doi.org/10.1201/B19074-10","url":null,"abstract":"","PeriodicalId":365485,"journal":{"name":"A Practical Guide to Microstructural Analysis of Cementitious Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2018-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"116994141","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Xin, Pan, I. Krivorotov, Xiaoqing Pan, Z. Siwy, P. Taborek, Jing Xia, Huolin L. Xin, Luis Jauregui, Javier Sanchez
{"title":"Electron microscopy","authors":"Xin, Pan, I. Krivorotov, Xiaoqing Pan, Z. Siwy, P. Taborek, Jing Xia, Huolin L. Xin, Luis Jauregui, Javier Sanchez","doi":"10.1201/b19074-8","DOIUrl":"https://doi.org/10.1201/b19074-8","url":null,"abstract":"","PeriodicalId":365485,"journal":{"name":"A Practical Guide to Microstructural Analysis of Cementitious Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2018-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"127808663","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
M. Palacios, Hadi Kazemi-Kamyab, S. Mantellato, P. Bowen
{"title":"Ternary phase diagrams applied to hydrated cement","authors":"M. Palacios, Hadi Kazemi-Kamyab, S. Mantellato, P. Bowen","doi":"10.1201/b19074-11","DOIUrl":"https://doi.org/10.1201/b19074-11","url":null,"abstract":"","PeriodicalId":365485,"journal":{"name":"A Practical Guide to Microstructural Analysis of Cementitious Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2015-12-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"116660346","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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