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Joining aluminium/nicalon composite by diffusion bonding 扩散连接铝/nicalon复合材料
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(95)00016-G
R.S. Bushby, V.D. Scott

The joining of aluminium/Nicalon composite has been investigated by diffusion bonding under pressure using metal interlayers. Bond strengths have been measured using a simple shear jig and the joint microstructures characterised by electron microscopy and electron-probe microanalysis. Using interlayers of copper and copper-silver alloy, joints were readily formed at 550 and 510°C, respectively, as a result of the formation of eutectic liquid which helped to disrupt the oxide film on the aluminium matrix and promote metal diffusion across the joint interface. In the case of copper, however, oxidation at the edge of the interlayer limited the bonded area to ∼80%. Using an interlayer of aluminium alloy (2124), a temperature of 500°C was sufficient to produce a satisfactory joint with ∼100% bonded area, in this case the aluminium oxide film being disrupted by reaction with magnesium in the alloy interlayer. The shear strength of all bonded specimens was ∼50 MPa, with failure occurring mainly through the adjacent composite rather than at the joint interface.

研究了铝/Nicalon复合材料在压力下用金属中间层进行扩散连接的方法。用简单的剪切夹具测量了粘结强度,并用电子显微镜和电子探针显微分析表征了接头的微观结构。在550°C和510°C的温度下,铜和铜银合金的中间层很容易形成接头,这是因为共晶液体的形成有助于破坏铝基体上的氧化膜,促进金属在接头界面上的扩散。然而,在铜的情况下,中间层边缘的氧化将键合面积限制在~ 80%。使用铝合金(2124)中间层,500℃的温度足以产生一个令人满意的连接,连接面积为100%,在这种情况下,氧化铝膜被合金中间层中的镁反应破坏。所有粘结试件的抗剪强度均为~ 50 MPa,破坏主要通过相邻复合材料发生,而不是在节理界面发生。
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引用次数: 3
NITINOL-reinforced plates: Part III. Dynamic characteristics 镍钛诺增强板:第三部分。动态特性
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(95)93982-2
J. Ro, A. Baz

The dynamic characteristics of NITINOL-reinforced composite plates are controlled by heating sets of NITINOL fibers embedded inside these plates. The activation of the shape memory effect of these NITINOL fibers increases the elastic energy, enchances the stiffness of the composite plates and modifies their modal characteristics. One of the objectives of the resulting modal modification is to shift the modes of vibration of the plates away from the excitation frequencies in order to avoid undesirable resonances. In this way, the modal characteristics can be tailored in response to the external disturbances acting on the plates. The classical finite element approach is used to form the equations of motion of the assembly of NITINOL-reinforced plate elements and the appropriate boundary conditions are then applied. The solution of the eigenvalues of the resulting homogeneous equations gives the natural frequencies of the NITINOLreinforced plate as influenced by the properties of the composite matrix and the NITINOL fibers. It is important to note that these properties are influenced by the temperature distribution inside the composite plate which is developed by virtue of activating and de-activating the NITINOL fibers. Emphasis is placed on the effect of intentional electrical heating of a selected subset of the NITINOL fibers on the overall dynamics of the plates. The effect of the associated thermal energy propagating through the composite on the unintentional thermal activation of additional subsets of the NITINOL fibers is accounted for. Such an effect is not only significant, but also essential to the thorough understanding of the operation of the NITINOL-reinforced plates.

镍钛醇增强复合材料板的动态特性是由嵌入板内的镍钛醇纤维加热组控制的。NITINOL纤维的形状记忆效应的激活增加了复合材料板的弹性能,提高了复合材料板的刚度,改变了复合材料板的模态特性。由此产生的模态修正的目标之一是将板的振动模态从激励频率移开,以避免不希望的共振。通过这种方式,模态特性可以根据作用在板上的外部扰动进行调整。采用经典有限元方法建立了镍钛醇增强板构件组合的运动方程,并采用了相应的边界条件。得到的齐次方程的特征值的解给出了复合材料基体和NITINOL纤维特性对NITINOL增强板固有频率的影响。值得注意的是,这些性能受到复合材料板内部温度分布的影响,这是由于NITINOL纤维的活化和失活而产生的。重点放在有意电加热NITINOL纤维的一个子集对板的整体动力学的影响。通过复合材料传播的相关热能对NITINOL纤维附加子集的无意热激活的影响被考虑在内。这样的效果不仅意义重大,而且对于彻底了解nitinol增强板的操作也是必不可少的。
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引用次数: 28
Stress-free edge influence on thermal fatigue damage in an SCS-6/Ti-24A1-11Nb composite 无应力边缘对SCS-6/Ti-24A1-11Nb复合材料热疲劳损伤的影响
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(94)00102-F
William C. Revelos, Joseph L. Kroupa

Unidirectionally reinforced [90]8 specimens of an SCS-6/Ti-24A1-11Nb (at.%) composite (35 vol.% fiber) in three different gage-section widths were thermally cycled in air between 150 and 815°C for 500 cycles. During thermal cycling, matrix cracks initiated at the composite surface and propagated into the composite normal to the fiber direction. However, near the stress-free edges of all specimens, a region void of cracks existed which extended an average of 5.4 fiber diameters into the width of the composite. This cracking pattern was attributed to the presence of a thermally induced cyclic tensile residual stress which dissipates to zero near the stress-free edge of the composite. The finite element method was employed to determine how the fiber-matrix interface shear resistance influences the development of these residual stresses. Using coulomb friction as a measure of shear resistance, the matrix residual stresses in the fiber direction had a peak value of 500 MPa. A frictional coefficient range of 0.18–0.22 was found to give between 95% and 99% of this peak value within 5.4 fiber diameters from the edge. Thermal cycling of the model between 150 and 815°C provided evidence that the resultant cyclic stresses were tensile in nature and were suggested as the probable cause of the periodic surface cracks. The reduction in post-cycling transverse strength with increasing gage-section width indicated that the smaller-width specimens exhibited less damage per cross-sectional area than the wider specimens.

单向增强[90]8个SCS-6/Ti-24A1-11Nb (at.%)复合材料(35 vol.%纤维)在三种不同规格截面宽度下在150至815°C的空气中热循环500次。在热循环过程中,基体裂纹在复合材料表面萌生,并沿纤维方向向复合材料法向扩展。然而,在所有试样的无应力边缘附近,存在一个空洞的裂纹区域,其宽度平均延伸到复合材料的5.4纤维直径。这种开裂模式归因于热诱导的循环拉伸残余应力的存在,该应力在复合材料的无应力边缘附近消散为零。采用有限元法分析了纤维-基体界面剪切阻力对残余应力发展的影响。以库仑摩擦作为抗剪性能指标,纤维方向的基体残余应力峰值为500 MPa。摩擦系数范围为0.18-0.22,在距离边缘5.4纤维直径的范围内给出了该峰值的95%至99%。模型在150 - 815°C之间的热循环提供了证据,表明所产生的循环应力本质上是拉伸的,并且被认为是周期性表面裂纹的可能原因。循环后横向强度随截面宽度的增加而降低,表明宽度较小的试件在每横截面积上的损伤要小于宽度较大的试件。
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引用次数: 0
Matrix crack induced stiffness reductions in [(Om/90n/+ θp/- θq)s]M composite laminates [(Om/90n/+ θp/- θq)s]M复合材料层合板基体裂纹引起的刚度降低
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(95)93983-3
Erik Adolfsson, Peter Gudmundson

Two- and three-dimensional linearly elastic glass/epoxy and carbon/epoxy laminates of the type [(Om/90n/+ θp/-θq)s]M containing periodically distributed matrix cracks have been analysed by aid of the finite element method. The presented finite element model enables modelling of several important thick and thin ply stacking sequences like cross-plies, angle plies and quasi-isotropic laminates. Due to periodicity it suffices to model a representative volume element of the laminate. The boundaries of this unit cell represent prospective crack surfaces. In this way varying crack configurations and crack densities could be simulated. By application of periodic boundary conditions the stiffness tensors for laminates containing different crack configurations were calculated. The results are presented in the form of reduced engineering stiffness parameters as functions of matrix crack densities for a thick quasi-isotropic [(0°/90°/+45°/−45°)s]M glass/epoxy laminate, a thick [(0°/90°/+55°/−55°)s]M carbon/epoxy laminate and a thin (0°/+45°/−45°)s glass/epoxy laminate. Comparisons are made to an approximate analytic model developed previously. An excellent agreement between the analytic predictions and the finite element results was found for all cases under consideration.

用有限元法分析了含周期性分布基体裂纹的[(Om/90n/+ θp/-θq)s]M型线弹性玻璃/环氧树脂和碳/环氧树脂层合板的二维和三维结构。所提出的有限元模型能够对交叉层、角度层和准各向同性层压板等几种重要的厚层和薄层叠加序列进行建模。由于其周期性,建立一个具有代表性的层压板体积单元就足够了。这个单元格的边界代表未来的裂纹表面。通过这种方法可以模拟不同的裂纹形态和裂纹密度。应用周期边界条件,计算了含不同裂纹形态层合板的刚度张量。结果表明:厚的准各向同性[(0°/90°/+45°/−45°)s]M玻璃/环氧层合板、厚的[(0°/90°/+55°/−55°)s]M碳/环氧层合板和薄的(0°/+45°/−45°)s玻璃/环氧层合板的工程刚度参数随基体裂纹密度的减小。与先前开发的近似分析模型进行了比较。在考虑的所有情况下,分析预测结果与有限元结果非常吻合。
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引用次数: 34
Influence of damage on the creep behaviour of ceramic matrix composites 损伤对陶瓷基复合材料蠕变行为的影响
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(95)00058-U
F. Lamouroux , J.L. Vallés, M. Steen
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引用次数: 4
The biomimetic design of worst bonding interface for ceramic matrix composites 陶瓷基复合材料最差结合界面的仿生设计
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(95)00061-Q
Benlian Zhou
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引用次数: 6
Experimental and theoretical study of the thermal expansion behavior of aluminium reinforced by continuous ceramic fibers 连续陶瓷纤维增强铝的热膨胀行为的实验与理论研究
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(95)93978-5
H.J. Böhm, H.P. Degischer, W. Lacom, J. Qu

The thermal expansion response of an ALTEX-aluminium continuous fiber reinforced metal matrix composite produced by gas pressure infiltration was measured experimentally by dilatometry. Theoretical predictions for the composite's thermal expansion behavior were made with simple analytical estimates and with a unit cell model employing the Finite Element method. By correlating experimental and computational results, improved data on the fibers' coefficient of thermal expansion were obtained.

用膨胀法测量了气压渗透法制备的altex -铝连续纤维增强金属基复合材料的热膨胀响应。对复合材料的热膨胀行为进行了理论预测,采用简单的分析估计和采用有限元方法的单位胞模型。将实验结果与计算结果相比较,得到了较好的纤维热膨胀系数数据。
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引用次数: 16
High temperature mechanical and thermal stability of silicate matrix composites 硅酸盐基复合材料的高温力学和热稳定性
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(95)00057-T
S. Sutherland, K.P. Plucknett , M.H. Lewis

Two silicate matrix composites, Pyrex/Nicalon and BaO-MgO-Al2O3-SiO2 (BMAS)/ Tyranno, have been used to study composite stability with respect to time at temperature, and under applied stress. Samples aged in an oxidizing atmosphere have been tested in flexure at room temperature, and also by fibre “push-down” to investigate the interfacial properties. Tensile tests have been carried out from room temperature up to 1200°C on the BMAS material, and it was found that a steady degradation in strength occurred from 500 to 1100°C, with a small but significant increase up to 1200°C. Creep experiments have been performed on both the Pyrex and BMAS materials, it was found that Pyrex has a creeping matrix and elastic fibres below the matrix softening point, whereas the BMAS composite showed creep in both components, though at long times the creep rate was shown to be fibre controlled. A simple model for the development of strain with time is reported and used to obtain values for the creep rate of both the matrix and fibres. Activation energies were calculated for the creep processes in both matrix and fibres. The values obtained were: Pyrex, 256 kJ mol−1, BMAS matrix, 300 kJ mol−1 and the Tyranno fibres, 495 kJ mol−1.

用两种硅酸盐基复合材料Pyrex/Nicalon和BaO-MgO-Al2O3-SiO2 (BMAS)/ Tyranno研究了复合材料在温度和外加应力下的稳定性。在氧化气氛中老化的样品在室温下进行了弯曲测试,也通过纤维“下推”来研究界面特性。在室温至1200°C范围内对BMAS材料进行了拉伸试验,发现在500至1100°C范围内强度稳定下降,在1200°C范围内强度有小幅但显著的提高。对Pyrex和BMAS材料进行了蠕变实验,发现Pyrex具有蠕变基体和弹性纤维,低于基体软化点,而BMAS复合材料在两种组分中都表现出蠕变,尽管在长时间内蠕变速率被证明是纤维控制的。报告了应变随时间发展的一个简单模型,并用于获得基体和纤维的蠕变速率值。计算了基体和纤维蠕变过程的活化能。得到的值为:Pyrex, 256 kJ mol−1,BMAS基质,300 kJ mol−1,Tyranno纤维,495 kJ mol−1。
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引用次数: 15
Floquet Analysis of Lamb Waves Propagating in Periodically-Layered Composites Lamb波在周期性层状复合材料中传播的Floquet分析
Pub Date : 1995-01-01 DOI: 10.1007/978-1-4615-1987-4_19
A. Safaeinili, D. Chimenti
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引用次数: 12
Design of multiple-row bolted composite joints under general in-plane loading 一般面内荷载作用下多排螺栓复合连接的设计
Pub Date : 1995-01-01 DOI: 10.1016/0961-9526(95)00044-N
Ingvar Eriksson, Jan Bäcklund, Peter Möller

A special purpose finite element method for design of multiple-row composite joints under generalized in-plane loading is presented. The stress analysis is carried out in two steps. In the first step (source analysis), the distribution of applied load within the joint and between the fasteners is determined. In the second step (target analysis), a series of detailed stress analyses of regions containing single bolt holes is performed to determine the stress distribution around the bolt holes. Far field stress distributions obtained in the source analysis are automatically transferred to the boundaries of the target models. The failure analysis includes evaluation of the failure modes (net-section, bearing and shear-out) according to simple point stress criteria. Experiments were performed using single-bolt specimens to validate the target and failure analyses for a graphite/epoxy material system. A complete analysis of a multiple-row glass-fiber/polyester joint is carried out. Computed results show good agreement with experimental data.

提出了一种适用于广义面内荷载作用下多排复合节点设计的专用有限元方法。应力分析分两步进行。在第一步(源分析)中,确定接头内部和紧固件之间的载荷分布。第二步(目标分析),对包含单个螺栓孔的区域进行一系列详细的应力分析,以确定螺栓孔周围的应力分布。源分析得到的远场应力分布自动转移到目标模型的边界上。破坏分析包括根据简单的点应力准则评估破坏模式(净截面、承载和剪切)。使用单螺栓试件进行了实验,以验证石墨/环氧树脂材料体系的目标和失效分析。对多排玻璃纤维/聚酯接头进行了全面分析。计算结果与实验数据吻合较好。
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引用次数: 33
期刊
Composites Engineering
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