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Mechanochemical synthesis of icosahedral phases in Mg-Zn-Al and Mg-Cu-Al alloys Mg-Zn-Al和Mg-Cu-Al合金中二十面体相的机械化学合成
Pub Date : 1989-06-01 DOI: 10.1016/0168-7336(89)80026-9
E.Yu. Ivanov, I.G. Konstanchuk, B.D. Bokhonov, V.V. Boldyrev

Mechanical alloying (MA) has been used to obtain the icosahedral phases: i-(Mg-Zn-Al) and i-(Mg-Cu-Al) from metal powders. X-ray diffraction peaks are identical to those of icosahedral obtained by the melt spun technique. SAD patterns from MA samples indicate 2,3,6 and 5-fold symmetry. Annealing of the MA icosahedral phases leads to the formation of related cubic Frank-Kasper phases, that can be transformed into the icosahedral phases by MA. The disclination network which appears in the cubic phase plastically deformed by MA seems to be intrinsic to producing an aperiodic phase with long-range icosahedral order.

采用机械合金化(MA)技术从金属粉末中获得了i-(Mg-Zn-Al)和i-(Mg-Cu-Al)二十面体相。x射线衍射峰与熔融纺丝法得到的二十面体的x射线衍射峰相同。MA样品的SAD模式显示2、3、6和5重对称。MA二十面体相的退火形成了相关的立方Frank-Kasper相,这些相可以通过MA转化为二十面体相。在MA塑性变形的立方相中出现的偏斜网络似乎是产生具有长程二十面体有序的非周期相所固有的。
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引用次数: 47
Synthesis and characterization of several La3+ and Sr2+ vanadates, active as methanol oxidation catalysts 几种具有甲醇氧化活性的La3+和Sr2+钒酸盐的合成与表征
Pub Date : 1989-06-01 DOI: 10.1016/0168-7336(89)80023-3
J.E. Sueiras , P. Salagre, J.L.G. Fierro

Substitution of Sr2+ for La3+ in strontium orthovanadates gives materials with interesting bulk and surface properties.

The results indicate that there are correlations between increasing selectivities to formaldehyde and (i) the decreasing crystallinity of the mixed vanadates, (ii) the increasing La migration from the surface towards the bulk, (iii) the decreasing initial temperature of reduction of V5+ in the catalysts.

The migration of the La3+ could leave the oxygen of the crystal structure more accessible to the reducing hydrogen (during TPR measurements) and to the reactants in the catalytic methanol oxidation. This La3+ migration into the bulk may also be the cause of the loss of the crystallinity. In addition the La3+ vacancies in the isostructural mixed vanadate catalysts should be responsible for their selectivities in the oxidation of methanol to formaldehyde.

在正钒酸锶中用Sr2+取代La3+,得到了具有有趣的体积和表面性质的材料。结果表明,对甲醛选择性的提高与(1)混合钒酸盐结晶度的降低,(2)La从表面向体体迁移的增加,(3)催化剂中V5+还原初始温度的降低存在相关性。La3+的迁移可以使晶体结构中的氧更容易被还原性氢(在TPR测量期间)和催化甲醇氧化中的反应物所接近。La3+向体内的迁移也可能是结晶性丧失的原因。此外,同构混合钒酸盐催化剂中的La3+空位可能是其甲醇氧化制甲醛选择性的原因。
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引用次数: 1
Interaction of carbon monoxide with the hydrogen storage alloy, CaNi5; kinetic and surface studies 一氧化碳与贮氢合金CaNi5的相互作用动力学和表面研究
Pub Date : 1989-06-01 DOI: 10.1016/0168-7336(89)80025-7
M.P.Sridhar Kumar, B. Viswanathan, C.S. Swamy, V. Srinivasan

Impurities in hydrogen affect the storage capacity of intermetallic systems. Carbon monoxide interacts with nickel-containing intermetallics such as CaNi5 to give volatile nickel carbonyl which leads to a fall in the transition metal content, the hydrogen storage capacity and the sorption kinetics. The implications of these effects are investigated here by X-ray Photoelectron Spectroscopy (XPS) and sorption kinetic data.

氢中的杂质影响金属间化合物体系的储存能力。一氧化碳与含镍的金属间化合物如CaNi5相互作用,产生挥发性羰基镍,导致过渡金属含量下降,储氢能力下降,吸附动力学下降。本文用x射线光电子能谱(XPS)和吸附动力学数据研究了这些效应的意义。
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引用次数: 5
Preferential formation of aluminium chloride by chlorination of a highly reactive powder obtained from metakaolin or kaolin by hydrochloric acid treatment 由偏高岭土或高岭土经盐酸处理得到的高活性粉末经氯化反应优先形成氯化铝
Pub Date : 1989-06-01 DOI: 10.1016/0168-7336(89)80021-X
Gert Blumenthal ∗, Gerhard Wegner

It has been found that highly reactive amorphous powders are obtained by treatment with concentrated hydrochloric acid of metakaolin or kaolin, followed by removal of the liquid by distillation and calcination of the residue. The result is a porous silica homogeneously mixed with chloride-containing alumina beginning to react with gaseous carbon tetrachloride at 450 K. At temperatures above 700 K aluminium chloride is formed in high yield and high selectivity. The reactivity of these powders is such that they are chlorinated even by gaseous silicon tetrachloride, a compound known to be stable towards metakaolinite up to 1300 K! Some advantages of technological relevance are listed in comparison to leaching and other dissolution processes.

用浓盐酸处理偏高岭土或高岭土,然后用蒸馏和焙烧的方法除去液体,可以得到高活性的非晶态粉末。结果是多孔二氧化硅与含氯化物的氧化铝均匀混合,在450 K时开始与气态四氯化碳反应。在700 K以上的温度下,以高收率和高选择性形成氯化铝。这些粉末的反应性是这样的,它们甚至被气态的四氯化硅氯化,一种已知的对偏高岭石稳定到1300 K的化合物!与浸出和其他溶解工艺相比,列举了一些技术相关的优点。
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引用次数: 2
Autocatalytic effect in MoO3 reduction in hydrogen 氢还原MoO3的自催化效应
Pub Date : 1989-04-01 DOI: 10.1016/0168-7336(89)80010-5
J. Słoczyński
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引用次数: 12
Oxidation behaviour of nitrided iron-silicon alloys 氮化铁硅合金的氧化行为
Pub Date : 1989-04-01 DOI: 10.1016/0168-7336(89)80011-7
Dong-Bok Lee, G. Simkovich
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引用次数: 1
Meeting report 会议报告
Pub Date : 1989-04-01 DOI: 10.1016/0168-7336(89)80018-X
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引用次数: 0
Editorial advisory board 编辑顾问委员会
Pub Date : 1989-04-01 DOI: 10.1016/0168-7336(89)80001-4
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引用次数: 0
Mechanistic aspects of atomization processes in microwave-induced plasma afterglows 微波诱导等离子体余辉中原子化过程的机理
Pub Date : 1989-04-01 DOI: 10.1016/0168-7336(89)80007-5
C. Vinckier ∗, S. De Jaegere

Some mechanistic aspects of the atomization processes in the afterglow of microwave-induced plasmas are reconsidered. Besides lattice atomization, where only heterogeneous interactions between radicals and the solid occur, a pure gas-phase atomization process also has to be taken into account. The latter mechanism becomes dominant with the chlorides or organic salts of transition metals.

The role of charged species in the overall atomization process is found to be negligible, indicating that an electrochemical mechanism is not important in most cases.

重新考虑了微波等离子体余辉中原子化过程的一些机理。除了晶格原子化,其中只有自由基和固体之间的非均相相互作用发生,纯气相原子化过程也必须考虑。后一种机制在过渡金属的氯化物或有机盐类中占主导地位。带电物质在整个雾化过程中的作用可以忽略不计,这表明电化学机制在大多数情况下并不重要。
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引用次数: 2
Initial stages of the interaction of nitrous oxide and oxygen with the (100) silicon surface under low pressures 在低压下氧化亚氮和氧与(100)硅表面相互作用的初始阶段
Pub Date : 1989-04-01 DOI: 10.1016/0168-7336(89)80002-6
M.R. Baklanov, V.N. Kruchinin, S.M. Repinsky, A.A. Shklyaev

The kinetics of the interaction of oxygen and nitrous oxide with the (100) silicon surface within the temperature range 20–830°C has been studied. At temperatures between 20 and 600°C, irreversible supermonolayer gas chemisorption occurs. At temperatures between 700 and 830°C, the character of the interaction of N2O and O2 with the silicon surface is determined by the ratio of the oxidizer pressure and the surface temperature of the sample. This results in either etching of the sample surface with relief formation or growth of a silicon dioxide layer on the surface. Reversible adsorption of the oxidizer molecules on the initially formed oxide layer experimentally observed here for the first time plays a key role in the mechanism of SiO2 formation.

研究了氧和氧化亚氮在20 ~ 830℃范围内与(100)硅表面相互作用的动力学。温度在20 ~ 600℃之间,发生不可逆的超单层气体化学吸附。在700 ~ 830℃的温度范围内,N2O和O2与硅表面的相互作用特性由氧化剂压力与样品表面温度的比值决定。这导致样品表面的蚀刻与浮雕形成或表面上二氧化硅层的生长。首次在实验中观察到氧化分子在初始形成的氧化层上的可逆吸附,在SiO2的形成机制中起着关键作用。
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引用次数: 10
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Reactivity of Solids
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