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Formulation of Watermelon Rind (Citrullus vulgaris schard) and Secang (Caesalpinia sappan L.) Jam as Functional Food Rich in Antioxidants 西瓜皮(Citrullus vulgaris schard)和西瓜皮(Caesalpinia sappan L.)的配方果酱是富含抗氧化剂的功能性食品
Pub Date : 2023-08-14 DOI: 10.30598//ijcr.2023.11-rah
Rahmawati Aziz, Elfira Jumrah, Ayu Safitri Agustina, Andi Nur Fitriani Abubakar, A. Mutiara Zulkarnain
The body's immune system is one of the natural defenses in the human body, functioning to ward off various diseases, including those that emerged after the Covid-19 pandemic. One plant with potential as an antioxidant and easily found in the environment is watermelon. Jam made from watermelon rind and secang wood, with various formulations, namely 100% watermelon rind: 0% secang (F1), 90% watermelon rind: 10% secang (F2), 80% watermelon rind: 2% secang (F3), and 70% watermelon rind: 3% secang (F4), is expected to possess good antioxidant properties. A promising antioxidant formulation for watermelon rind jam and secang is the one with 70% watermelon rind and 30% secang (F4), having an IC50 value of 144.27 g/mL, which is classified as a moderate antioxidant. Among the four jam formulations, panelists preferred the jam formulation (F4) without the addition of sweetened condensed milk in terms of color and texture. However, for the jam formulation (F4) with the addition of sweetened condensed milk, panelists favored it in terms of aroma and taste. The jam formulation (F4) meets the quality standards for fruit jam based on INS 3746:2008, including total plate count, arsenic, and tin categories.
人体的免疫系统是人体的天然防御系统之一,可以抵御各种疾病,包括新冠肺炎大流行后出现的疾病。西瓜是一种很容易在环境中发现的具有抗氧化剂潜力的植物。以西瓜皮和香槟木为原料,采用100%西瓜皮:0%香槟木(F1)、90%西瓜皮:10%香槟木(F2)、80%西瓜皮:2%香槟木(F3)、70%西瓜皮:3%香槟木(F4)等配方制成的果酱具有良好的抗氧化性能。以70%西瓜皮和30%西瓜皮(F4)为原料的西瓜皮果酱和西瓜皮的抗氧化性能较好,IC50值为144.27 g/mL,属于中等抗氧化剂。在四种果酱配方中,小组成员在颜色和质地方面更倾向于不添加甜炼乳的果酱配方(F4)。然而,对于添加了甜炼乳的果酱配方(F4),小组成员在香气和味道方面都很喜欢它。果酱配方(F4)符合基于INS 3746:2008的果酱质量标准,包括总盘子数、砷和锡类别。
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引用次数: 0
Water Stability Characteristic of Nile Tilapia (Oreochromis niloticus) Feed Coated with Tapioca Flour-beeswax-based Edible Coating 木薯粉-蜂蜡基可食用涂层对尼罗罗非鱼饲料水稳定性的影响
Pub Date : 2023-08-09 DOI: 10.30598//ijcr.2023.11-ing
Inggit Kresna Maharsih, Fadhil Muhammad Tarmidzi, Memik Dian Pusfitasari, Riza Alviany, Ahmad Yuli, Asnawi Asnawi
One of the reasons in increasing water turbidity in nile tilapia aquaculture is the presence of spoilage in fish feed that is easily disintegrate and decompose as organic matters in the water. Therefore, a thin layer or edible coating is needed to coat the tilapia feed to slow down the decomposition of the feed due to water absorption. The main ingredients for tilapia feed are tapioca flour added with beeswax solution and glycerol as a plasticizer. In this study, the glycerol concentrations used were 3%, 5%, and 7%, and the beeswax concentrations used were 0.25% w/v, 0.50 % w/v, and 0.75 % w/v. The purpose of this study was analysed the effect of plasticizers and beeswax on the characteristics of the edible coating. The method used to coat tilapia feed is the dipping method, where the product is dipped in a coating solution. The results of the research can be demonstrated by performing a and functional group test using FTIR spectra, contact angle test, and water resistance test of coated fish feed.
尼罗罗非鱼养殖水体浑浊度增加的原因之一是鱼饲料中存在腐坏物,易在水中分解为有机物。因此,需要在罗非鱼饲料中包裹一层薄薄的或可食用的涂层,以减缓饲料因吸水而分解的速度。罗非鱼饲料的主要成分是木薯粉,添加蜂蜡溶液和甘油作为增塑剂。在本研究中,使用的甘油浓度分别为3%、5%和7%,蜂蜡浓度分别为0.25%、0.50%和0.75% w/v。研究了增塑剂和蜂蜡对食用涂料特性的影响。罗非鱼饲料包衣的方法是浸渍法,将产品浸在包衣溶液中。研究结果可以通过FTIR光谱测试、接触角测试和涂膜鱼饲料耐水性测试来验证。
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引用次数: 0
Biosynthesis of ZnO Nanoparticles from Aqueous Extract of Moringa Oleifera L.: Its Application as Antibacterial and Photocatalyst 辣木水提物生物合成ZnO纳米粒子及其抗菌和光触媒应用
Pub Date : 2022-08-01 DOI: 10.15294/ijcs.v11i2.52498
Fastabiqul Khairati Rhamdiyah, D. K. Maharani
ZnO nanoparticles were successfully synthesized by the biosynthesis method using water extract of Moringa leaf (Moringa oleifera L.) as a reducing agent and stabilizer as well as a capping agent. This study aimed to characterize ZnO nanoparticles and their application as antibacterial and photocatalyst. Characterization was carried out using Fourier Transform Infrared (FT-IR) Spectroscopy and X-Ray Diffraction (XRD). The biosynthesis ZnO nanoparticles have a hexagonal wurtzite phase with an average crystal size of 16.97 nm and a crystallinity level of 78.49%. Antibacterial activity of ZnO nanoparticles with concentrations of 3%, 6%, 9% resulted in an average inhibition zone of bacterial growth in S. aureus was 19.6  0.16; 21.8  0.33; 24.3  0.14  and in E.coli it is 9.87  0.2; 11.3  0.04; 11.57  0.06. The greater the concentration of ZnO nanoparticles, the larger the diameter of the inhibition zone. The result of photodegradation of methylene blue is greatest with variations in the mass of ZnO nanoparticles and the concentration of methylene blue is 95% with a nanoparticle mass of 120 mg, methylene blue concentration of 10 ppm, and an irradiation time of 150 minutes.
以辣木叶水提物为还原剂、稳定剂和封盖剂,采用生物合成方法成功合成了ZnO纳米颗粒。本研究旨在研究氧化锌纳米颗粒及其在抗菌和光催化剂方面的应用。利用傅里叶变换红外光谱(FT-IR)和x射线衍射(XRD)对其进行了表征。生物合成ZnO纳米颗粒为六方纤锌矿相,平均晶粒尺寸为16.97 nm,结晶度为78.49%。3%、6%、9%氧化锌纳米粒子对金黄色葡萄球菌的平均抑菌带为19.6 ~ 0.16;21.8 - 0.33;大肠杆菌为9.87 0.2;11.3 - 0.04;11.57 - 0.06。ZnO纳米粒子的浓度越大,抑制带的直径越大。当纳米颗粒质量为120 mg、亚甲基蓝浓度为10 ppm、辐照时间为150 min时,亚甲基蓝的光降解效果随ZnO纳米颗粒质量的变化而变化,亚甲基蓝的光降解效果为95%。
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引用次数: 1
Synthesis of The Tangerine-based Cdots and AgNp-Cdots Composite 橘子基Cdots及AgNp-Cdots复合材料的合成
Pub Date : 2022-08-01 DOI: 10.15294/ijcs.v11i2.55582
Aprilia Kristian, S. Wahyuni
Silver nanoparticles (AgNp) have been widely developed, one of which is an antibacterial agent. The ability of AgNp to inhibit bacteria is unquestionable. These properties and characteristics can be studied further by adding defects. The defect used is Cdots from tangerines. Cdots are new materials that can be synthesized from natural materials and have unique properties. AgNp itself was synthesized by the chemical reduction method with sodium citrate as a reducing agent, while Cdots was synthesized by hydrothermal method. The results of the synthesis were analyzed using the Fourier Transform Infrared (FT-IR) method. Absorption appears at a wave number of 1637 cm-1 which indicates the presence of C=C, C=O bonds which are characteristic of Cdots. For AgNp, absorption appears at a wave number of 593.11 cm-1 which indicates the presence of Ag vibrations. Analysis with UV-Vis spectrophotometer gave the results at a wavelength of 431 nm absorbance AgNp-Cdots of 0.723 and a wavelength of 422 nm AgNp absorbance of 0.285. The results of the Particle Size Analyzer (PSA) analysis showed that AgNp-Cdots had an average size of 38.7 nm with a PI of 0.499 and pure AgNp of 51.8 nm with a PI of 0.566. Antibacterial activity of AgNp-Cdots against E. coli bacteria showed an inhibition zone of 2 mm while AgNp showed an inhibition zone of 5 mm.
银纳米颗粒(AgNp)已得到广泛的开发,其中之一是抗菌药物。AgNp抑制细菌的能力是毋庸置疑的。这些性质和特征可以通过添加缺陷来进一步研究。使用的缺陷是来自橘子的Cdots。Cdots是一种由天然材料合成的新型材料,具有独特的性能。以柠檬酸钠为还原剂,化学还原法合成AgNp,水热法合成Cdots。利用傅里叶变换红外(FT-IR)方法对合成结果进行了分析。吸收出现在波数为1637 cm-1的地方,这表明存在C=C, C=O键,这是Cdots的特征。对于AgNp,吸收波数为593.11 cm-1,表明存在Ag振动。紫外可见分光光度计分析结果表明,在431 nm波长处AgNp- cdots的吸光度为0.723,在422 nm波长处AgNp的吸光度为0.285。PSA分析结果表明,AgNp- cdots的平均粒径为38.7 nm, PI为0.499;纯AgNp的粒径为51.8 nm, PI为0.566。AgNp- cdots对大肠杆菌的抑菌活性为2 mm, AgNp的抑菌活性为5 mm。
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引用次数: 0
Synthesis of Chitosan/Activated Carbon Composite Beads as an Adsorbent of Pb(II) and Cu(II) ions in Aqueous Solution: A Review 壳聚糖/活性炭复合微球在水溶液中吸附铅(II)和铜(II)离子的研究进展
Pub Date : 2022-08-01 DOI: 10.15294/ijcs.v11i2.54943
Indah Larasati Dwi Wijayanti, F. W. Mahatmanti
Water is the most important substance for the life of living things. The development of various industries causes water pollution by metal ions. Adsorption is a way to remove metal ions in water. The adsorbents commonly used for adsorption are chitosan and activated carbon. Chitosan has weaknesses such as being easily soluble in acid, low selectivity, and less strong mechanical strength. One way to improve the properties of chitosan is to modify it with activated carbon. In this study, a literature review was conducted on the manufacture of chitosan/activated carbon composite beads for Pb(II) and Cu(II) ions adsorbents. Reference sources articles obtained from the Google Scholar database were selected using exclusion and inclusion criteria. The results obtained from the literature review show that chitosan/activated carbon can be made by dissolving chitosan in a CH3COOH solution, adding with activated carbon to form a mixture and the mixture is formed into beads by dripping it into a NaOH solution. The adsorption process of chitosan/activated carbon is influenced by pH, contact time, and solution concentration. The reaction mechanism that occurs is thought to be through electrostatic bonds, the formation of complex compounds, and the pores of the adsorbent. Chitosan/activated carbon adsorbent is an adsorbent that can be regenerated and reused for adsorption 5 times.
水是生物生命最重要的物质。各种工业的发展造成了金属离子对水体的污染。吸附是一种去除水中金属离子的方法。常用的吸附剂有壳聚糖和活性炭。壳聚糖具有易溶于酸、选择性低、机械强度不强等缺点。改善壳聚糖性能的一种方法是用活性炭对其进行改性。本文综述了壳聚糖/活性炭复合微球对Pb(II)和Cu(II)离子吸附剂的制备。根据排除标准和纳入标准选择从Google Scholar数据库中获得的参考文献。文献综述的结果表明,壳聚糖/活性炭的制备方法是将壳聚糖溶解在CH3COOH溶液中,加入活性炭形成混合物,将混合物滴入NaOH溶液中形成小球。壳聚糖/活性炭的吸附过程受pH、接触时间和溶液浓度的影响。发生的反应机理被认为是通过静电键、复杂化合物的形成和吸附剂的孔隙。壳聚糖/活性炭吸附剂是一种可再生、可重复使用吸附5次的吸附剂。
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引用次数: 0
Effect of Mannitol Concentration on The Stability of Encapsulated Yeast Black Rice Extract 甘露醇浓度对酵母黑米浸膏包封稳定性的影响
Pub Date : 2022-08-01 DOI: 10.15294/ijcs.v11i2.55200
Fikaliah Kusnandar Ririn Uli Riwu, R. Agustini
The encapsulation process of black rice yeast extract with mannitol was able to minimize the occurrence of protein aggregation and degradation processes due to encapsulated preparations that had low bioavailability. This study aims to determine the effect of mannitol concentration on the stability of encapsulated black rice yeast extract using sonication techniques and a poloxamer support matrix. The addition of mannitol used concentration variations (0 ppm, 25 ppm, 50 ppm, 75 ppm dan 100 ppm). The stability of the encapsulated results was measured using a TDS (Total Dissolve Solid) meter to see the level of turbidity and characterized using infrared spectroscopy (FTIR) to see the shift in the spectra of the functional groups. The results showed that the encapsulation of formula 3 has the best stability because it has a small TDS value for a period of 7 with a turbidity of 16 ppm and the resulting color display looks clearer. Based on the results of the study, it was found that the addition of mannitol concentration affected the turbidity value without chemical interactions that damaged the active compounds in the encapsulation.
黑米酵母浸膏与甘露醇包封工艺可以最大限度地减少由于包封制剂的生物利用度低而导致的蛋白质聚集和降解过程的发生。本研究旨在利用超声技术和波洛沙姆支撑基质研究甘露醇浓度对黑米酵母浸膏包封稳定性的影响。甘露醇的添加使用浓度变化(0 ppm, 25 ppm, 50 ppm, 75 ppm和100 ppm)。用TDS(总溶解固体)仪测量包封结果的稳定性,观察浊度水平,并用红外光谱(FTIR)观察官能团光谱的移位。结果表明,配方3的包封稳定性最好,因为其TDS值在7周期内很小,浊度为16 ppm,并且得到的颜色显示更清晰。根据研究结果发现,甘露醇浓度的加入对浊度值有影响,但没有破坏包封物中活性化合物的化学相互作用。
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引用次数: 0
Determination of Total Phenolic, Total Flavonoid, and Antioxidant Activity of India Onion Extract 印度洋葱提取物中总酚、总黄酮及抗氧化活性的测定
Pub Date : 2022-08-01 DOI: 10.15294/ijcs.v11i2.54610
Laila Ayuni Hidayah, M. A. Anggarani
Degenerative diseases can be triggered by free radicals. The disease can be inhibited by antioxidant compounds that can neutralize and destroy free radicals. The content of antioxidant compounds can be found in the genus Allium, one of which is the Indian red onion. Knowing the antioxidant activity, total phenolics, and total flavonoids of Indian shallot extract was the aim of this study. The extraction process was carried out from three solvents, namely dichloromethane, ethyl acetate, and 96% ethanol, using the multilevel maceration method with different levels of polarity. The samples tested included testing antioxidant activity using the DPPH method, total phenolics using the Folin Ciocalteu method, and total flavonoids using the aluminum chloride calorimetric method. The results showed that there were no phenolic and flavonoid compounds that had the potential as antioxidants in the dichloromethane and ethyl acetate extracts. Total phenolics, total flavonoids, and IC50 values ​​in the ethanol extract were 2,381 mg GAE/g extract, respectively; 0.330 mg QE/g extract, and 297.8689 ppm. The IC50 value obtained is classified as a weak antioxidant.
自由基可以引发退行性疾病。抗氧化化合物可以中和和破坏自由基,从而抑制这种疾病。抗氧化化合物的含量可以在葱属植物中找到,其中之一是印度红洋葱。了解印度葱提取物的抗氧化活性、总酚类物质和总黄酮的含量。以二氯甲烷、乙酸乙酯和96%乙醇为溶剂,采用不同极性的多级浸渍法进行提取。采用DPPH法测定样品的抗氧化活性,采用Folin Ciocalteu法测定样品的总酚类,采用氯化铝量热法测定样品的总黄酮。结果表明,二氯甲烷和乙酸乙酯提取物中不含具有抗氧化潜力的酚类和类黄酮类化合物。乙醇提取物的总酚、总黄酮和IC50值分别为2381 mg GAE/g提取物;0.330 mg QE/g提取物,297.8689 ppm。所得IC50值被归类为弱抗氧化剂。
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引用次数: 2
The The Effect of MRD (Milk of Red Rice and Dates) Composition on the Degradation Stability of Milk Dyes and The Content of Milk Microbial Contamination 红米枣乳组成对乳染料降解稳定性及乳微生物污染含量的影响
Pub Date : 2022-08-01 DOI: 10.15294/ijcs.v11i2.56016
R. N. Latifah
Milk is a nutritious drink that contains nutrients and vitamins needed by the body. In this study, a variant of the composition of red rice with Sukari dates and tested to obtain the best level of milk stability in the form of MRD. The composition of MRD was varied, namely MRD type I and MRD type II. The method used in this research is the analysis of milk dye degradation, milk stability analysis, microbial contamination analysis, and organoleptic testing. The results of the research on the degradation of milk dyes showed that both types of milk were in 2nd order with the reaction rate constant for type I MRD being 0.0582 and MRD type II was 0.0181. The level of stability of milk from MRD type I is 2nd order with a rate constant of 0.0953 and MRD type II is 1st order with a rate constant of 0.0998. For the microbial contamination assay showed that the microbial contamination test, showed that the two types of MRD, namely MRD type I and MRD type II were still within the safe limits and did not exceed the safe limits required by the SNI 7388:2009. The results of the hedonic test showed that the MRD type II was more favored by the respondents than the MRD type I.
牛奶是一种营养饮料,含有人体所需的营养和维生素。在这项研究中,用苏卡里枣组成的红米的一种变体进行了测试,以获得MRD形式的最佳乳稳定性。MRD的组成多种多样,分为MRD I型和MRD II型。本研究采用的方法是牛奶染料降解分析、牛奶稳定性分析、微生物污染分析和感官检测。对乳染料降解的研究结果表明,两种乳染料均为二级降解,ⅰ型MRD的反应速率常数为0.0582,ⅱ型MRD的反应速率常数为0.0181。MRD I型为二级,速率常数为0.0953;MRD II型为一级,速率常数为0.0998。对于微生物污染检测显示,微生物污染检测显示,MRD I型和MRD II型两种类型的MRD仍在安全范围内,未超过SNI 7388:2009要求的安全范围。享乐性测试结果显示,被调查者对II型MRD的偏好程度高于I型MRD。
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引用次数: 0
Toothpaste Gel Preparation from Composite of Hydroxyapatite-Chitosan-Green Betel Leaf (Piper Batle L.) Extract 羟基磷灰石-壳聚糖-槟榔叶复合材料制备牙膏凝胶提取
Pub Date : 2022-08-01 DOI: 10.15294/ijcs.v11i2.54583
Yossy Nur Annisa, S. E. Cahyaningrum
The use of toothpaste aims to reduce plaque and remineralize tooth enamel as a result of the reduction caused by the activity of oral bacteria. Toothpaste is generally added with antibiotics to treat bacterial caries, but the addition of calcium remineralization compounds to teeth is rarely found so the development of toothpaste with three ingredients, namely hydroxyapatite as an ingredient for remineralization, chitosan, and green betel leaf extract as an antibiotic. The purpose of this study was to manufacture a toothpaste gel formula from the hydroxyapatite-chitosan-green betel leaf extract composite and to determine the physical and chemical properties of each formula. This research is a laboratory experimental research. The results of the organoleptic test showed that the variation of green betel leaf extract affected the color, texture, and aroma of each formula. The homogeneity test showed the homogeneity of the third formula. The third formula has good dispersion between 5-7 cm and good adhesion, which is more than 1 second. The pH test shows that the results of formula one (F1) and formula two (F2) meet the pH range according to SNI (12-3524- 1995) which is 4.5-10 while formula three (F3) is far below it.
使用牙膏的目的是减少牙菌斑,并使牙釉质再矿化,因为口腔细菌的活动导致牙釉质减少。牙膏中一般会添加抗生素来治疗细菌性龋齿,但在牙齿中添加钙再矿化化合物的情况很少,因此开发了三种成分的牙膏,即羟基磷灰石作为再矿化成分,壳聚糖和槟榔叶提取物作为抗生素。本研究以羟基磷灰石-壳聚糖-槟榔叶提取物为原料制备牙膏凝胶配方,并测定各配方的理化性质。本研究是一项实验室实验研究。感官试验结果表明,槟榔叶提取物的变化对各配方的颜色、质地和香气均有影响。同质性检验表明第三公式具有同质性。第三种配方在5- 7cm之间分散性好,附着力好,1秒以上。pH试验表明,公式1 (F1)和公式2 (F2)的结果满足SNI(12-3524- 1995)的pH范围4.5-10,而公式3 (F3)则远远低于此范围。
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引用次数: 0
A Review: Nanoparticles NiFe2O4 Synthesis and Its Application as Hyperthermia Agents in Biomedicine 纳米NiFe2O4的合成及其在生物医学热疗中的应用
Pub Date : 2022-08-01 DOI: 10.15294/ijcs.v11i2.52590
Novi Nurjanah, Qurratu Aini Alya Adzkia, Riki Rustana, Selvi Citra Carolline, Shabrina Maulida Agustine, A. Nandiyanto
  Nickel ferrite (NiFe2O4) is one of the spinel ferrite nanoparticles that is useful for scientific and technological, like biomedicine. This paper discusses the synthesis of NiFe2O4 nanoparticles by various methods. This paper aims to find out the most efficient method for the synthesis of NiFe2O4 nanoparticles which are used as hyperthermia agents in biomedicine. The method used is a literature study of an article with publications from 1956-2018 by discussing several methods of NiFe2O4 syntheses, such as sol-gel, hydrothermal, co-precipitation, and combustion. From these methods, it was found that co-precipitation is the most efficient method among the other methods because it produces a relatively small NiFe2O4 nanoparticle size, which is 28 nm, causing these small particles to tend to be superparamagnetic and is good to be used as hyperthermia agent in biomedicine. This study is expected to be used as a reference to determine the method for synthesizing NiFe2O4 nanoparticles.
镍铁氧体(NiFe2O4)是尖晶石铁氧体纳米粒子之一,在生物医学等科学技术领域具有广泛的应用价值。本文讨论了不同方法合成纳米NiFe2O4的方法。本文旨在寻找合成纳米二氧化钛纳米粒子的最有效方法,并将其作为生物医学中的热疗剂。该方法是对1956-2018年发表的一篇文章进行文献研究,讨论了溶胶-凝胶法、水热法、共沉淀法和燃烧法等几种合成NiFe2O4的方法。从这些方法中发现,共沉淀法是其他方法中效率最高的方法,因为它产生的NiFe2O4纳米颗粒尺寸相对较小,为28 nm,使这些小颗粒倾向于超顺磁性,很适合用作生物医学中的热疗剂。本研究有望为确定纳米NiFe2O4的合成方法提供参考。
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引用次数: 1
期刊
Indonesian Journal of Chemical Science
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