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Zinc‐mediated efficient and environmentally benign synthesis of salicylate esters 锌介导的高效、无害环境的水杨酸酯合成技术
IF 2.6 3区 农林科学 Q3 CHEMISTRY, APPLIED Pub Date : 2024-06-28 DOI: 10.1002/ffj.3800
Harun Taşdemir, Semih Traş, Yesim Çat, Sonay Gürer, Akın Sağırlı
Considerable synthetic effort has been devoted to acid‐ or base‐catalysed transesterification of alkyl salicylate with alcohol in order to synthesize salicylate esters efficiently. In this study, the transesterification of methyl salicylate with 12 different alcohols was carried out by the use of Zn dust as a catalyst. Depending on the alcohol used in the transesterification reaction, the completion of the reaction was within a range of 8–15 h at a temperature between 100 and 170°C. The use of Zn dust provided reusability and almost complete recovery with moderate to excellent yields (42%–97%). The structural elucidation of the products was performed using IR, 1H NMR, 13C NMR and GC–MS data obtained from the Wiley GC/MS Library and the in‐house “Parkim Fragrance House GC/MS Library.”
为了有效合成水杨酸酯,人们在酸或碱催化水杨酸烷基酯与醇的酯交换反应方面投入了大量的精力。本研究以 Zn 粉尘为催化剂,进行了水杨酸甲酯与 12 种不同醇类的酯交换反应。根据酯交换反应中使用的不同醇类,反应在 100 至 170 摄氏度的温度下完成的时间范围为 8 至 15 小时。锌粉的使用提供了可重复使用性和几乎完全的回收率,以及中等到极好的产率(42%-97%)。利用从 Wiley GC/MS 库和内部 "Parkim Fragrance House GC/MS 库 "获得的红外光谱、1H NMR、13C NMR 和 GC-MS 数据,对产品进行了结构阐释。
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引用次数: 0
Identification and variation of specific volatile compounds during fruit development and postharvest stage in Japanese apricot (Prunus mume Sieb. et Zucc.) fruit 日本杏(Prunus mume Sieb. et Zucc.)
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-06-12 DOI: 10.1002/ffj.3797
Aoting Li, Kang Liu, Silas Segbo, Zhihong Gao
Fruit aroma of Japanese apricot is distinct, and the specific volatile compounds are not clearly known during fruit development and during post‐harvest stage. This study therefore aimed to explore the volatile compounds present during these stages. The volatile compounds were analysed by headspace solid‐phase microextraction and gas chromatography–mass spectrometry. OAV, PCA and electronic nose techniques were used to determine the characteristic aroma components. Enzyme‐linked immunoassay (ELISA) was also applied to determine the activity of enzymes. The results showed that in the cultivars ‘Xiyeqing’ a total of 52 components that included 20 terpenes, 15 aldehydes, 9 esters, 3 ketones and 5 other substances were detected during fruit development and post‐harvest stage. While in the cultivar ‘Xiaoyezhugan’ a total of 49 components that included 25 terpenes, 7 aldehydes, 11 esters, 1 alcohol, 3 ketones and 2 other substances were also detected during fruit development and post‐harvest stage. We concluded that the characteristic volatile compounds of mature Japanese apricot fruit were (+)‐limonene, linalool, damascenone, β‐damascenone and nonanal, finding the basis for the fruity, floral and sweet aroma of the Japanese apricot fruit. Further analysis indicated that low temperature inhibited the synthesis of esters and terpenes, and dark conditions were more favourable to the synthesis of volatile compounds than light conditions. Short‐term storage of Japanese apricot fruit at room temperature and dark conditions was conducive for the maintenance of volatile compounds, and low‐temperature storage was the most destructive to the fruit volatile compounds. These findings form a theoretical foundation for exploring the specific volatile compound of Japanese apricot and helped to determine the optimal storage condition of post‐harvest stage for Japanese apricot fruit.
日本杏的果实香气独特,在果实发育和采后阶段的特定挥发性化合物尚不清楚。因此,本研究旨在探索这些阶段的挥发性化合物。研究采用顶空固相微萃取和气相色谱-质谱法对挥发性化合物进行了分析。采用 OAV、PCA 和电子鼻技术确定了特征香气成分。酶联免疫吸附法(ELISA)也用于测定酶的活性。结果表明,"西叶青 "品种在果实发育和采后阶段共检测到 52 种成分,包括 20 种萜烯、15 种醛、9 种酯、3 种酮和 5 种其他物质。而在栽培品种 "Xiaoyezhugan "中,在果实发育和采后阶段也检测到了总共 49 种成分,包括 25 种萜烯、7 种醛、11 种酯、1 种醇、3 种酮和 2 种其他物质。我们得出结论,成熟日本杏果实的特征挥发性化合物为 (+)- 柠檬烯、芳樟醇、大马士革酮、β-大马士革酮和壬醛,这为日本杏果实的果香、花香和甜香奠定了基础。进一步的分析表明,低温抑制了酯类和萜烯类化合物的合成,黑暗条件比光照条件更有利于挥发性化合物的合成。日本杏果实在室温和黑暗条件下的短期贮藏有利于挥发性化合物的保持,而低温贮藏对果实挥发性化合物的破坏性最大。这些发现为探索日本杏的特定挥发性化合物奠定了理论基础,并有助于确定日本杏果实采后阶段的最佳贮藏条件。
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引用次数: 0
Identification of characteristic volatiles of Zhenjiang aromatic vinegar using HS‐SPME‐GC/MS coupled with multivariate analysis 利用 HS-SPME-GC/MS 结合多元分析鉴定镇江香醋的特征挥发物
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-06-07 DOI: 10.1002/ffj.3796
Zhihua Li, Wenbing Fang, Siwen Wang, Jiyong Shi, Xiaobo Zou, Xiaowei Huang
This study employed headspace solid phase micro‐extraction gas chromatography mass spectrometry (HS‐SPME‐GC–MS) coupled with multivariate statistical analysis to identify volatile markers in various levels of Zhenjiang Aromatic Vinegar (ZAV). A full range of 40 volatile organic compounds (VOCs) were identified and categorized into acids, alcohols, esters, aldehydes, ketones, heterocyclic compounds and others. Principal component analysis (PCA) and hierarchical cluster analysis (HCA) demonstrated a clear clustering effect among different levels of ZAV, indicating distinct volatile characteristics at the relative content level. Furthermore, using Orthogonal partial least squares discrimination analysis (OPLS‐DA), 20 significant volatile organic compounds (VOCs) were identified as markers for distinguishing between the various levels of ZAV. To differentiate among the levels of ZAV, two volatile compounds, acetic acid and n‐hexanol, were identified as characteristic volatile compounds using a combination of Venn diagram, analysis of variance (ANOVA) and boxplot analysis. The results showed notable variations in VOCs among ZAV samples of different grades. Acetic acid and n‐hexanol can serve as reliable markers for grade distinction, providing valuable technical and theoretical support for the production and quality control of ZAV.
本研究采用顶空固相微萃取气相色谱质谱法(HS-SPME-GC-MS),结合多元统计分析,对镇江香醋(ZAV)中不同含量的挥发性标记物进行了鉴定。共鉴定出 40 种挥发性有机化合物(VOC),并将其分为酸类、醇类、酯类、醛类、酮类、杂环化合物等。主成分分析(PCA)和层次聚类分析(HCA)显示,不同级别的 ZAV 之间存在明显的聚类效应,表明在相对含量水平上存在不同的挥发性特征。此外,利用正交偏最小二乘判别分析(OPLS-DA),确定了 20 种重要的挥发性有机化合物(VOC),作为区分不同水平 ZAV 的标记。为了区分不同水平的 ZAV,结合使用 Venn 图、方差分析 (ANOVA) 和方框图分析,确定了醋酸和正己醇这两种挥发性化合物为特征挥发性化合物。结果表明,不同等级的 ZAV 样品在挥发性有机化合物方面存在显著差异。乙酸和正己醇可作为区分等级的可靠标记,为 ZAV 的生产和质量控制提供了宝贵的技术和理论支持。
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引用次数: 0
The effect of different hydrodistillation times on the composition and yield of bergamot (Citrus bergamia Risso) peel essential oil and a comparison of the cold‐pressing method 不同水蒸馏时间对佛手柑(Citrus bergamia Risso)果皮精油成分和产量的影响以及冷压法的比较
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-05-28 DOI: 10.1002/ffj.3789
Burcu Bozova, Muharrem Gölükcü, Angelo Maria Giuffrè
Bergamot (Citrus bergamia Risso) is not consumed as fresh fruit as other members of Citrus. Bergamot essential oil has a unique aroma. Bergamot essential oil is a very valuable product used in perfumery, cosmetics, aromatherapy and food industry due to its beautiful scent and functional properties. As with other Citrus species, the composition of bergamot essential oil can vary according to harvest time, climate and extraction technology. Bergamot essential oil could be obtained by cold press extraction or distillation method. Within the scope of the study, the effect of four different hydrodistillation (HD) times (5, 10, 60 and 120 min) on the composition of bergamot essential oil obtained from Turkish fruits was investigated. In the first 60 min, 96.11% of the total essential oil was obtained. Research findings have shown that the distillation time is quite effective in the composition of bergamot essential oil. Limonene, linalool and linalyl acetate, which are the main components of bergamot essential oil, varied in the range, 42.36%–53.25%, 5.59%–12.18% and 20.84%–26.73%, respectively, with respect to distillation time. In cold press method, bergamot essential oil has lower linalool/linalyl acetate ratio (0.15) compared to HD method and a higher quality essence was obtained.
佛手柑(Citrus bergamia Risso)不像其他柑橘类水果那样作为新鲜水果食用。佛手柑精油具有独特的香气。佛手柑精油因其美丽的香味和功能特性,成为香水、化妆品、芳香疗法和食品工业中非常珍贵的产品。与其他柑橘类植物一样,佛手柑精油的成分也会因收获时间、气候和萃取技术的不同而有所变化。佛手柑精油可以通过冷压萃取法或蒸馏法获得。本研究调查了四种不同的水蒸馏(HD)时间(5、10、60 和 120 分钟)对从土耳其水果中提取的佛手柑精油成分的影响。在第一个 60 分钟中,获得了总精油的 96.11%。研究结果表明,蒸馏时间对佛手柑精油成分的影响相当有效。佛手柑精油的主要成分柠檬烯、芳樟醇和乙酸芳樟酯随蒸馏时间的变化范围分别为 42.36%-53.25%、5.59%-12.18% 和 20.84%-26.73%。冷压法与 HD 法相比,佛手柑精油的芳樟醇/乙酸芳樟酯比率(0.15)更低,获得的精油质量更高。
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引用次数: 0
Refinement of flavour substance intake estimates using probability of addition: A proposed method based on sales data 利用添加概率完善香料摄入量估算:基于销售数据的拟议方法
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-05-02 DOI: 10.1002/ffj.3785
Giulia Vilone, Christina Hickey, Natalie Slickers, John O'Brien, Benjamin Smith

Most dietary intake estimates used in the regulatory risk assessment of flavouring substances assume that the flavouring substance is present in all foods at a given concentration. They do not account for the use of alternate flavouring substances for the same taste modality, nor do they consider the use of differing concentrations within a particular food category. This highly conservative assumption leads to an over-estimation of exposure. To refine this assumption in exposure models, the probability of addition can be utilised. In this study, a methodology to estimate the probability of addition was developed, using the volume of a flavouring substance sold for flavours created for a particular food category against its total volume sold for all flavouring use. The method was trialled, as a proof of principle, using historical data sets of two test flavouring substances, benzaldehyde (a large volume/use material) and bornyl acetate (a low volume/use material), and the impact on dietary exposure assessment was assessed. The resulting exposure estimates for both flavouring substances were shown to be significantly lower than those without the incorporation of probability of addition, demonstrating that current methods are overly conservative and that the use of probability of addition provides a more realistic estimate of exposure of flavouring substances present in foods.

大多数用于香料物质监管风险评估的膳食摄入量估计值都假定香料物质以特定浓度存在于所有食品中。它们没有考虑到同一口味模式中使用其他调味物质的情况,也没有考虑到某一特定食品类别中使用不同浓度调味物质的情况。这种高度保守的假设会导致过高估计暴露量。为了完善暴露模型中的这一假设,可以利用添加概率。本研究开发了一种估算添加概率的方法,使用为特定食品类别制作的香料的香料物质销售量与所有香料用途的总销售量进行对比。作为原理验证,利用苯甲醛(一种大容量/使用量物质)和乙酸硼酯(一种低容量/使用量物质)这两种测试香料物质的历史数据集试用了该方法,并评估了该方法对膳食暴露评估的影响。结果表明,这两种香料物质的暴露量估计值大大低于未纳入添加概率的估计值,这表明目前的方法过于保守,而使用添加概率可对食品中香料物质的暴露量进行更切合实际的估计。
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引用次数: 0
Chemical composition and discrimination with volatile profiles of Yongchuan Xiuya green tea with different baking treatments 不同烘焙处理下永川秀芽绿茶的化学成分及挥发性特征鉴别
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-04-29 DOI: 10.1002/ffj.3783
Hongyu Luo, Yi Wang, Rui Chang, Shanmin Chen, Tinghua Wang, Quan Wu, Yingfu Zhong

This study aimed to explore the effects of different baking treatments on the quality of Yongchuan Xiuya (YCXY) green tea. It was found that a long time baking at low temperature was beneficial to keep green colour, faint scent, mellow and fresh taste quality, whereas baking under high temperature was adverse to the quality. Baking treatments slightly regulated (−)-epigallocatechin, (−)-epicatechin, (−)-gallocatechin gallate, total chlorophyll and carotenoid. As the baking temperature rose, the content of tea polyphenols, gallic acid, catechins, caffeine, soluble sugar and polyphenols/amino acids ratio obviously decreased. A total of 40 kinds of volatiles were detected in these six tea samples. A model for aroma type discrimination was successfully established based on partial least squares-discriminant analysis (PLS-DA). Ten kinds of volatile substances were the key characteristic markers for the faint scent, chestnut aroma and high-fired aroma types of YCXY green tea. 1-hexanol, hotrienol and dimethyl sulfide were furtherly used to discriminant aroma type based on Fisher discriminant analysis (FDA).

本研究旨在探讨不同烘焙处理对永川秀芽(YCXY)绿茶品质的影响。结果发现,长时间低温烘焙有利于保持茶叶色泽翠绿、香气淡雅、滋味醇和鲜爽的品质,而高温烘焙则对茶叶品质不利。烘焙处理对(-)-表没食子儿茶素、(-)-表儿茶素、(-)-没食子儿茶素没食子酸酯、总叶绿素和类胡萝卜素有轻微的调节作用。随着烘焙温度的升高,茶多酚、没食子酸、儿茶素、咖啡碱、可溶性糖含量和茶多酚/氨基酸比值明显下降。这六种茶叶样品中共检测到 40 种挥发性物质。基于偏最小二乘判别分析(PLS-DA),成功建立了香气类型判别模型。其中 10 种挥发性物质是 YCXY 绿茶淡香型、栗香型和高火型的主要特征标记。基于费雪判别分析(FDA),进一步利用 1-己醇、热三烯醇和二甲基硫醚来判别香气类型。
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引用次数: 0
Chemical constituents and bioactivities of the essential oils of Magnolia biondii flower buds from three provinces in China 中国三省厚朴花蕾精油的化学成分和生物活性
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-04-22 DOI: 10.1002/ffj.3787
Tian-Xiao Li, Li‐Peng Li, Da‐Yuan Zhang, Guo‐Liang Zhao, Yong‐Wei Liang, Xue‐Wei Jia, Lei Guo, Chun-Ping Xu, Xin Gao
Magnolia biondii flower buds are a well‐known medicinal plant in China, and it is important to determine the differences in aroma, flavour components, and biological activity of the essential oils of M. biondii flower buds (EOM) from different origins. In this study, the essential oils of M. biondii flower buds from Sichuan (EOM‐SC), Anhui (EOM‐AH) and Henan (EOM‐HN) provinces were extracted by hydrodistillation. The condition of the extraction process was optimized. The differences in the flavour compounds were further confirmed by GC–MS and relative odour activity value (ROAV) analyses. In addition, the antibacterial and antioxidant activity was also evaluated. The results showed that the optimized condition for steam distillation was water: flower powder ratio = 10:1 with extraction time for more than 3.0 h. Interestingly, special floral, fruity and freshness flavours were found for EOM‐SC, and the medicinal herb and sweetness odours of EOM‐HN were more prominent. The numbers and contents of flavour compounds in EOM‐SC and EOM‐HN were higher than those of EOM‐AH. Eucalyptol, β‐pinene, linalool, α‐terpineol and sabinene could be proposed as the key mutual flavour compounds for three essential oils. In addition, the strong floral, fruity and freshness aroma of EOM‐SC could be associated with the high ROAVs of α‐terpineol, linalool and sabinene. Moreover, EOM‐SC exhibited better antibacterial and antioxidant activity than those of the other two essential oils.
厚朴花蕾是中国著名的药用植物,确定不同产地厚朴花蕾精油(EOM)在香气、风味成分和生物活性方面的差异具有重要意义。本研究采用水蒸馏法萃取了四川(EOM-SC)、安徽(EOM-AH)和河南(EOM-HN)三省的藤黄科植物花蕾精油。对提取过程的条件进行了优化。通过气相色谱-质谱(GC-MS)和相对气味活性值(ROAV)分析,进一步证实了风味化合物的差异。此外,还对抗菌和抗氧化活性进行了评估。结果表明,蒸汽蒸馏的最佳条件是水:花粉的比例为 10:1,萃取时间超过 3.0 小时。有趣的是,EOM-SC 具有特殊的花香、果香和清新的味道,而 EOM-HN 的药草味和甜味则更为突出。EOM-SC和EOM-HN中风味化合物的数量和含量均高于EOM-AH。桉叶油醇、β-蒎烯、芳樟醇、α-松油醇和沙比利烯被认为是三种精油的主要互味化合物。此外,EOM-SC 强烈的花香、果香和清新香气可能与 α-松油醇、芳樟醇和沙比利烯的高 ROAV 值有关。此外,EOM-SC 的抗菌和抗氧化活性也优于其他两种精油。
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引用次数: 0
Isolation and identification of non-Saccharomyces yeasts and their flavour characteristics while brewing Yinhong plum wine 殷红梅酒酿造过程中非酵母菌的分离鉴定及其风味特征
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-04-17 DOI: 10.1002/ffj.3786
Yu Lei, Tian Li, Li Chen, Meng-Sheng Deng, Lei Jin, Yu-Hao Li, Dong Li

The objective of this study was to screen non-Saccharomyces yeast suitable for enhancing the aroma of Yinhong plum wine. Five non-Saccharomyces yeasts with strong ester-producing ability, namely, Wa3 (Wickerhamomyces anomalus), Hu12 (Hanseniaspora uvarum), Pk2A2, PkW2 and PkY2 (Pichia kluyveri), were selected from various naturally fermented fruit juices for molecular biological identification, analyses of physiological characteristics and tolerance and determination of their effects on the flavour of Yinhong plum wine. Analysis of brewing characteristics showed that they differed in their abilities of producing acetic acid, hydrogen sulfide, killer activity and tolerance. Among them, Wa3 showed the best tolerance to high concentrations of alcohol, sugar and SO2. Compared to the control Saccharomyces cerevisiae FX10, Yinhong plum wine fermented with non-Saccharomyces yeast exhibited a decrease in alcohol content, while residual sugar, glycerol content and the types and quantities of volatile compounds all showed an increase. Among the fermented wines, PkY2 generated the highest content of ester compounds in the fermented wine, which was 5.66 times higher than that generated by the control. The compounds produced by PkY2 were closely related to various ethyl and acetate odour-active compounds (odour-active value >1), which could impart a rich floral and fruity aroma to Yinhong plum wine. Sensory analysis revealed that both floral and fruity aromas were significantly increased in Yinhong plum wine fermented by non-Saccharomyces yeasts, with the highest scores of floral and fruity aromas for PkY2. In conclusion, a Pichia kluyveri strain, PkY2, with excellent brewing characteristics and potential for enhancing the aroma of Yinhong plum wine was identified.

本研究的目的是筛选适合提升殷红李子酒香味的非酵母菌。从多种天然发酵果汁中筛选出五种产酯能力强的非酿酒酵母,即 Wa3(Wickerhamomyces anomalus)、Hu12(Hanseniaspora uvarum)、Pk2A2、PkW2 和 PkY2(Pichia kluyveri),进行分子生物学鉴定、生理特性和耐受性分析,并测定其对殷红李子酒风味的影响。酿造特性分析表明,它们在产生醋酸、硫化氢、杀菌活性和耐受性方面存在差异。其中,Wa3 对高浓度酒精、糖和二氧化硫的耐受性最好。与对照的酿酒酵母 FX10 相比,用非酿酒酵母发酵的殷红李子酒的酒精含量有所下降,而残糖、甘油含量和挥发性化合物的种类和数量均有所增加。在发酵酒中,PkY2 产生的酯类化合物含量最高,是对照组的 5.66 倍。PkY2 产生的化合物与各种乙酸乙酯气味活性化合物(气味活性值为 1)密切相关,可为殷红李子酒带来浓郁的花香和果香。感官分析表明,用非酵母菌发酵的殷红李子酒的花香和果香都明显增加,其中 PkY2 的花香和果香得分最高。总之,研究发现了一种具有优良酿造特性和提高殷红李子酒香气潜力的 Pichia kluyveri 菌株 PkY2。
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引用次数: 0
Characterization of important odorants from Persian silk tree flowers, Albizia julibrissin 波斯绢树花(Albizia julibrissin)重要气味物质的特征描述
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-04-08 DOI: 10.1002/ffj.3779
Thien Nguyen, Melissa Dein, Danielle Trudelle, John P. Munafo Jr

The Persian silk tree (Albizia julibrissin) has delicate flowers with a pleasant aroma profile, displaying notes of hyacinth and rose with subtle nuances of citrus, coconut and spice. In this study, a total of 29 odorants were identified in the flowers from a single A. julibrissin selection by the application of a cold-solvent extraction (CSE), followed by solvent-assisted flavour evaporation (SAFE) and aroma extract dilution analysis (AEDA). Subsequently, nine odorants with flavour dilution (FD) factors ≥16 were quantitated by stable isotope dilution analysis (SIDA), and odour activity values (OAVs) were calculated. Odorants with OAV ≥1 included 2-phenylacetaldehyde (OAV 3638), linalool (OAV 797), eugenol (OAV 231), geraniol (OAV 161), 1H-indole (OAV 93), β-ionone (OAV 31), 2-phenylethanol (OAV 11) and γ-octalactone (OAV 1). An aroma simulation model was prepared based on the quantitation data, and it closely matched the aroma of the flower isolate. Chiral chromatography was performed, and (S)-(+)-linalool was the only enantiomer detected. This study advances our understanding of A. julibrissin flower aroma chemistry and lays the groundwork for future investigations for the development of delicate floral aromas for flavour and fragrance applications.

波斯绢花(Albizia julibrissin)的花朵细腻,香气宜人,有风信子和玫瑰的香味,还带有柑橘、椰子和香料的细微差别。在这项研究中,通过冷溶剂萃取(CSE)、溶剂辅助香气蒸发(SAFE)和香气提取物稀释分析(AEDA),从单个 A. julibrissin 选种的花朵中鉴定出了 29 种气味物质。随后,通过稳定同位素稀释分析法(SIDA)对风味稀释因子(FD)≥16 的九种气味物质进行定量,并计算出气味活性值(OAVs)。OAV ≥1的气味物质包括 2-苯乙醛(OAV 3638)、芳樟醇(OAV 797)、丁香酚(OAV 231)、香叶醇(OAV 161)、1H-吲哚(OAV 93)、β-酮(OAV 31)、2-苯乙醇(OAV 11)和γ-辛内酯(OAV 1)。根据定量数据建立了香气模拟模型,该模型与花卉分离物的香气十分吻合。进行了手性色谱分析,发现(S)-(+)-芳樟醇是唯一的对映体。这项研究加深了我们对 A. julibrissin 花芳香化学的了解,为今后开发用于香精香料的精致花香奠定了基础。
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引用次数: 0
Effect of Hemerocallis essence aroma on brain activity and sleep processes via scalp electroencephalogram 通过头皮脑电图观察 Hemerocallis 香精对大脑活动和睡眠过程的影响
IF 2.6 3区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-04-08 DOI: 10.1002/ffj.3782
Qinfei Ke, Jiaqi Yang, Jiancai Zhu, Qingran Meng, Yunchong Zhang, Yihao Guo, Yunwei Niu, Qinglei Liu, Xin Huang, Xingran Kou

Sleep disorders are widespread. Inhaled aromatherapy has shown advantages over medication in treating insomnia. Daylily (Hemerocallis fulva) has been found to positively affect sleep either by ingestion or inhalation, but there is a lack of research on the sleep aid effect of its inhalation route. At present, the floral scent characteristics of daylily are not obvious, and the extraction rate of essential oil is low. Based on the above problems, this study developed daylily essence which replicates the natural aroma of plants and investigated the effect of inhaling daylily essence aroma on sleep activity by using Pittsburgh Sleep Quality Index (PSQI) and electroencephalogram (EEG). According to PSQI results, inhaling the aroma of daylily essence improved participants' subjective sleep quality. The difference between men and women was statistically significant (p < .05). The slow-wave sleep activity of EEG in the experimental group was significantly stronger than that in the control group (p < .01). In addition, the frontal and central regions were more responsive to aroma stimuli (p < .05). The results of this study show that the aroma of daylily can promote the subjective and objective sleep quality of healthy college students, and the use of fragrance intervention is a potential scheme to improve sleep quality and insomnia.

睡眠障碍很普遍。在治疗失眠方面,吸入芳香疗法比药物疗法更具优势。研究发现,萱草(Hemerocallis fulva)通过摄入或吸入都能对睡眠产生积极影响,但对其吸入途径的助眠效果缺乏研究。目前,萱草的花香特征不明显,精油提取率低。基于上述问题,本研究开发了复制植物天然香气的萱草香精,并利用匹兹堡睡眠质量指数(PSQI)和脑电图(EEG)研究了吸入萱草香精香气对睡眠活动的影响。PSQI结果显示,吸入萱草香精能改善参与者的主观睡眠质量。男女之间的差异具有统计学意义(p < .05)。实验组的脑电图慢波睡眠活动明显强于对照组(p < .01)。此外,实验组的额叶和中枢区域对香气刺激的反应更强烈(p <.05)。本研究结果表明,萱草香气能促进健康大学生的主观和客观睡眠质量,使用香气干预是改善睡眠质量和失眠的潜在方案。
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引用次数: 0
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Flavour and Fragrance Journal
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