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Evaluation of Process Control During On-Line Consolidation of Thermoplastic Composites 热塑性复合材料在线固结过程控制评价
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0627
C. Pistor, M. Yardimci, Raoul Castro, S. Güçeri
Laser assisted tape winding is a manufacturing technique to produce thermoplastic composite parts of high quality. It is an additive semi-freeform fabrication process that utilizes thermoplastic composite prepreg tape as the base material. The tape is fused by the heat delivered from a laser beam, while it is wound onto a cylindrical mandrel. To ensure proper consolidation to the substrate, a roller applies the necessary compaction pressure. The fabrication of high quality rings with circular (Beyeler, 1988 and Irwin, 1994) and non-circular (Pistor et al. 1995) shape using quarter inch wide prepreg tape (PPS/Carbon, PEEK/Carbon) has been successfully demonstrated. The shape of the beam utilized in these investigations was determined by a series of lenses that formed the circular beam of the CO2 laser into a vertical narrow ellipse approximately 6.4 mm high and 2 mm wide (Pistor et al., 1995). The area illuminated by the infrared laser was therefore preset and not adjustable, limiting the set-up to the processing of quarter inch wide tape. One of the advantages of using a laser beam for the consolidation of thermoplastic resins is the that extremely high heat trnsfer rates to the resin are possible. This can be exploited not only for laser power adjustments in response to variations in tape laying velocity (Pistor et al., 1995), but also for scanning of a circular beam spot over the desired consolidation area. For the described set-up, a vertical slit of adjustable height was realized by scanning the laser beam vertically with a frequency of 100–500 Hz. Scanning height and frequency as well as motion and laser power are computer controllable.
激光辅助卷绕是一种生产高质量热塑性复合材料零件的制造技术。它是一种以热塑性复合预浸料带为基材的增材半自由成形制造工艺。当胶带缠绕在圆柱形芯轴上时,由激光束发出的热量将其熔化。为了确保基材的适当固结,辊子施加必要的压实压力。使用四分之一英寸宽的预浸料带(PPS/Carbon, PEEK/Carbon)制造高质量的圆形(Beyeler, 1988年和Irwin, 1994年)和非圆形(Pistor等人,1995年)形状的环已被成功证明。这些研究中使用的光束形状是由一系列透镜决定的,这些透镜将CO2激光器的圆形光束形成一个垂直的窄椭圆,高约6.4 mm,宽约2mm (Pistor et al., 1995)。因此,红外激光照射的区域是预设的,不可调节的,限制了设置,以处理四分之一英寸宽的磁带。使用激光束固化热塑性树脂的优点之一是,极高的热传递率树脂是可能的。这不仅可以用于激光功率调整以响应胶带铺设速度的变化(Pistor等人,1995年),还可以用于扫描所需固化区域上的圆形光束点。对于所描述的设置,通过以100-500 Hz的频率垂直扫描激光束来实现高度可调的垂直狭缝。扫描高度、频率、运动和激光功率均由计算机控制。
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引用次数: 1
Rotational Molding of Low-Density LLDPE Foams 低密度LLDPE泡沫塑料的旋转成型
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0618
Guobin Liu, Chul B. Park, J. Lefas
This paper presents plastic foam processing for the manufacture of LLDPE foams in rotomolding. In order to better understand the mechanisms of foaming, a fundamental study on the foaming process in rotomolding has been conducted. First, the decomposition behavior of the chemical blowing agents was studied by a thermogravimetric analyzer (TGA). The rheological properties of zero-shear viscosity and melt elasticity for LLDPEs were measured using a rotational stress rheometer. Also, an optical microscope with a hot stage was effectively used to study the cell nucleation, growth, coalescence and coarsening in LLDPE melts which provide an improved understanding of the foaming dynamics with a chemical blowing agent in rotational molding. Finally, the actual foaming behavior in rotomolding has also been studied. The experimental results indicate that the amount of blowing agent, the heating time, and the processing temperature play an important role in determining the cell morphology in rotational foam molding.
介绍了用滚塑法制造LLDPE泡沫塑料的发泡工艺。为了更好地了解发泡机理,对滚塑发泡过程进行了基础研究。首先,用热重分析仪(TGA)研究了化学发泡剂的分解行为。用旋转应力流变仪测量了lldpe的零剪切粘度和熔体弹性的流变特性。同时,利用热台光学显微镜对LLDPE熔体的成核、生长、聚结和粗化过程进行了有效的研究,为进一步了解化学发泡剂在旋转成型过程中的发泡动力学提供了依据。最后,对滚塑过程中的实际发泡行为进行了研究。实验结果表明,发泡剂的用量、加热时间和加工温度对旋转发泡成型中孔的形态有重要影响。
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引用次数: 3
Intelligent Processing of Carbon-Black Loaded Plastics 炭黑负载塑料的智能加工
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0635
V. Bouda
The electrical conductivity of alternating current (AC) and permittivity of carbon-black (CB)-filled low density polyethylene (LDPE) has been measured as function of time at a temperature higher than the melting temperature of matrix polymer. The conductivities measured at lower frequencies (If) can be used for the characterization of the properties of the interlayer between the CB-particles. The conductivities measured at higher frequencies (hf) reflects the properties of the internal structure of the individual CB-aggregate. At a characteristic time t°, the lf AC conductivity suddenly increased up to the hf conductivity and the permittivity suddenly decreased. The CB aggregates are probably linked together by paracrystalline layers after a certain time of annealing. The time t° increases with the weight percent of CB. It was also found that t° increases as the temperature of annealing decreases. The time t° is interpreted as a relaxation of potential energy of electrostatic repulsion forces between the reversible disintegrated CB particles. The poor reproducibility and stability of CB-filled plastics can be explained by the observed changes of conductivity.
在高于基体聚合物熔化温度的温度下,测定了炭黑填充低密度聚乙烯(LDPE)的交流电电导率和介电常数随时间的变化。在较低频率(If)下测量的电导率可用于表征cb粒子之间的中间层的性质。在高频(hf)下测量的电导率反映了单个cb -聚集体内部结构的性质。在特征时间t°时,低频交流电导率突然增大到高频电导率,而介电常数突然减小。经过一定时间的退火后,炭黑聚集体可能通过准晶层连接在一起。时间t°随炭黑质量百分比的增加而增加。t°随退火温度的降低而增大。时间t°被解释为可逆分解的CB粒子间静电斥力势能的松弛。cb填充塑料的重现性和稳定性较差,可以用观察到的电导率变化来解释。
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引用次数: 1
Orientation Formation in Planar Mold Filling: Theory and Numerical Predictions 平面充型中的取向形成:理论与数值预测
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0637
Jufang He, K. Olivero, M. Altan
Orientation formation in a steady, Newtonian, Hele-Shaw flow containing rigid, neutrally buoyant, slender fibers is numerically analyzed. The Hele-Shaw model is used to simulate flows through mold cavities consisting of thin planar sections. In this study, orientation results are calculated for a mold cavity containing a three to one sudden contraction. The suspension is injected from a single inlet gate at constant volume flow rate. Initially, the planar stream function is numerically solved by an Eulerian finite difference method to obtain the flow field. Subsequently, a Lagrangian particle tracking method is used to calculate the orientation field from the flow kinematics. The three-dimensional orientation formation throughout the mold cavity is obtained by a new method which calculates the second-order orientation tensors directly from flow kinematics and particle aspect ratio. With this new method, time-consuming integrals and inaccurate closure approximations commonly used in orientation calculations are avoided. The rotational dynamics of each particle are described by Jeffery’s theory. The numerical results are valid for multi-particle, dilute suspensions in which the orientation field can be fully described by the second-order moment of the orientation probability density function (OPDF). The orientation results are presented at different layers through the thickness of the mold cavity, ranging from the midplane to the top wall. In addition, the second-order orientation tensor is averaged through the mold thickness at a number of points in the vicinity of sudden contraction. These averaged orientation tensors are compared with the experimental data obtained from the same flow configuration by Olivero et al. (1997).
在稳定的、牛顿的、Hele-Shaw流动中,包含刚性的、中性浮力的、细长的纤维,对取向形成进行了数值分析。Hele-Shaw模型用于模拟由薄平面截面组成的模腔内的流动。在本研究中,取向结果计算了模具型腔包含三比一突然收缩。悬浮液以恒定体积流量从单个入口闸门注入。首先采用欧拉有限差分法对平面流函数进行数值求解,得到流场。在此基础上,利用拉格朗日粒子跟踪法,从流体运动学出发,计算了流体的方向场。通过直接从流动运动学和颗粒长径比计算二阶取向张量的新方法,得到了整个模腔的三维取向形成。该方法避免了方向计算中常用的耗时积分和不准确的闭包近似。每个粒子的旋转动力学用杰弗里理论来描述。数值结果适用于多粒子稀悬液,其中取向场可以用取向概率密度函数(OPDF)的二阶矩完全描述。定向结果通过模腔的厚度呈现在不同的层上,从中间平面到顶壁。此外,二阶方向张量通过在突然收缩附近的一些点的模具厚度平均。将这些平均方向张量与Olivero等人(1997)从相同流动配置中获得的实验数据进行比较。
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引用次数: 1
Calculation and Optimisation of the Feeding System in Thermoplastics Injection 热塑性塑料注射喂料系统的计算与优化
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0644
N. Van Rutten, F. Dupret
During the filling stage of injection molding, important thermal phenomena take place in the mold feeding system. We present a non-isothermal model for the flow through the runners and the gates that permits us to accurately simulate the filling of thermoplastics parts. Comparison with experiments demonstrates the validity of our approach.
在注射成型的充型阶段,在送模系统中会发生重要的热现象。我们提出了通过流道和浇口流动的非等温模型,使我们能够准确地模拟热塑性塑料零件的填充。实验结果表明了该方法的有效性。
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引用次数: 0
A Novel Process Control for Injection Molding Based Upon On-Line CAE Systems 基于在线CAE系统的新型注射成型过程控制
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0634
Pei-Jen Wang, Jin-Yow Lin
A novel process control system for injection molding based on the integration of Computer Aided Engineering systems (CAE) and process control models has been studied and verified. The objective is to develop a scientific approach for on-line process control by making use of the results from the CAE systems. Initially, the design of injection molded products should be finished with the help of the CAE systems after the dimensions of the products have been determined. From a set of process conditions given by the CAE results, an automatic design of experimentation procedure was conducted for locating the processing window. The processing window was then employed as the CAE inputs for establishing a process model by employing adaptive fuzzy-neural networks. In addition, a set of quasi-optimal process condition was achieved if an optimization objective had been determined based on production requirement. Finally, appropriate cycle-to-cycle control actions on tuning process conditions were taken while the pertinent feedback signals from the process were stored. This process control methodology has been demonstrated with test cases showing promising results.
研究并验证了一种基于计算机辅助工程系统(CAE)与过程控制模型相结合的新型注射成型过程控制系统。目标是通过利用CAE系统的结果,开发一种在线过程控制的科学方法。最初,在确定产品尺寸后,应借助CAE系统完成注塑产品的设计。根据CAE结果给出的一组工艺条件,对加工窗口的定位进行了实验程序的自动设计。然后将加工窗口作为CAE输入,利用自适应模糊神经网络建立过程模型。根据生产需求确定优化目标,得到一组准最优工艺条件。最后,对调谐过程条件采取适当的周期对周期控制动作,同时存储过程的相关反馈信号。这个过程控制方法已经用测试用例进行了演示,显示出有希望的结果。
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引用次数: 0
Finite Element Prediction of Sink Marks in Injection Molded Plastic Parts 注塑件凹痕的有限元预测
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0639
D. J. Battey, M. Gupta
A numerical procedure to simulate the formation of a sink mark near the base of a rib in an injection molded plastic part has been presented. Two commercially available software packages, C-Mold and Abaqus, have been used to predict sink marks. Dependence of sink mark depth on various geometric and molding parameters has been analyzed. The predicted sink mark depth is found to be in good agreement with experimental results from the literature.
介绍了一种模拟注塑件肋部凹痕形成的数值方法。两个商业上可用的软件包,C-Mold和Abaqus,已经被用来预测下沉分数。分析了凹痕深度与各种几何参数和成型参数的关系。预测的沉标深度与文献实验结果吻合较好。
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引用次数: 0
Real-Time Resin Temperature Measurements for Polymer Processing Using Fluorescence Spectroscopy 荧光光谱用于聚合物加工的实时树脂温度测量
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0630
A. J. Bur, K. Migler, Mark G. Vangel, D. Johnsonbaugh
We have developed a measurement methodology for measuring resin temperature and temperature profiles during processing using fluorescence spectroscopy. The technique consists of mixing a temperature sensitive fluorescent dye with a polymer resin at very low concentration, on the order of 10−6 molar concentration, and monitoring the temperature dependence of the fluorescence spectra. Two classes of fluorescent dyes are used: (a) excimer producing dyes such as bis-(pyrene) propane, and (b) band broadening dyes such as perylene and benzoxazolyl stilbene. Because the fluorescence measurement reflects the temperature in the neighborhood of the dye molecule, true resin temperature is observed and effects due the large thermal mass of the processing machine are minimized. Real-time monitoring was achieved using optical fiber sensors which were inserted into the process line at existing instrumentation ports. We monitored both injection molding and extrusion observing effects due to shear heating, crystallization and thermal diffusion. Temperature profiles in a flowing resin were measured using a sensor with confocal focusing optics. With this sensor, excitation light is focused to a point in the resin and the temperature at that point is deduced from the resultant fluorescence. In most cases, the fluorescence data must be corrected for effects due to pressure in order to yield an accurate temperature measurement.
我们已经开发了一种测量方法,用于测量树脂温度和温度分布过程中使用荧光光谱。该技术包括将温度敏感的荧光染料与聚合物树脂以非常低的浓度混合,大约为10−6摩尔浓度,并监测荧光光谱的温度依赖性。使用两类荧光染料:(a)产生准分子的染料,如双(芘)丙烷,和(b)增带染料,如苝和苯并恶唑二苯乙烯。由于荧光测量反映了染料分子附近的温度,因此可以观察到真实的树脂温度,并且可以将加工机器的大热质量所造成的影响降至最低。利用光纤传感器实现实时监测,光纤传感器插入到现有仪器端口的工艺线上。我们对注塑成型和挤压成型进行了监测,观察了剪切加热、结晶和热扩散的影响。用共聚焦光学传感器测量了流动树脂中的温度分布。利用该传感器,激发光聚焦到树脂中的一点,并从所得荧光推断出该点的温度。在大多数情况下,荧光数据必须纠正由于压力的影响,以产生准确的温度测量。
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引用次数: 0
Characterizing the Microstructure of Fused Deposition Polymer Components 熔融沉积聚合物构件的微观结构表征
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0636
J. Rodríguez, James P. Thomas, J. Renaud
The speed and accuracy with which Fused Deposition (FD) ABS plastic components can be made gives this rapid-prototyping technology unique potential as a new method for manufacturing complex structural components. Quantitative relationships between the FD process variables and the resulting mechanical properties are needed for intelligent manufacture of polymer components with tailored strength properties. This work examined the influence of the process variables on the resulting microstructure (void and interface bond length densities) of two configurations with uniaxial fiber orientation. The results showed the void and interface densities to be strongly dependent on the fiber-to-fiber gap and extrusion flow rate settings; the influence of extrusion and envelope temperatures is much smaller. The skewed fiber configuration exhibited the lowest void density but also the lowest interface density values. However, the difference observed in the values for the interface density were not as big as for the case of the void density. An investigation of the influence of the process variables on the interface bond strengths and the tensile behavior of pre- and post-extruded fibers as a function of loading rate and test temperature is in progress.
熔融沉积(FD) ABS塑料部件的速度和精度使这种快速成型技术成为制造复杂结构部件的一种新方法。智能制造具有定制强度性能的聚合物部件需要FD过程变量与所得力学性能之间的定量关系。本研究考察了工艺变量对两种单轴纤维取向结构的微观结构(空隙和界面键长密度)的影响。结果表明,孔隙密度和界面密度与纤维间间隙和挤出流速设置密切相关;挤压温度和包壳温度的影响要小得多。弯曲纤维结构的孔隙密度最低,界面密度值也最低。然而,界面密度值的差异并不像空洞密度值的差异那么大。研究了工艺变量对挤压前后纤维界面结合强度和拉伸性能的影响,并将其作为加载速率和测试温度的函数。
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引用次数: 2
Synthesis and Analysis of Quality Control Methods for Intelligent Processing of Polymeric Materials 高分子材料智能加工质量控制方法的合成与分析
Pub Date : 1997-11-16 DOI: 10.1115/imece1997-0633
D. Kazmer, T. Petrova
Global manufacturers of thermoplastic molded parts increasingly require 100% quality inspection levels that are difficult to achieve. While process complexity makes it difficult to attain the desired part properties during start-up. the stochastic nature of the process causes difficulty in maintaining part quality during production. This paper formally compares several alternative quality control methods that are currently utilized for processing of polymeric materials. To identify the technical issues associated with this goal, the injection molding process is described utilizing a control systems approach. Afterwards, four different methods of quality regulation are synthesized for injection molding: open loop quality control, statistical process control, trained parameter control, and on-line quality regression. For each strategy, the level of quality observability and controllability are determined against the dynamics of the manufacturing system. The results indicate that none of the quality regulation strategies have the underlying design architecture to deliver 100% quality assurance across a diverse set of application characteristics (quality requirements, material properties, mold geometries, and machine dynamics). As such, subsequent discussion focuses on defining the system requirements for achieving ‘intelligent’ processing of polymeric materials that are needed by industry.
全球热塑性模塑件制造商越来越多地要求100%的质量检测水平,这是很难实现的。而工艺的复杂性使其在启动时难以达到所需的零件性能。该工艺的随机性导致在生产过程中难以保持零件质量。本文正式比较了几种可供选择的质量控制方法,目前用于加工聚合物材料。为了确定与此目标相关的技术问题,使用控制系统方法描述了注射成型过程。然后,综合了四种不同的注射成型质量控制方法:开环质量控制、统计过程控制、训练参数控制和在线质量回归。对于每种策略,质量的可观察性和可控性水平是根据制造系统的动态来确定的。结果表明,没有一种质量管理策略具有潜在的设计架构,可以在各种应用特性(质量要求、材料特性、模具几何形状和机器动力学)中提供100%的质量保证。因此,后续讨论的重点是定义实现工业所需的聚合物材料“智能”加工的系统要求。
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引用次数: 0
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CAE and Intelligent Processing of Polymeric Materials
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