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PEROVSKITE PHOTOELECTRIC CONVERTERS WITHOUT HOLE-CONDUCTING BUFFER LAYERS 无空穴导电缓冲层的钙钛矿光电转换器
V. Kinev, A. D. Dmitrieva, P. Gladyshev
The review article is devoted to research in the field of the formation of photoelectric converters based on organic-inorganic perovskites without hole-conducting buffer layers using carbon materials as the back contact.
本文主要研究了以碳材料为背触点的无空穴导电缓冲层的有机-无机钙钛矿型光电转换器的形成。
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引用次数: 0
PHARMACEUTICAL FORMULATION MANUFACTURER DISCRIMINATION BY INFRARED SPECTROSCOPY AND PRINCIPAL COMPONENT ANALYSIS 红外光谱和主成分分析鉴别制剂生产厂家
E. Basova, Yu.N. Litvinenko, N. Polotnyanko
In the present work Fournier transform infrared (IR) spectroscopy in association with chemometric technique was employed to identify kind of tablet formulations containing paracetamol and/or caffeine as active pharmaceutical ingredients. 13 samples of 5 commercially available brand tablets of different manufacturers and batches were bayed in local pharmacies. IR spectra of samples were recorded in the range 600—4000 cm-1 and subjected to and principal component analysis (PCA) which allowed to clearly identify 5 clusters in the scores plot using the third and the second principal components, corresponding to the brands of tablets. For Paracetamol and Caffeine-sodium benzoate tablets the combination of IR spectroscopy and PCA was able to recognize the manufacturer on the basis of distance between samples in clusters in the PCA scores plot.
本文采用傅里叶变换红外光谱结合化学计量技术,对含有对乙酰氨基酚和/或咖啡因的片剂配方进行了鉴定。5个市售品牌、不同生产厂家、不同批次的13个样品在本地药店出售。在600-4000 cm-1范围内记录样品的红外光谱,并进行主成分分析(PCA),利用第三主成分和第二主成分在分数图中清晰地识别出5个簇,对应的是片剂的品牌。对于扑热息痛片和咖啡因苯甲酸钠片,红外光谱和主成分分析结合可以根据主成分分析评分图中聚类样本之间的距离来识别生产厂家。
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引用次数: 0
DEVELOPMENT OF A METHOD FOR DETERMINATION OF ALCOHOLS IN FORMATION WATER 地层水中醇类含量测定方法的建立
I. Mukhina, E.D. Gribovа, E. A. Denisova, D.A. Dyagil, A.V. Agaltsova
In this paper we propose an algorithm for the analysis of monohydric aliphatic alcohols in formation water, which makes it possible to eliminate the influence of non-polar components of oil. A sample of produced water is passed through a sorbent, removing non-polar organic compounds interfering with the analysis. In the resulting eluate add salting out agent and conduct a quantitative analysis of alcohols in the vapor phase by gas chromatography.
本文提出了一种分析地层水中一氢脂肪醇的算法,该算法可以消除油中非极性组分的影响。采出水样品通过吸附剂,去除干扰分析的非极性有机化合物。在所得洗脱液中加入盐析剂,用气相色谱法对气相中的醇类进行定量分析。
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引用次数: 0
FEASIBILITY OF THE BETA-ALBEDO-ABSORPTION TECHNIQUE APPLICATION FOR BUILDING NON-DESTRUCTIVE DEVICES APPLIED IN THE PRODUCTION OF NANOMATERIALS WITH MAIN DIMENSION PARAMETERS (THICKNESS, SURFACE DENSITY, AND COATING) -反照吸收技术在主要尺寸参数(厚度、表面密度、涂层)纳米材料生产中构建无损器件的可行性
V. G. Fedorkov
The explanation is given of the feasibility of using of a relatively unknown beta-albedo-absorption (BAA) technique, which was the research topic of the PHD thesis of the author, for the creation of a modern, unparalleled anywhere in the world, non-destructive testing (NDT) system to be used for the production of nanomaterials with main dimension parameters (thickness, surface density, and coating) in the nanorange, i.e., practically from zero to several hundreds of nanometers. The importance of the problem is determined by the present time intense development both in Russia and all over the world of the production of nanomaterials of different types in the practical absence of the development and production of NDT devices. Analytical expressions are given for the calculation of the main quantitative characteristics of BAA measurement geometry, namely, the radial density distribution and the integral electron backscattering coefficient at the variables of the parameters of the reflecting gas or air medium. The principle of developing the optimum measurement geometry, little dependent on changing parameters of the reflecting medium and minimizing measurement errors for BAA method, is described. The design of the developed detectors is shown. The following recommendations are given on additional experimental studies of the BAA method aiming to provide a possibility of parameter measurement in the nanorange: using the industrial beta sources with a lower value of the maximum beta spectrum energy; increasing the activity of beta sources or measurement time; using special filters for degradation of the beta source emission spectrum; and using beta radiation detectors with the largest possible measurement area.
解释了使用相对未知的β -反射率吸收(BAA)技术的可行性,这是作者博士论文的研究课题,用于创建现代的,世界上任何地方都无与伦比的无损检测(NDT)系统,用于生产纳米材料,其主要尺寸参数(厚度,表面密度和涂层)在纳米橙中,即实际上从零到几百纳米。这个问题的重要性是由目前俄罗斯和世界各地在实际缺乏无损检测装置的开发和生产的情况下,不同类型的纳米材料生产的紧张发展决定的。给出了BAA测量几何主要定量特征的解析表达式,即在反射气体或空气介质参数变量处的径向密度分布和积分电子后向散射系数。描述了BAA方法的最佳测量几何原理,该原理不依赖于反射介质参数的变化,并使测量误差最小化。最后给出了所研制的探测器的设计。对BAA方法的进一步实验研究提出了以下建议,旨在为纳米橙的参数测量提供可能性:使用最大光谱能量值较低的工业β源;增加β源的活度或测量时间;采用特殊滤波器对β源发射光谱进行降解;使用辐射探测器,测量面积最大。
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引用次数: 0
CAUCASUS DOLMENS PHOTOGRAMMETRY EFFICIENT EXPERIENCE IN RESOURCE-LIMITED SETTINGS 高加索石碑摄影测量在资源有限的情况下有效的经验
V.S. Stepchenkov, S. V. Valganov
The article presents a field experience in photogrammetric imagery and the Caucasus dolmen culture objects processing. This work objective is developing creative high quality three dimensional simple method in resource-limited settings. This approach analyzes insufficiently explored and hard-to-reach dolmen groups with interesting technical and cult elements. The objects are located in the Tuapse region: on the Mezetsu and Bzeuls ridges and on the upper of the Psynako river. As a result, we received eight high-precision models. There are seven standalone objects models and the three dolmens in these. Also, this article the collecting features and field data processing indicates. We believe our experience might be useful not in archaeology only but in other disciplines with similar objects fixing difficulties.
本文介绍了摄影测量成像和高加索石碑文物处理的实地经验。这项工作的目标是在资源有限的环境下发展创造性的高质量三维简单方法。这种方法分析了未充分探索和难以触及的具有有趣技术和邪教元素的墓葬群。这些物体位于Tuapse地区:Mezetsu和Bzeuls山脊以及Psynako河的上游。结果,我们得到了8个高精度模型。有7个独立的对象模型和其中的3个模型。并对采集特点和现场数据处理进行了说明。我们相信,我们的经验可能不仅对考古学有用,而且对其他具有类似物体的学科解决困难也有用。
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引用次数: 0
FORMATION OF ECOLOGICAL CULTURE AT THE PRESENT STAGE 现阶段生态文化的形成
O. Savvateeva, N. Shakhova, I. A. Starostina
In this article the condition of society ecological culture formation process at the present stage is considered. Ecological culture is directed to forming of harmonious relationship between the person and the environment, the organization of any activity according to fundamental laws of the nature and the principles of sustainable development in society. Without ecological aspects in our daily life it is impossible to pass to sustainable development. In work factors of ecological culture formation process, the main aspects and problems, trends in the field of ecological culture, experience of foreign countries and also experience of Dubna city in the sphere of ecological education system creation for increase of population ecological culture level are analyzed.
本文对现阶段社会生态文化形成过程的条件进行了思考。生态文化是指人与环境的和谐关系的形成,是指按照自然的基本规律和社会的可持续发展原则组织一切活动。在我们的日常生活中没有生态方面,就不可能过渡到可持续发展。在生态文化形成过程的工作因素中,分析了生态文化领域的主要方面和问题、发展趋势、国外的经验以及杜纳市在提高人口生态文化水平的生态教育体系创建方面的经验。
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引用次数: 0
FEATURES OF LONG-TERM SEISMICITY VARIATIONS OF ACTIVE MEGASTRUCTURES OF THE MODERN EARTH 现代地球大型活动构造地震活动性的长期变化特征
E. V. Arkhipova, A. Zhigalin, G. Bryantseva, I. Guseva, E.E. Tormysheva
On the basis of comparative analysis of long - term variations in the number of earthquakes, a number of characteristic features of the seismic regime in various geodynamic settings, including the subduction, collision, riftogenesis and spreading, are established. Among them there is a coordinated synchronous or antiphase change in the number of earthquakes for the regions within a single megastructure, coordinated changes in the activity of earthquakes at different deep levels. The data obtained indicate the systemic unity of the manifestations of the earth's seismicity and allow us to use the method of comparative analysis to identify dynamically connected volumes of the lithosphere.
在对地震次数的长期变化进行对比分析的基础上,建立了俯冲、碰撞、裂陷和扩张等不同地球动力学背景下地震活动的若干特征。其中,在同一巨型构造内各区域的地震次数有协调的同步或反相位变化,不同深层地震活动有协调的变化。所获得的数据表明地球地震活动性表现的系统统一性,使我们能够使用比较分析的方法来确定岩石圈的动态连接体。
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引用次数: 0
INVESTIGATION OF THE COMPOSITION OF MOSS, WHICH IS A NATURAL BIOINDICATOR, FOR AIR MONITORING IN THE EAST KAZAKHSTAN REGION 东哈萨克斯坦地区空气监测中天然生物指示剂苔藓成分的调查
N. Omarova, A. К. Tashenov, M. U. Nurkassimova, A. Kokoraeva
Here are the results of determining the chemical composition of moss in the East Kazakhstan region. The following research stages were carried out: harvesting plant materials; methods of taking samples of the studied material for analysis; determination of the concentration of elements by inductively coupled plasma mass spectrometry (ICP-MS). Developed methods for dry and wet ashing bioindicator. The results of the analysis of moss obtained by the ICP-MS method and the instrumental neutron activation analysis (INAA) method are compared. The reliability of the results of the analysis by the method of additives and photometric determination of the concentration of elements was determined.
这是测定东哈萨克斯坦地区苔藓化学成分的结果。研究分为以下几个阶段:收获植物材料;研究材料的取样分析方法;电感耦合等离子体质谱法测定元素浓度。开发干湿灰化生物指示剂的方法。比较了ICP-MS法和仪器中子活化分析(INAA)法对苔藓的分析结果。测定了添加剂法和光度法分析结果的可靠性。
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引用次数: 0
THE CHEMICAL COMPOSITION OF THE WATER OF THE FRESH LAKE BELOE (NP «MESHERA») ACCORDING TO THE METHOD OF ATOMIC EMISSION SPECTROMETRY WITH INDUCTIVELY COUPLED PLASMA 用电感耦合等离子体原子发射光谱法测定了贝洛伊(np«meshera»)淡水湖水的化学成分
E. Popova, A. V. Mikhailova, S. V. Morzhukhina, B. Zuev
The paper presents new data on the chemical composition of the water of Lake Beloye (FSFI «NP «Meshera», Ryazan region) for 2018, which supplement those obtained earlier – in 2013, 2014 and 2016. The choice of the method of analysis is justified – AES (OES) -ISP, as express and highly sensitive. The obtained data characterize the elemental composition of the Lake water, and are also ecological information for the state of the natural object. According to the available observations, it can be said that at present the waters of Lake Beloe are completely defined as «clean» by quality.
本文介绍了2018年贝洛耶湖(梁赞地区FSFI«NP«Meshera»)水化学成分的新数据,补充了2013年、2014年和2016年获得的数据。分析方法的选择是合理的- AES (OES) - isp,具有快速、高灵敏度的特点。获得的数据表征了湖水的元素组成,也是自然物体状态的生态信息。根据现有的观察,可以说,目前贝洛湖的水质完全被定义为“干净”。
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引用次数: 0
ACTIVE MOSS BIOMONITORING USING THE «MOSS BAG TECHNIQUE» AT THE STATE MUSEUM-RESERVE «TSARITSYNO» 使用“苔藓袋技术”在国家博物馆保护区“tsaritsyno”进行主动苔藓生物监测
M. Shvetsova, I. Kamanina, M. Frontasyeva, A. Madadzada, I. Zinicovscaia, S. Pavlov, K. Vergel, N. Yushin
Moscow is a large metropolis in which the air is affected by the constant effects of chemicals produced by industrial facilities, vehicles, residential heating and other human activities on a daily basis. The protected and park areas on the territory of Moscow have an important recreational role, therefore, air quality control in these territories should be carried out first. Active moss biomonitoring has been used as an alternative method to conventional atmospheric monitoring for more than 40 years. This type of biomonitoring is successfully applied all over the world: in China, Serbia, Moldova, Azerbaijan, Italy, Romania, etc. In this study, active moss biomonitoring was used for the first time on the territory of the Tsaritsyno Museum-Reserve to assess the air pollution. The moss species Sphagnum girgensohnii was chosen for the experiment. Neutron activation analysis was used to determine the concentrations of the elements: Na, Mg, Al, Cl, K, Ca, Sc, V, Cr, Mn, Fe, Co, Ni, Zn, Se, As, Br, Rb, Mo, Sr , Sb, Ba, Cs, La, Sm, Tb, Ce, Hf, Ta, W, Th, and U. The concentrations of Pb, Cu, and Cd were determined by atomic absorption spectrometry.
莫斯科是一个大城市,空气受到工业设施、车辆、住宅供暖和其他日常人类活动产生的化学物质的持续影响。莫斯科境内的保护区和公园具有重要的娱乐作用,因此,应首先对这些地区的空气质量进行控制。活性苔藓生物监测作为传统大气监测的替代方法已有40多年的历史。这种类型的生物监测在世界各地都得到了成功的应用:中国、塞尔维亚、摩尔多瓦、阿塞拜疆、意大利、罗马尼亚等。本研究首次在Tsaritsyno博物馆保护区使用活性苔藓生物监测对空气污染进行评价。实验选用苔藓植物Sphagnum girgensohnii。采用中子活化法测定了Na、Mg、Al、Cl、K、Ca、Sc、V、Cr、Mn、Fe、Co、Ni、Zn、Se、As、Br、Rb、Mo、Sr、Sb、Ba、Cs、La、Sm、Tb、Ce、Hf、Ta、W、Th、u等元素的浓度,采用原子吸收光谱法测定了Pb、Cu、Cd的浓度。
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引用次数: 0
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Bulletin of Dubna International University for Nature, Society, and Man. Series: Natural and engineering sciences
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