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Perbandingan Aktifitas Fotokatalis Nanotitania Tanpa Dan Dengan Penambahan Etanolamina Di Bawah Sinar Matahari 不含纳米纳米光质活性与太阳中乙酰氨基纳的补充进行比较
Pub Date : 2023-02-20 DOI: 10.23960/jtaf.v11i1.2767
Dita Rahmayanti, Posman Manurung, Roniyus Marjunus
Degradasi zat warna remazol kuning keemasan dilakukan dengan nanotitania. Sintesis nanotitania dipreparasi menggunakan metode sol gel dengan penambahan etanolamina sebagai surfaktan. Penelitian ini dilakukan bertujuan untuk mengetahui pengaruh penambahan etanolamina terhadap aktivitas fotokatalis dan energi celah pita nanotitania. Dalam penelitian ini penggunaan titanium butoksida, etanol dan HCl. Penambahan etanolamina yang divariasikan adalah 0 dan 1 ml. Sampel dikalsinasi pada suhu 500ºC selama 4 jam. Nanotitania dikaraterisasi menggunakan Spektrofotometri UV-Vis dan UV-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS) menggunakan metode Kubelka-Munk dalam menentukan energi celah pita. Uji aktivitas fotokatalis dengan mendegradasi larutan remazol kuning keemasan menggunakan sinar matahari sebagai pembantu terjadinya reaksi. Hasil karaterisasi UV-Vis DRS energi celah pita yaitu 3,18 dan 3,03 eV pada masing-masing sampel tanpa penambahan dan dengan penambahan etanolamina berturut-turut.
金黄色雷唑物质的退化是用纳米粒子进行的。使用sol凝胶合成物进行后悔修复,以补充乙酰氨基酚。这项研究的目的是确定光子化活性和纳米塔纳空间裂隙能量受到的影响。在这项研究中使用钛、乙醇和HCl。etanolamina增加不同的是0和1 500 ml。温度下样品dikalsinasiºC 4个小时。纳米火山利用UV-Vis光谱仪和uv - visiffuse反射反射器进行焦糖测定,使用Kubelka-Munk方法确定带孔能量。通过利用阳光作为反应辅助,通过降低金黄色雷南溶液的光合作用进行光化活动。对UV-Vis DRS能量段段化为3.18和3.03 eV的输出,而不需要连续添加乙酰氨基。
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引用次数: 0
SINTESIS DAN KARAKTERISASI WOLLASTONITE BERBASIS PREKUSOR BIOGENIK SILIKA ABU SEKAM PADI 以稻壳介质为基础的沃尔夫石合成和特性
Pub Date : 2023-02-20 DOI: 10.23960/jtaf.v11i1.2845
Amilia Rasitiani, Dwi Asmi, M. Badaruddin
The aim of this research is to make wollastonite from silica obtained from rice husk ash and commercial calcium carbonate using the solids reaction method. The DTA-TGA results show mass due to the evaporation of H2O and the decomposition of CaCO3 into CaO along with the calcination temperature, in addition, the DTA results also identify the formation of the β-CaSiO3 phase and the α-CaSiO3 phase. The XRD results of wollastonite obtained were dominated by the β-CaSiO3 phase and the minor phase was α-CaSiO3 this was indicated by the peak intensity of the β-CaSiO3 phase which was higher than the peak intensity of the α-CaSiO3 phase. the second phase in wollastonite is also the result of FTIR results through the analysis of the Si-O-Ca functional group in each wollastonite sample. In addition, the results of the SEM analysis showed the shape of the spheroidal particles (spherical) with an average grain size of 0.19 m, 0.35 m and 0.68 m for the calcination temperatures of 900 oC, 1000 oC and 1100 oC, respectively. The results of this study indicate that the manufacture of wollastonite from the basic ingredients of rice husk silica and commercial calcium carbonate has potential as an alternative material for the manufacture of wollastonite.
本研究以稻壳灰和商品碳酸钙为原料,采用固相反应法制备硅灰石。DTA- tga结果表明,随着煅烧温度的升高,H2O的蒸发和CaCO3分解为CaO产生了质量,DTA结果还确定了β-CaSiO3相和α-CaSiO3相的形成。所得硅灰石的XRD结果以β-CaSiO3相为主,次要相为α-CaSiO3相,可见β-CaSiO3相的峰值强度高于α-CaSiO3相的峰值强度。硅灰石中的第二相也是通过分析各硅灰石样品中Si-O-Ca官能团的FTIR结果得出的。SEM分析结果表明,在900℃、1000℃和1100℃的煅烧温度下,晶粒形状为球状,平均晶粒尺寸分别为0.19 m、0.35 m和0.68 m。本研究结果表明,以稻壳二氧化硅和商品碳酸钙为基本原料制备硅灰石具有作为硅灰石生产替代材料的潜力。
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引用次数: 1
Nanofiber PVA/ZnO Sebagai Material Antimikroba Pada Wound Dressings 纳米纤维聚乙烯醇/氧化锌Sebagai材料
Pub Date : 2023-02-20 DOI: 10.23960/jtaf.v11i1.3006
putri uzalia, D. Kusumawati
Nanofibers are ideal for forming multifunctional medical products, one of which is wound dressings. Nanofibers wound dressings made from polyvynyl alcohol (PVA) and zinc oxide (ZnO) using the electrospinning method with varying voltages of 15 kv, 16 kv, 18 kv, and 20 kv, to determine the effect of stress on morphology, absorption and antibacterial activity. The resulting nanofibers have a smooth surface and an almost uniform fiber diameter. SEM analysis showed that the diameter of PVA 10% with a magnification of 50000X was 252 nm and PVA/ZnO 20 kv with a magnification of 30000X was obtained 231 nm, the EDX spectrum contained elements of C, O, and Zn respectively 37.40%, 62.14%, and 0.46%. The results of the FTIR analysis showed that the functional groups seen in the PVA/ZnO samples were O-H, CH2, C-H, C-O, and Zn-O. UV-Vis transmission showed that PVA had a high UV transmission of 12% but all PVA/ZnO nanofibers showed a UV transmission of almost 0%. Antimicrobial activity showed that the number of bacterial colonies in PVA/ZnO samples was less than the control. The average nanofibers diameter increases when ZnO nanoparticles are added, but when tension is increased, the average diameter of the nanofibers decreases. The morphology of the nanofibers is very uniform and there are no ZnO nanoparticle crystals, so PVA/ZnO nanofibers can be chosen as an ideal biomaterial for wound dressings.
纳米纤维是制造多功能医疗产品的理想材料,其中之一就是伤口敷料。以聚乙烯醇(PVA)和氧化锌(ZnO)为原料,在15kv、16kv、18kv和20kv电压下采用静电纺丝法制备纳米纤维创面敷料,研究了应力对其形貌、吸收和抗菌活性的影响。得到的纳米纤维表面光滑,纤维直径几乎均匀。SEM分析表明,放大倍数为50000X、放大倍数为10%的PVA直径为252 nm,放大倍数为30000X、放大倍数为20kv的PVA/ZnO直径为231 nm, EDX光谱中C、O和Zn元素含量分别为37.40%、62.14%和0.46%。FTIR分析结果表明,PVA/ZnO样品中的官能团为O-H、CH2、C-H、C-O和Zn-O。紫外-可见透射结果表明,PVA/ZnO纳米纤维的紫外透射率高达12%,而所有PVA/ZnO纳米纤维的紫外透射率几乎为0%。抑菌活性表明,PVA/ZnO样品的菌落数量少于对照。随着ZnO纳米粒子的加入,纳米纤维的平均直径增加,但随着张力的增加,纳米纤维的平均直径减小。PVA/ZnO纳米纤维形态均匀,不存在ZnO纳米颗粒晶体,是一种理想的伤口敷料生物材料。
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引用次数: 0
Penerapan Jaringan Saraf Tiruan / JST (Backpropagation) untuk Prakiraan Cuaca di Bandar Udara Radin Inten II Lampung
Pub Date : 2023-02-20 DOI: 10.23960/jtaf.v11i1.3164
A. Saputra, S. Sulistiyanti, Roniyus Marjunus, Yanti Yuliant, J. Junaidi, Arif Surtono
Weather prediction is needed in planning daily life, one of which is to make decisions. The success of a weather prediction will have an impact on decision making in various fields, including agriculture and aviation. In the field of aviation, weather prediction is important to determine the time, location, direction of motion, altitude and plan the movement of aircraft to take into account operational disturbances that can be caused if the weather is bad and also to consider in determining flight routes or determining in carrying additional fuel if in an emergency. In the case of the aircraft having to return due to unfavorable weather conditions. Therefore the need for a good weather prediction method so as to reduce losses and damage. In this case the author tries to focus on the maximum parameters in the development of weather forecasting information design based on Artificial Neural Networks / Backpropagation by adding input data of rainfall, temperature, humidity, sunlight, air pressure, wind direction and wind speed. This research was conducted in the area of Radin Inten II Airport, Lampung. The material used in this study is in the form of daily data on meteorological conditions in the Radin Inten II Lampung Airport area from the Radin Inten II Meteorological Station for the last 3 years, from 2017 to 2019. This data is needed as input data for the algorithm that will be used in study. Based on the research results, the best training accuracy is 100% on the artificial neural network architecture with levenberg-marquardt training function parameters (trainlm) and scaled conjugate gradient (trainscg), binary sigmoid and bipolar sigmoid activation functions, and the number of neurons 20, 40, 60, 80, and 100. Meanwhile, the best test accuracy is 74,359% on the artificial neural network architecture with the training function parameters gradient descent wit momentum and adaptive learning rate (trainingdx) and binary sigmoid activation function (logsig) and the number of neurons 20 and 80.
天气预报是规划日常生活所需要的,其中之一就是做决定。天气预报的成功将对包括农业和航空在内的各个领域的决策产生影响。在航空领域,天气预报对于确定飞机的时间、地点、运动方向、高度和计划飞行十分重要,以考虑到天气恶劣时可能造成的操作干扰,并在确定飞行路线或在紧急情况下决定是否携带额外燃料时加以考虑。在飞机因恶劣天气条件不得不返回的情况下。因此需要一种良好的天气预报方法,以减少损失和损害。在本案例中,作者试图通过增加降雨量、温度、湿度、日照、气压、风向、风速等输入数据,关注基于人工神经网络/反向传播的天气预报信息设计开发中的最大参数问题。这项研究是在南榜的Radin Inten II机场进行的。本研究使用的材料是Radin Inten II气象站近3年(2017年至2019年)的Radin Inten II楠榜机场区域气象条件的每日数据。该数据需要作为将在研究中使用的算法的输入数据。基于研究结果,在levenberg-marquardt训练函数参数(trainlm)和尺度共轭梯度(trainscg)、二元s型和双极s型激活函数、神经元个数分别为20、40、60、80和100的人工神经网络架构下,训练精度达到100%。同时,在训练函数参数为带动量和自适应学习率的梯度下降(trainingdx)和二进制s型激活函数(logsig),神经元个数为20和80的人工神经网络结构上,测试准确率达到了74,359%。
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引用次数: 0
Plasma Non Thermal Sebagai Sterilisasi Masker untuk Inaktivasi Virus Corona (COVID-19) 非热等离子体,用于皮下抑制日冕病毒(COVID-19)
Pub Date : 2022-07-31 DOI: 10.23960/jtaf.v10i2.2935
Fadila Abdullah, Valentinus Galih Vidia Putra
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引用次数: 0
Perhitungan Desain Konsep Reaktor Cepat Berpendingin Karbondioksida Superkritis dan Berbahan Bakar Uranium Metalik Alam 计算设计的快速冷处理的二氧化碳概念超临界和自然金属铀燃料
Pub Date : 2022-07-31 DOI: 10.23960/jtaf.v10i2.3129
Via Vionita, Fiber Monado, Menik Ariani, Idha Royani
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引用次数: 0
Karakteristik Struktur Mikro, Struktur Fasa dan Sifat Fisis Komposit Silika Sekam Padi dengan Aspal 微结构、相位结构和沥青壳硅复合复合材料的特征
Pub Date : 2022-07-31 DOI: 10.23960/jtaf.v10i2.2658
Devi Ika Safitri, Simon Sembiring, Leni Rumiyanti
Synthesis and characterization silica of rice husks and asphalt composites have been carried out with a ratio of 65%: 35%; 70%: 30% and 75%: 25%. Silica synthesis from rice husk was carried out using the sol-gel method. The materials used in this research are rice husks, asphalt, aquades, gasoline, NaOH and HNO3. The purpose of this study was to determine the effect of silica and asphalt mass variations on the characteristics of microstructure, phase structure and physical properties namely density and porosity. Based on the research that has been done, it can be concluded that the results of SEM analysis show the formation of wad and cracks on the surface of the sample with an average grain size of 3,236 µm, 3,728 µm and 2,924 µm. In the EDS analysis results it can be seen that the elemental content contained in the samples is silica, oxygen, carbon, sulfur, sodium and aluminum. Where are the elements that dominate are the elements of silica, oxygen and carbon. Then based on XRD characterization results it is known that the sample has structure amorphous silica and amorphous carbon . The amorphous silica structure experiencing a shift 2θ with the highest peak intensity, from 2θ = 21˚ to 2θ = 22˚. Furthermore, the physical properties test of density 2.402 g / cm3, 2.692 g / cm3 and 2.852 g / cm3. In the physical properties test the porosity obtained was 9,825%, 8,028% and 6,835%.
以65%:35%的比例进行了稻壳硅与沥青复合材料的合成与表征;70%: 30%, 75%: 25%。以稻壳为原料,采用溶胶-凝胶法制备了二氧化硅。本研究使用的材料为稻壳、沥青、水、汽油、NaOH和HNO3。本研究的目的是确定二氧化硅和沥青质量变化对微观结构、相结构和物理性质(即密度和孔隙率)特征的影响。根据已做的研究可知,SEM分析结果显示试样表面形成了团块和裂纹,平均晶粒尺寸分别为3236µm、3728µm和2924µm。在EDS分析结果中可以看出,样品中所含的元素含量为二氧化硅、氧、碳、硫、钠和铝。占主导地位的元素是二氧化硅,氧和碳。然后根据XRD表征结果可知样品具有结构无定形二氧化硅和无定形碳。无定形二氧化硅结构发生2θ位移,峰强度最高,从2θ = 21˚到2θ = 22˚。并进行了密度为2.402 g / cm3、2.692 g / cm3和2.852 g / cm3的物理性能测试。物性测试获得的孔隙度分别为9825%、8028%和6835%。
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引用次数: 0
SINTESIS DAN KARAKTERISASI SERAT NANOTITANIA DENGAN METODE ELECTROSPINNING 通过电纺纱方法合成和合成纳米纤维
Pub Date : 2022-07-31 DOI: 10.23960/jtaf.v10i2.2730
Nurul Oktavia, Posman Manurung, J. Junaidi, Pulung Karo-Karo
. Titanium Dioxide (TiO 2 ) nanofibers have been prepared using the electrospinning method. This study aims to determine the morphology and crystal structure of the TiO 2 nanofibers and to determine the effect of viscosity on the morphology and crystal structure formed. This study used titanium tetraisopropoxide as a precursor, ethanol as a solvent, acetic acid as a solution stabilizer and controlled the hydrolysis reaction of the precursor, and PVP as a fiber-making material. The amount of variations of acetic acid is 2; 2.5; 3; 3.5; and 4 ml respectively. The results of the viscosity test showed that the greater the acetic acid used, the smaller the viscosity. The electrospinning process was carried out at a high voltage of 13 kV with a flow rate of 1.5 ml/hour. The fiber obtained was then calcined at 450 o C for 3 hours. The calcined sample was then analyzed using X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), and Transmission Electron Microscopy (TEM). SEM characterization results on samples B, C, and D showed that the sample diameters were 313 ± 28 nm, 275 ± 57 nm, and 242 ± 59 nm, respectively. The results of XRD characterization on sample D showed that the resulting sample had a tetragonal crystal structure with a mixed phase between anatase and rutile. The results of TEM characterization in sample D showed the fiber diameter with a size of 68.05 nm.
. 采用静电纺丝法制备了二氧化钛纳米纤维。本研究旨在确定二氧化钛纳米纤维的形貌和晶体结构,并确定粘度对形成的形貌和晶体结构的影响。本研究以四异丙醇钛为前驱体,乙醇为溶剂,乙酸为溶液稳定剂,控制前驱体的水解反应,PVP为制纤维材料。乙酸的变化量为2;2.5;3;3.5;分别是4ml。粘度测试结果表明,醋酸用量越大,粘度越小。静电纺丝过程在13 kV高压下进行,流速为1.5 ml/h。所得纤维在450℃下煅烧3小时。然后用x射线衍射(XRD)、扫描电子显微镜(SEM)和透射电子显微镜(TEM)对煅烧后的样品进行分析。样品B、C和D的SEM表征结果表明,样品直径分别为313±28 nm、275±57 nm和242±59 nm。样品D的XRD表征结果表明,样品具有锐钛矿和金红石混合相的四方晶体结构。样品D的TEM表征结果表明,纤维直径为68.05 nm。
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引用次数: 0
Analisis Pengaruh Ketinggian Tanah dan Kedalaman Sumur terhadap Suhu dan pH Air Sumur di Kabupaten Blitar
Pub Date : 2022-07-31 DOI: 10.23960/jtaf.v10i2.3010
Muhammad Syafa Tirtana Sanjaya, Tamara Pingki
{"title":"Analisis Pengaruh Ketinggian Tanah dan Kedalaman Sumur terhadap Suhu dan pH Air Sumur di Kabupaten Blitar","authors":"Muhammad Syafa Tirtana Sanjaya, Tamara Pingki","doi":"10.23960/jtaf.v10i2.3010","DOIUrl":"https://doi.org/10.23960/jtaf.v10i2.3010","url":null,"abstract":"","PeriodicalId":314761,"journal":{"name":"Jurnal Teori dan Aplikasi Fisika","volume":"31 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"116450612","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
CALIBRATION TEST RESULT ACCELEROMETER SENSOR 校准加速度计传感器的测试结果
Pub Date : 2022-07-31 DOI: 10.23960/jtaf.v10i2.2813
Quart Ferrina, S. R. Sulistiyanti, J. Junaidi
{"title":"CALIBRATION TEST RESULT ACCELEROMETER SENSOR","authors":"Quart Ferrina, S. R. Sulistiyanti, J. Junaidi","doi":"10.23960/jtaf.v10i2.2813","DOIUrl":"https://doi.org/10.23960/jtaf.v10i2.2813","url":null,"abstract":"","PeriodicalId":314761,"journal":{"name":"Jurnal Teori dan Aplikasi Fisika","volume":"29 3 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128707904","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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