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THE EFFECT OF THE DC-SPUTTERING PROCESS ON CHANGES IN THE HARDNESS VALUE AND ELEMENTS COMPOSITION OF BIOCOMPATIBLE STAINLESS STEEL 316L MATERIAL 直流溅射工艺对生物相容性不锈钢 316l 材料硬度值和元素组成变化的影响
Pub Date : 2024-03-14 DOI: 10.55981/gnd.2023.6834
Nuha Nazilah Sahabudin, Uli Aprilia Mukaromah, W. Andriyanti, Heri Sutanto
Titanium Dioxide (TiO2) thin films have intriguing optical, photocatalytic, and electrical properties and have been investigated for various applications, including solar cells, biomaterials, corrosion-resistant materials, and gas sensor. In this study, TiO2 thin films were deposited on the surface of 316L Stainless Steel  to improve its mechanical properties as an implant material. The deposition method used was DC sputtering with variations in deposition times of 30, 60, 90, 120, and 150 minutes. Vickers hardness test and SEM-EDX characterization were carried out to determine the hardness value, elemental composition, and thickness of the TiO2 thin film formed. Based on these tests, it was discovered that the optimal hardness value of316L stainless Steel  material was attained at a deposition period of 90 minutes with a hardness value of 170.10 VHN, and the average thickness of the layer formed was ± 119.02 μm.
二氧化钛(TiO2)薄膜具有引人入胜的光学、光催化和电学特性,已被研究用于太阳能电池、生物材料、耐腐蚀材料和气体传感器等多种应用。本研究在 316L 不锈钢表面沉积了二氧化钛薄膜,以改善其作为植入材料的机械性能。采用的沉积方法是直流溅射,沉积时间分别为 30、60、90、120 和 150 分钟。通过维氏硬度测试和 SEM-EDX 表征,确定了所形成的二氧化钛薄膜的硬度值、元素组成和厚度。根据这些测试发现,316L 不锈钢材料在沉积时间为 90 分钟时达到了最佳硬度值,硬度值为 170.10 VHN,所形成薄膜的平均厚度为 ± 119.02 μm。
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引用次数: 0
PENENTUAN TINGKAT KLIERENS LIMBAH RADIOAKTIF HASIL SEMENTASI KONSENTRAT EVAPORASI DAN TINJAUAN KESELAMATAN PEMBUANGANNYA 确定蒸发浓缩胶结产生的放射性废物的等级并对其处置进行安全审查
Pub Date : 2024-03-13 DOI: 10.55981/gnd.2023.6839
S. Suhartono, Noor Anis Kundari, M. Romli, Sumarbagiono Sumarbagiono
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引用次数: 0
CESIUM CHEMISORPTION ONTO STAINLESS STEEL UNDER SIMULATED LIGHT WATER REACTOR SEVERE ACCIDENT 模拟轻水反应堆严重事故下不锈钢上的铯化学吸附作用
Pub Date : 2024-03-13 DOI: 10.55981/gnd.2023.6809
Wayan Ngarayana
During light water reactor severe accident, source terms may interact with structural materials, generating new compounds and affecting their volatility which make the existing codes could not accurately estimate the radioactive release. Cesium is one of the source terms that can interact with structural materials and contributes greatly to the late release phenomenon. Several studies have been conducted to predict the physicochemical interactions between cesium and structural materials. However, the types of chemisorbed cesium compounds onto structural materials are still under discussion. For this reason, this study was carried out using advanced techniques, involving TEM, SEM, EDS and FIB to estimate the chemisorbed cesium compounds onto stainless steel structural material under simulated light water severe accident. This study indicates that cesium is strongly adsorbed on the oxide layer of stainless steel in the form of cesium silica, cesium aluminum silica, and/or cesium ferro silica. CsFeSiO4 and CsAlSiO4 could dominate these compounds.
在轻水反应堆严重事故中,源项可能与结构材料发生相互作用,生成新的化合物并影响其挥发性,这使得现有的代码无法准确估计放射性释放。铯是能与结构材料相互作用的源项之一,对后期释放现象有很大影响。已有多项研究对铯与结构材料之间的物理化学相互作用进行了预测。然而,结构材料上化学吸附铯化合物的类型仍在讨论之中。因此,本研究采用先进技术,包括 TEM、SEM、EDS 和 FIB,对模拟轻水严重事故下不锈钢结构材料上的化学吸附铯化合物进行了估算。研究表明,铯以铯硅石、铯铝硅石和/或铯铁硅石的形式强烈吸附在不锈钢的氧化层上。CsFeSiO4 和 CsAlSiO4 可能是这些化合物中的主要成分。
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引用次数: 0
AN IMPROVEMENT OF ARJUNA 1.0 CONVEYOR SYSTEM FOR 3D IRRADIATION 改进 Arjuna 1.0 输送系统,用于 3D 辐照
Pub Date : 2024-03-13 DOI: 10.55981/gnd.2023.6826
Saefurrochman Saefurrochman, Agus Tri Purwanto, S. R. Adabiah, Sukaryono Sukaryono, Galih Setiaji, Dwi Handoko Arthanto, Karina Anggraeni, Isti Dian Rachmawati, Agus Dwiatmaja, Wijono Wijono, Elin Nuraini, W. Andriyanti, D. Darsono, Andreas Bimo Putro Adjie
An improved design of the conveyor system of Arjuna 1.0 electron accelerator for 3D object irradiation has been done. The penetration of low energy electrons is less than 1 cm in the surface, causing a challenge for the irradiation process for sterilization of 3D objects. We design a conveyor that can be rotated 360o to irradiate objects evenly. The dimension of this conveyor is 1750 x 600 x 800 mm and the maximum diameter of the object is 7 cm. Based on the Frame Bending Stress analysis to calculate the strength of the conveyor frame, it is shown that the maximum displacement is only 0.029 mm, which is very small so it will cause no disturbance to power transfer from the motor to the conveyor. The normal stress (Smax) is 3.926 MPa and the bending stress for Smax (Mx) and Smax (My), are 2.391 MPa and 3.925 MPa respectively. We also calculate the stress analysis of the 3 mm-thickness of the motor mount and found that the Von-Misses Stress, first, and third Principal Stress are 4.425 MPa, 5.01 MPa, and 1.95 MPa respectively. These results confirm that the design and the material used for the conveyor are safe because the stress is very low than the material’s yield strength which is 207 MPa. The power needed for this conveyor is 0.01724 kW, with a maximum speed is 880 rpm. The new model of 3D conveyor has been constructed and can be implemented to ARJUNA 1.0 to irradiate objects on all its surfaces
Arjuna 1.0 电子加速器用于三维物体辐照的传送系统的改进设计已经完成。低能电子在物体表面的穿透力小于 1 厘米,这给三维物体的辐照灭菌过程带来了挑战。我们设计了一种可 360 度旋转的传送带,以均匀辐照物体。该传送带的尺寸为 1750 x 600 x 800 毫米,物体的最大直径为 7 厘米。根据框架弯曲应力分析计算传送带框架的强度,结果表明最大位移仅为 0.029 毫米,非常小,因此不会对从电机到传送带的动力传输造成干扰。法向应力(Smax)为 3.926 兆帕,Smax(Mx)和 Smax(My)的弯曲应力分别为 2.391 兆帕和 3.925 兆帕。我们还计算了厚度为 3 毫米的电机支架的应力分析,发现 Von-Misses 应力、第一主应力和第三主应力分别为 4.425 兆帕、5.01 兆帕和 1.95 兆帕。这些结果证实,输送机的设计和所用材料是安全的,因为应力比材料的屈服强度(207 兆帕)非常低。该输送机所需的功率为 0.01724 kW,最高转速为 880 rpm。新的 3D 输送机模型已经制作完成,可以在 ARJUNA 1.0 中实施,对物体的所有表面进行辐照。
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引用次数: 0
STUDY OF POISSON NOISE REDUCTION ON GAMMA CAMERA IMAGE USING SPATIAL DOMAIN FILTER 利用空间域滤波器降低伽马相机图像上的泊松噪声研究
Pub Date : 2024-03-13 DOI: 10.55981/gnd.2023.6822
Ayu Jati Puspitasari, R. Karthika, Puspa Ayu Nugrahani, Widya Febrianti, Nur Rahmah Hidayati
A gamma camera image is produced by a gamma camera that detects the gamma radiation emitted by the radioactive substance or radiopharmaceutical injected into the body. The gamma camera image sometimes has noise that can interfere with the diagnosis. This image is commonly affected by a Poisson-type random noise. This research proposes using a spatial domain filter to study Poisson noise reduction in gamma camera images. The image sample used is the image of a mouse injected with Lu-177-DOTA Trastuzumab with 100 µCi activity detected using a dual-head gamma camera with NaI(Tl) detectors. The grayscale image is treated with Poisson noise, then improved using a spatial domain filter. The spatial domain filters used include Mean, Median, Wiener, and Spatial Lowpass Filters. The mean filter is the best one that can reduce Poisson noise among the four applied filters. The best filter size for noise reduction is 3 with MSE 5.07, PSNR 41.08 dB, and SSIM 0.99.
伽马相机图像是由伽马相机产生的,它能检测到注入体内的放射性物质或放射性药物所发出的伽马射线。伽马相机图像有时会出现干扰诊断的噪声。这种图像通常会受到泊松型随机噪声的影响。本研究建议使用空间域滤波器来研究伽马相机图像中的泊松噪声降低问题。所使用的图像样本是一只注射了 Lu-177-DOTA 曲妥珠单抗的小鼠的图像,其活性为 100 µCi,使用带有 NaI(Tl) 探测器的双头伽马相机进行检测。灰度图像采用泊松噪声处理,然后使用空间域滤波器进行改进。使用的空间域滤波器包括均值滤波器、中值滤波器、维纳滤波器和空间低通滤波器。平均值滤波器是四种滤波器中能降低泊松噪声的最佳滤波器。最佳降噪滤波器大小为 3,MSE 为 5.07,PSNR 为 41.08 dB,SSIM 为 0.99。
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引用次数: 0
ANALISIS KESELAMATAN UNTUK MENCEGAH KECELAKAAN PADA PROSES EVAPORASI DI INSTALASI ELEMEN BAKAR EKSPERIMENTAL DENGAN METODE HAZOPS 用危害分析法对实验燃烧元件厂蒸发过程中的事故预防进行安全分析
Pub Date : 2024-03-13 DOI: 10.55981/gnd.2023.6844
Putra Oktavianto, Noor Anis Kundari, A. Saputra, Imam Abdurrosyid, Andri Saputra
SAFETY ANALYSIS TO PREVENT ACCIDENTS IN THE EVAPORATION PROCESS AT EXPERIMENTAL FUEL ELEMENT INSTALLATION WITH THE HAZOPS METHOD. The Experimental Fuel Element Installation (IEBE) DPFK-BRIN has implemented safety standards as a safety reference using Hazard Identification Risk Assessment Determining Control (HIRADC). The HIRADC method has several lacks, so its application is not optimal. In this study, as a complement to the HIRADC method, a risk analysis was carried out using the Hazard and Operability Study (HAZOPS). The hazard identification was carried out during the evaporation process of the uranyl nitrate solution in the E-601 evaporator tank. The HAZOPS method is based on process and instrumentation diagrams (P&ID) to determine the potential hazards during evaporation. It is carried out by determining the nodes and parameters, analyzing deviations from each node or the potential danger of each node, the possible causes of deviations and their consequences, determining the likelihood scale and the level of risk, and making recommendations. Based on the assessment, six nodes were obtained, resulting in 11 deviations caused by 13 equipment malfunctions or failures. The risk assessment of 13 damages resulted in 1 potential low-hazard risk and 12 potential medium-hazard risks. The low-hazard risk category can be overcome by routine handling, such as preventive maintenance and regular equipment calibration. For the medium-hazard risk category, recommendations such as those for the low-hazard risk category and others are necessary to overcome deviations that may occur according to deviation type. According to safety assessment results, it can be concluded that HAZOPS can complement HIRADC to ensure safety is maintained during the process.
在实验燃料元件装置的蒸发过程中采用危害分析方法预防事故的安全分析。燃料元件实验装置(IEBE)DPFK-BRIN 采用危害识别风险评估确定控制法(HIRADC),将安全标准作为安全参考。HIRADC 方法存在一些缺陷,因此其应用效果并不理想。在本研究中,作为对 HIRADC 方法的补充,使用了危险和可操作性研究(HAZOPS)进行风险分析。危险识别是在 E-601 蒸发罐中硝酸铀酰溶液的蒸发过程中进行的。HAZOPS 方法基于工艺和仪表图 (P&ID),用于确定蒸发过程中的潜在危险。它通过确定节点和参数、分析每个节点的偏差或每个节点的潜在危险、偏差的可能原因及其后果、确定可能性标度和风险等级,并提出建议。根据评估结果,获得了 6 个节点,导致 13 个设备故障或失灵造成 11 个偏差。对 13 项损害进行风险评估后,得出 1 项潜在低危害风险和 12 项潜在中等危害风险。低危害风险类别可通过日常处理来克服,如预防性维护和定期设备校准。对于中度危险风险类别,有必要根据偏差类型提出低度危险风险类别的建议和其他建议,以克服可能出现的偏差。根据安全评估结果,可以得出 HAZOPS 可以作为 HIRADC 的补充,确保工艺过程中的安全。
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引用次数: 0
Effect of Collimator Elements on the Beam Spectrum and KERMA In Gamma Irradiator 准直器元件对γ辐照器光束谱和KERMA的影响
Pub Date : 2021-11-19 DOI: 10.17146/gnd.2021.24.2.6307
R. Tursinah, B. Bunawas, Tri Cahyo, A. Suherman, P. Sukmabuana
In the development of low-medium energy photon calibration facilities we have simulated several types of gamma irradiator collimator materials with ISO 4037-1 design connected to the output beam spectrum and the resulting kerma. Four types of collimator material, namely Al, Fe, Pb, and WCu have been simulated with gamma radiation sources 241Am, 57Co, 137Cs, and 60Co. Simulations were carried out using the Monte Carlo method with the PHITS computer program. Based on the comparison of air kerma produced, collimators made from Al are suitable for gamma sources 241Am, Fe material for gamma sources 57Co, and Pb material for sources 137Cs and 60Co.
在中低能量光子校准设备的开发中,我们模拟了几种类型的伽玛辐照准直器材料,采用ISO 4037-1设计,连接到输出光束光谱和由此产生的克尔玛。用241Am、57Co、137Cs、60Co等γ辐射源对Al、Fe、Pb、WCu四种准直材料进行了模拟。采用蒙特卡罗方法和PHITS计算机程序进行了模拟。通过对制备的空气准直器的比较,Al准直器适用于241Am源,Fe准直器适用于57Co源,Pb准直器适用于137Cs和60Co源。
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引用次数: 0
PERANCANGAN DAN IDENTIFIKASI KENDALI PID PADA ALIRAN HIDROGEN SUMBER ION SIKLOTRON DECY 13
Pub Date : 2021-11-19 DOI: 10.17146/gnd.2021.24.2.6320
Fajar Sidik Permana, Nazrul Effendy, A. Wardana
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引用次数: 1
Preliminary Study on Minor Actinide Incineration in RSG-GAS without Isotope Separation 无同位素分离的RSG-GAS中微量锕系元素焚烧的初步研究
Pub Date : 2021-11-19 DOI: 10.17146/gnd.2021.24.2.6241
R. A. P. Dwijayanto, M. Alfarisie
Minor actinides (MA) resulted from nuclear power plants is often considered as nuisance in spent fuel management due to its considerably long half-life. One of available strategies to deal with MA is to incinerate it, in order to reduce its radioactivity. This paper presents a study on MA incineration in RSG-GAS research reactor. Unlike previous study, this work did not separate the MA into individual isotopes, but incinerated as a whole. ORIGEN2.1 code is employed to calculate MA incineration within RSG-GAS core. MA composition used in this study consists of Np, Am, and Cm isotopes. The Central Irradiation Position (CIP) of RSG-GAS is loaded by 6 kg of MA and irradiated for two years. The result shows that about 1 kg of MA were incinerated after two years of irradiation, or 18,87% of the initial concentration. However, the increase of Cm-242 isotope, along with newly-formed Pu isotopes, were found to be significantly increasing short-term radioactivity compared to un-irradiated MA. Thus, two years-worth of MA incineration cannot be considered as effective, and other strategies must be pursued.
核电厂产生的微量锕系元素由于其相当长的半衰期,在乏燃料管理中经常被认为是一个麻烦。处理放射性物质的一种有效策略是将其焚烧,以降低其放射性。本文介绍了在RSG-GAS研究堆中进行MA焚烧的研究。与以前的研究不同,这项工作没有将MA分离成单独的同位素,而是作为一个整体焚烧。采用ORIGEN2.1代码计算RSG-GAS堆芯内的MA焚烧量。本研究中使用的MA组成由Np、Am和Cm同位素组成。RSG-GAS的中心照射位置(CIP)装载6 kg MA,照射2年。结果表明,经过两年的辐照后,约有1kg的MA被焚烧,占初始浓度的18.87%。然而,与未辐照的MA相比,Cm-242同位素的增加以及新形成的Pu同位素显著增加了短期放射性。因此,两年的MA焚烧不能被认为是有效的,必须采取其他策略。
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引用次数: 1
PLANAR SCINTIGRAPHY IMAGE DE-NOISING USING COIFLET WAVELET 基于螺旋小波的平面闪烁图像去噪
Pub Date : 2021-11-19 DOI: 10.17146/gnd.2021.24.2.6280
Ayu Jati Puspitasari, Ika Cismila Ningsih, Muhammad Sulthonur Ridwan, H. Hamadi
The planar scintigraphic image usually has poor resolution and contains noise. This noise can be removed using the coiflet wavelet method so that the image quality gets better. This coiflet wavelet method is a noise reduction method based on frequency analysis. The planar scintigraphy image is the reconstructed image of the gamma radiation count data (phantom with the Cs-137 source in it). The original image is 15×15 pixel. Before the de-noising process, the image went through an interpolation process, which is to increase the pixel size of the image. The original image enlarged to 70×70, 480×480, and 1200×1200 pixel. After de-noising with coiflet wavelet, the image quality is measured based on MSE and PSNR parameters. The resulting images are quite good, with MSE values are close to zero and PSNR values of more than 60 dB. The smaller the MSE and the bigger the PSNR, is getting the better the image quality. In this study, the results show that the 1200×1200 pixel image has the best quality. It means that the image enlargement process has a good effect on the de-noising process, especially if the original image has a low resolution.
平面闪烁图像通常分辨率较差,且含有噪声。利用coiflet小波方法可以去除这些噪声,从而提高图像质量。螺旋小波法是一种基于频率分析的降噪方法。平面闪烁图像是伽马辐射计数数据的重建图像(其中含有Cs-137源的幻像)。原始图像为15×15像素。在去噪之前,对图像进行插值处理,即增加图像的像素大小。将原始图像放大到70×70、480×480和1200×1200像素。用coiflet小波去噪后,基于MSE和PSNR参数测量图像质量。得到的图像效果非常好,MSE值接近于零,PSNR值大于60 dB。MSE越小,PSNR越大,图像质量越好。在本研究中,结果表明1200×1200像素图像的质量最好。这意味着图像放大过程对去噪过程有很好的效果,特别是在原始图像分辨率较低的情况下。
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引用次数: 0
期刊
Ganendra Majalah IPTEK Nuklir
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