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A microfluidic study of transient flow states in permeable media using fluorescent particle image velocimetry 利用荧光粒子图像测速技术研究可渗透介质中瞬态流动状态的微流体
Q1 Physics and Astronomy Pub Date : 2021-10-26 DOI: 10.46690/capi.2021.04.03
Jindi Sun, Ziqiang Li, F. Furtado, Saman A. Aryana
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引用次数: 8
Development of adsorption ratio equation and state equation of liquid and their geological significance 液体吸附比方程和状态方程的发展及其地质意义
Q1 Physics and Astronomy Pub Date : 2021-08-23 DOI: 10.46690/capi.2021.04.01
Junqian Li
There have been many theories to describe adsorbed or free gas. However, quantitative description of the occurrence characteristics of liquids in porous media has always been a great challenge due to a lack of basic theory. Through years of research, two theoretical equations, i.e., adsorption ratio equation and state equation of liquid, have been proposed to describe the characteristics of liquids in porous media, and revealed the mechanism of liquid occurrence. Further, a quantitative evaluation technology for the microscopic distribution of liquids was established by combining nuclear magnetic resonance theory. This research will be of great significance for studying the microscopic distribution of liquids in tight reservoirs, such as shale, coal, and tight sandstone. Cited as:  Li, J. Development of adsorption ratio equation and state equation of liquid and their geological significance. Capillarity, 2021, 4(4): 63-65, doi: 10.46690/capi.2021.04.01
已经有许多理论来描述吸附气体或游离气体。然而,由于缺乏基础理论,对多孔介质中液体赋存特征的定量描述一直是一个巨大的挑战。通过多年的研究,提出了描述多孔介质中液体特性的吸附比方程和液体状态方程两个理论方程,揭示了液体的发生机理。结合核磁共振理论,建立了液体微观分布的定量评价技术。该研究对研究页岩、煤、致密砂岩等致密储层流体微观分布具有重要意义。李静。液体吸附比方程和状态方程的发展及其地质意义。毛细管学,2021,4(4):63-65,doi: 10.46690/capi.2021.04.01
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引用次数: 10
An experimental study of imbibition process and fluid distribution in tight oil reservoir under different pressures and temperatures 不同压力和温度条件下致密油储层渗吸过程及流体分布的实验研究
Q1 Physics and Astronomy Pub Date : 2021-08-17 DOI: 10.46690/capi.2021.04.02
Yishen Liang, F. Lai, Yuting Dai, H. Shi, Gongshuai Shi
Cited as: Liang, Y., Lai, F., Dai, Y., Shi, H., Shi, G. An experimental study of imbibition process and fluid distribution in tight oil reservoir under different pressures and temperatures. Capillarity, 2021, 4(4): 66-75, doi: 10.46690/capi.2021.04.02 Abstract: Tight reservoirs are a major focus of unconventional reservoir development. As a means to improve hydrocarbon recovery from tight reservoirs, imbibition has been received increasing attentions in recent years. This study evaluates how the changes in temperature and pressure affect imbibition through conducting experimental tests under various conditions on samples from the Yan Chang formation, a tight reservoir in Ordos Basin. The fluid distribution is compared before and after imbibition in core samples by nuclear magnetic resonance method. The results show that the imbibition recovery is significantly improved through increasing temperature and pressure. A high temperature facilitates molecular thermal movements, increasing oil-water exchange rate. The core samples are characterized with nano-mesopores, which is followed by nano-macropores, micropores, mesopores, and nano-micropores. Comparative analysis of nuclear magnetic resonance shows that the irreducible water saturation increases after imbibition and is mainly distributed in nanopores. Increasing pressure increases the amount of residual water in nano pores, with the relatively more significant increase in the amount of residual water in nanomacro-pores compared with other types of pores.
引用本文:梁毅,赖峰,戴毅,石辉,石刚。不同压力和温度下致密油储层渗吸过程及流体分布的实验研究。摘要:致密储层是非常规油藏开发的重点之一。渗吸作为提高致密储层油气采收率的一种手段,近年来受到越来越多的关注。通过对鄂尔多斯盆地延昌组致密储层样品进行不同条件下的渗吸实验,研究了温度和压力变化对渗吸的影响。用核磁共振法比较了吸胀前后岩心样品的流体分布。结果表明,提高温度和压力可显著提高渗吸采收率。高温有利于分子热运动,提高油水交换速率。岩心样品以纳米介孔为主,依次为纳米大孔、纳米微孔、中孔和纳米微孔。核磁共振对比分析表明,吸胀后不可还原水饱和度增加,主要分布在纳米孔中。压力的增加使纳米孔隙中残余水的含量增加,且纳米宏观孔隙中残余水含量的增加相对于其他类型的孔隙更为显著。
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引用次数: 14
Numerical study of the effect of tortuosity and mixed wettability on spontaneous imbibition in heterogeneous porous media 非均质多孔介质中弯曲度和混合润湿性对自发吸胀影响的数值研究
Q1 Physics and Astronomy Pub Date : 2021-07-24 DOI: 10.46690/capi.2021.03.02
Zhenhan Diao, Sheng Li, Wei Liu, Haihu Liu, Q. Xia
Spontaneous imbibition in porous media plays an important role in numerous industrial processes, but its underlying mechanisms are still poorly understood due to the complicated structure and multiple surface properties of natural porous media. In order to fill this gap, a quasi-three-dimensional color-gradient lattice Boltzmann model is applied to simulate the spontaneous imbibition in heterogeneous porous media micromodels, where the influence of viscosity ratio, tortuosity and mixed wettability is systematically investigated. Results show that the tortuosity has less influence on imbibition than the viscosity ratio, which leads to unstable displacement for viscosity ratios smaller than unity and to stable displacement for viscosity ratios greater than unity. By establishing the power-law relationship between wetting fluid saturation and time, it is found that the scaling exponent is not only affected by tortuosity, but also related to pore throat structure of the micromodel. In addition, the mixed wettability is found to significantly influence the stability of displacement, especially when the contact angle difference of two constituents is large. Specifically, the greater the mixing degree of two wettabilities, the more unstable the displacement will become, which results in an enhanced interface roughening. Accordingly, the scaling exponent deviates more from the prediction from the Lucas-Washburn equation. Due to the reduced connectivity of flow paths, the wetting fluid imbibition rate in mixed wettability condition is lower than that in uniform wettability condition, no matter whether the latter theoretically corresponds to a slow displacement or not. Cited as: Diao, Z., Li, S., Liu, W., Liu, H., Xia, Q. Numerical study of the effect of tortuosity and mixed wettability on spontaneous imbibition in heterogeneous porous media. Capillarity, 2021, 4(3): 50-62, doi: 10.46690/capi.2021.03.02
多孔介质的自发渗吸在许多工业过程中发挥着重要作用,但由于天然多孔介质结构复杂、表面性质多样,人们对其潜在机制仍知之甚少。为了填补这一空白,采用准三维颜色梯度晶格玻尔兹曼模型模拟非均质多孔介质微模型中的自发吸胀,系统地研究了粘度比、扭曲度和混合润湿性对自发吸胀的影响。结果表明:挠度对吸胀的影响小于粘度比,当粘度比小于1时,驱替不稳定,当粘度比大于1时,驱替稳定;通过建立润湿流体饱和度与时间的幂律关系,发现尺度指数不仅受扭曲度的影响,还与微模型的孔喉结构有关。此外,混合润湿性对驱替稳定性有显著影响,特别是当两组分接触角差较大时。具体来说,两种润湿性的混合程度越大,位移越不稳定,导致界面粗化增强。因此,标度指数更偏离卢卡斯-沃什伯恩方程的预测。由于流路连通性降低,混合润湿性条件下的润湿液吸吸速率低于均匀润湿性条件下的润湿液吸吸速率,无论后者在理论上是否对应缓慢驱替。引用本文:刁中,李生,刘伟,刘辉,夏强。非均质多孔介质中弯曲度和混合润湿性对自发吸胀影响的数值研究。毛细管学,2021,4(3):50-62,doi: 10.46690/capi.2021.03.02
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引用次数: 19
Dynamic behavior of droplet formation in dripping mode of capillary flow focusing 毛细聚焦滴模式下液滴形成的动力学行为
Q1 Physics and Astronomy Pub Date : 2021-07-02 DOI: 10.46690/capi.2021.03.01
T. Si
Experimental study on the liquid dripping in a capillary flow focusing process is performed. Due to the high-speed gas stream that drives the inner liquid co-flowing through an orifice, complex phenomena for the droplet formation in dripping regime can be found as the gas pressure drop and the liquid flow rate change. Periodic dripping mode can produce uniform droplets, and non-periodic ones can result in satellites and droplets of different diameters. The droplet-droplet coalescence in the core of co-flowing gas stream is also obtained. The size of resultant droplets is measured under different values of gas pressure drop and liquid flow rate. It can be seen that the droplet size tends to decrease as the gas pressure drop increases and keeps nearly the same as the liquid flow rate increases. The results also indicate that the dynamic behavior of droplet formation in dripping mode of capillary flow focusing is mainly dominated by the gas pressure drop, and the capillary flow focusing technique can produce droplets with high throughput even in the dripping regime. Cited as:  Si, T. Dynamic behavior of droplet formation in dripping mode of capillary flow focusing. Capillarity, 2021, 4(3): 45-49, doi: 10.46690/capi.2021.03.01
对毛细管流动聚焦过程中液体滴下进行了实验研究。由于高速气流驱动内部液体共流通过孔板,在滴落状态下,随着气体压力的下降和液体流量的变化,液滴形成的复杂现象。周期滴法可以产生均匀的水滴,非周期滴法可以产生不同直径的卫星和水滴。还得到了共流气流核心处的液滴-液滴聚并现象。在不同的气压降和液体流速下,测量了所得液滴的大小。可以看出,随着气体压降的增大,液滴尺寸有减小的趋势,随着液体流量的增大,液滴尺寸基本保持不变。结果还表明,毛细聚焦滴注模式下的液滴形成动力学行为主要受气体压降的影响,毛细聚焦技术即使在滴注状态下也能产生高通量的液滴。引自:Si, T.毛细聚焦滴模式下液滴形成的动力学行为。毛细管学,2021,4(3):45-49,doi: 10.46690/capi.2021.03.01
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引用次数: 1
Investigation of the dynamics of immiscible displacement of a ganglion in capillaries 毛细血管中神经节不混相位移动力学的研究
Q1 Physics and Astronomy Pub Date : 2021-06-03 DOI: 10.46690/capi.2021.02.02
A. Salama, Jianchao Cai, Jisheng Kou, Shuyu Sun, M. El-Amin, Yi Wang
In this work the problem of displacing a ganglion of a fluid by another immiscible one in capillaries is investigated. A modeling approach is developed to predict the location of the ganglion with time. The model describes two patterns; namely, when the ganglion totally exists inside the tube, and when the advancing interface of the ganglion has broken through the exit of the tube. The model is valid for the case in which the ganglion is wetting as well as when it is nonwetting to the wall of the tube. It also considers the situation in which both the advancing and the receding interfaces assume, generally, different contact angles. For the special case when the displacement process is quasistatic, both the receding and the advancing contact angles may be considered the same. Under these conditions, interfacial tension force plays no role and the ganglion moves as a plug inside the tube with a constant velocity. When the viscosity ratio between the invading fluid and the ganglion is one (i.e., both phases are having the same viscosity) the motion reduces to the Hagen-Poiseuille flow in pipes. Once the advancing interface breaks through the exit of the tube, interfacial tension starts to take part in the displacement process and the ganglion starts to accelerate or decelerate according to the viscosity ratio. When the ganglion is nonwetting, interfacial tension becomes in the direction of the flow and is opposite to the flow otherwise. The model accounts for external forces such as pressure and gravity in addition to capillarity. A computational fluid dynamics analysis of this system is conducted for both types of wettability scenarios and shows very good match with the results of the developed model during both the two modes of flow patterns. This builds confidence in the developed modeling approach. Other cases have also been explored to highlight the effects of other scenarios. Cited as:  Salama, A., Cai, J., Kou, J., Sun, S., EI-Amin, M. F., Wang, Y. Investigation of the dynamics of immiscible displacement of a ganglion in capillaries. Capillarity, 2021, 4(2): 31-44, doi: 10.46690/capi.2021.02.02
在这项工作中,用另一种不混相的神经节取代一种流体在毛细血管中的问题进行了研究。提出了一种预测神经节位置随时间变化的建模方法。该模型描述了两种模式;即神经节完全存在于管内,且神经节前进界面已突破管出口。该模型既适用于神经节湿润的情况,也适用于神经节不湿润管壁的情况。它还考虑了前进界面和后退界面通常具有不同接触角的情况。对于位移过程为准静态的特殊情况,后退接触角和前进接触角可以认为是相同的。在这些条件下,界面张力不起作用,神经节在管内以恒定速度作为塞子运动。当侵入流体与神经节之间的黏度比为1时(即两相黏度相同),运动减少为管道内的hagan - poiseuille流动。一旦前进界面突破管道出口,界面张力开始参与位移过程,神经节根据粘度比开始加速或减速。当神经节处于非润湿状态时,界面张力与流动方向相反,反之则相反。该模型除考虑毛细作用外,还考虑了诸如压力和重力等外力。对两种润湿性情况下的系统进行了计算流体力学分析,结果表明,在两种流动模式下,所建立的模型与计算结果吻合良好。这建立了对开发的建模方法的信心。还探讨了其他案例,以突出其他情景的影响。引用自:Salama, A., Cai, J., Kou, J., Sun, S., EI-Amin, M. F., Wang, Y.毛细血管中神经节不混相位移动力学的研究。毛细管学,2021,4(2):31-44,doi: 10.46690/capi.2021.02.02
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引用次数: 9
Derivations of the Young-Laplace equation 杨-拉普拉斯方程的推导
Q1 Physics and Astronomy Pub Date : 2021-05-22 DOI: 10.46690/CAPI.2021.02.01
L. M. Siqveland, S. Skjaeveland
The classical Young-Laplace equation relates capillary pressure to surface tension and the principal radii of curvature of the interface between two immiscible fluids. In this paper the required properties of space curves and smooth surfaces are described by differential geometry and linear algebra. The equilibrium condition is formulated by a force balance and minimization of surface energy. Cited as:  Siqveland, L. M., Skjaeveland, S. M. Derivations of the Young-Laplace equation. Capillarity, 2021, 4(2): 23-30, doi: 10.46690/capi.2021.02.01
经典的Young-Laplace方程将毛细管压力与表面张力和两种不混相流体界面的主曲率半径联系起来。本文用微分几何和线性代数描述了空间曲线和光滑曲面的必要性质。平衡条件由力平衡和表面能最小化表述。引自:Siqveland, L. M., Skjaeveland, S. M. Young-Laplace方程的推导。毛细管学,2021,4(2):23-30,doi: 10.46690/capi.2021.02.01
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引用次数: 13
Prediction of spontaneous imbibition in fractal porous media based on modified porosity correlation 基于修正孔隙度相关性的分形多孔介质自吸预测
Q1 Physics and Astronomy Pub Date : 2021-03-25 DOI: 10.46690/CAPI.2021.01.02
Yinglin Li, Di Yu, B. Niu
Spontaneous imbibition plays a significant role in different technical applications, and several analytical models have been proposed for predicting the fluid imbibition mass into porous media based on the fractal theory. Herein, these previous models are reconsidered in view of the obvious difference between the effective porosity and the areal porosity of porous media. Firstly, an implicit equation for fractal tortuosity is proposed and a modified correlation for the areal porosity is presented; then, a semi-analytical prediction model for fluid imbibition mass with gravity pressure is derived; finally, comparisons of predictions among several previous models with the present model are carried out. The modeling results show consistency with the experimental data published in the literature. Cited as: Li, Y., Yu, D., Niu, B. Prediction of spontaneous imbibition in fractal porous media based on modified porosity correlation. Capillarity, 2021, 4(1): 13-22, doi: 10.46690/capi.2021.01.02
自发吸积在不同的技术应用中发挥着重要的作用,基于分形理论提出了几种预测流体在多孔介质中的吸积的分析模型。鉴于多孔介质的有效孔隙率与面孔隙率存在明显差异,本文对上述模型进行了重新考虑。首先,提出了分形弯曲度的隐式方程,并提出了面孔隙度的修正关系式;在此基础上,推导了流体吸胀质量随重力压力的半解析预测模型;最后,将几种模型的预测结果与本模型进行了比较。模拟结果与文献中发表的实验数据一致。引用本文:李勇,于东,牛波。基于修正孔隙度相关性的分形多孔介质自吸预测。毛细管学,2021,4(1):13-22,doi: 10.46690/capi.2021.01.02
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引用次数: 7
Dynamic capillary pressure analysis of tight sandstone based on digital rock model 基于数字岩石模型的致密砂岩动毛管压力分析
Q1 Physics and Astronomy Pub Date : 2020-06-14 DOI: 10.46690/capi.2020.02.02
Yixin Cao, Mingming Tang, Qian Zhang, Jiafan Tang, Shuangfang Lu
In recent studies, dynamic capillary pressure has shown significant impacts on the flow behaviors in porous media under transient flow condition. However, the effect of dynamic capillary pressure effect on tight sandstone is still not very clear. Since lattice Boltzmann method (LBM) is a very promising and widely used method in analyzing flow behaviors, therefore, a two-phase D3Q27 LBM model is adopted in this paper to simulate the flow behaviors and analyze the dynamic capillary pressure effect in tight sandstone. Moreover, a new pore segmentation method for tight sandstone base on U-net deep learning model is implemented in this study to improve the pore boundary qualities of pore space, which is crucial for two-phase LBM simulation of tight sandstone. A total of 3800 3D sub-volume data sets extracted from computed tomography data of 19 tight sandstone samples are selected as ground truth data to train the network and segment the pore space afterward. The simulation results based on the segmented digital rock model, show that nonwetting phase fluid prefer the path with lower dynamic capillary pressure in the seepage process before breaking through the porous model. Furthermore, the increase of injection rate causes the saturation changes more quickly, injection rate also shows apparent positive correlation relationship with capillary pressure, which implies that dynamic capillary pressure effect also exists in tight sandstone, and LBM based two-phase flow simulation could be used to quantitatively analyze such effect in tight sandstone. Cited as : Cao, Y., Tang, M., Zhang, Q., Tang, J., Lu, S. Dynamic capillary pressure analysis of tight sandstone based on digital rock model. Capillarity, 2020, 3(2): 28-35, doi: 10.46690/capi.2020.02.02.
近年来的研究表明,在瞬态流动条件下,动毛管压力对多孔介质的流动行为有重要影响。然而,动毛管压力效应对致密砂岩的影响还不是很清楚。由于晶格玻尔兹曼方法(lattice Boltzmann method, LBM)是一种非常有前途和广泛应用的流动特性分析方法,因此,本文采用两相D3Q27玻尔兹曼模型对致密砂岩的流动特性进行模拟,分析动态毛管压力效应。此外,本文还提出了一种基于U-net深度学习模型的致密砂岩孔隙分割新方法,以改善孔隙空间的孔隙边界质量,这对致密砂岩两相LBM模拟至关重要。选取19个致密砂岩样品的ct数据提取的3800个三维子体数据集作为地面真值数据,进行网络训练和孔隙空间分割。基于分段数字岩石模型的模拟结果表明,非润湿相流体在渗流过程中倾向于沿动毛管压力较低的路径突破多孔模型。注入速度的增加使饱和度变化更快,注入速度与毛管压力也呈现出明显的正相关关系,说明在致密砂岩中也存在动毛管压力效应,基于LBM的两相流模拟可以定量分析这种效应在致密砂岩中的作用。引用本文:曹勇,唐明,张强,唐军,陆生。基于数字岩石模型的致密砂岩动态毛管压力分析。毛细管学,2020,3(2):28-35,doi: 10.46690/capi.2020.02.02。
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引用次数: 27
A comparative study of ion diffusion during water imbibition in shale, sandstone and volcanic rock 页岩、砂岩和火山岩吸水过程中离子扩散的对比研究
Q1 Physics and Astronomy Pub Date : 2020-06-01 DOI: 10.46690/capi.2020.02.01
Liu Yang, Chenjiu Chen, Yifan Liu, Yuanhan Zheng
The recovered fracturing fluid is generally high in salinity (close to 200 kppm), which is related to the diffusion of salt ions from shale reservoir to the fracturing fluid. However, it is not clear about the diffusion capacity of salt ions in different types. In this paper, the shale, tight volcanic and sandstone are selected as comparative study and a series of tests are carried out for the porosity, permeability and mineral composition. The results show that the shale immersing in fracturing fluid will cause ions dissolution and diffusion, which will increase the salinity of the fracturing fluid. The solution salinity increases rapidly in the early stage and gradually slows down in the later stage. The salinity of the fracturing fluid has a linear relationship with the square root of time, so the slope of the curve can be used as a characteristic parameter to evaluate the ion diffusion rate. The process of dissolution and diffusion of salt ions will induce the expansion of micro-cracks, increasing the contact area between the fracturing fluid and shale and enhancing the solution salinity. The ion diffusion rate is positively related with the content of clay minerals and carbonate. The soluble ions include mainly SO 4 2− , Ca 2+ , Na + and K + . The Na + /Cl − ratio is closely related to the content of clay minerals and carbonate minerals. It has a positive correlation with content of illite and chlorite, and a negative correlation with carbonate minerals, suggesting NaCl source from illite and chlorite. This study is significant for understanding the salinity characteristics of recovered fracturing fluid and evaluating the fracture network shape. Cited as : Yang, L., Chen, C., Liu, Y., Zheng, Y. A comparative study of ion diffusion during water imbibition in shale, sandstone and volcanic rock. Capillarity, 2020, 3(2): 16-27, doi: 10.46690/capi.2020.02.01.
采出的压裂液含盐量普遍较高(接近200 kppm),这与页岩储层盐离子向压裂液扩散有关。然而,不同类型盐离子的扩散能力尚不清楚。本文选取页岩、致密火山岩和砂岩进行对比研究,对其孔隙度、渗透率和矿物组成进行了一系列测试。结果表明,页岩浸没在压裂液中会引起离子的溶解和扩散,使压裂液的矿化度升高。溶液盐度在早期迅速升高,在后期逐渐降低。压裂液的矿化度与时间的平方根呈线性关系,因此曲线的斜率可以作为评价离子扩散速率的特征参数。盐离子的溶解和扩散过程会诱发微裂缝的扩展,增加压裂液与页岩的接触面积,提高溶液盐度。离子扩散速率与黏土矿物和碳酸盐含量呈正相关。可溶性离子主要有so4.2−、ca2 +、Na +和K +。Na + /Cl−比值与黏土矿物和碳酸盐矿物含量密切相关。与伊利石和绿泥石含量呈正相关,与碳酸盐矿物呈负相关,表明NaCl来源为伊利石和绿泥石。该研究对了解压裂液的矿化度特征和评价裂缝网络形态具有重要意义。引用本文:杨磊,陈超,刘勇,郑勇。页岩、砂岩和火山岩吸水过程中离子扩散的对比研究。毛细管学,2020,3(2):16-27,doi: 10.46690/capi.2020.02.01。
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引用次数: 10
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Capillarity
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