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Computational and Experimental Methods in Multiphase and Complex Flow X最新文献

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BED EXPANSION CHARACTERISTICS IN MICROJET AND VIBRATION ASSISTED FLUIDIZATION OF TIO2 NANOPARTICLES 微射流床层膨胀特性及振动辅助流化tio2纳米颗粒
Keju An, J. Andino
A microjet and vibration assisted (MVA) fluidized bed was designed and tested to improve the fluidization quality of nanosized particles. Previous work relied on the addition of alcohol support in order to minimize electrostatic forces, thereby improving fluidization. The MVA method increased the fluidized bed height smoothly without the need for alcohol support. Thus, the MVA system is more versatile for use where the addition of a chemical may impact the process (e.g. environmental remediation). Commercial, nanosized TiO2 particles (P25 from Evonik Degussa) were analyzed in the MVA system. It was operated at its resonance frequency (50Hz), under different vibrational amplitude levels. The microjet was operated using a flow of nitrogen at 135.8, 170.3, 204.7, 239.2, 273.7 and 308.2 kPa resulting in a downward stream through the micronozzle (500 μm). The additional vibrational support enabled nanoparticle fluidization under lower inlet pressure and velocity conditions compared to systems where only a microjet was used. In the MVA system, the micronozzle velocity coupled with a vibrational intensity of 1.6 showed 5 times higher fluidized bed height compared to the packed bed. Optimal operating/processing conditions of the MVA system are suggested based on the experimental results. The results presented provide valuable parameters to develop computer simulations of large commercial and pilot scale fluidized bed systems.
为提高纳米颗粒的流化质量,设计并试验了一种微射流振动辅助流化床。以前的工作依赖于添加醇载体,以尽量减少静电力,从而改善流化。MVA法在不需要酒精支撑的情况下平稳地提高了流化床高度。因此,MVA系统在添加化学物质可能影响过程(例如环境修复)的情况下使用更为通用。在MVA系统中分析了商用纳米TiO2颗粒(来自赢创德固赛的P25)。在不同的振动幅值水平下,以其共振频率(50Hz)运行。在135.8、170.3、204.7、239.2、273.7和308.2 kPa的氮气流量下,微射流向下流过500 μm的微喷嘴。与仅使用微射流的系统相比,额外的振动支撑使纳米颗粒在更低的进口压力和速度条件下流化。在MVA系统中,微喷嘴速度耦合振动强度为1.6时,流化床高度比填充床高5倍。根据实验结果,提出了MVA系统的最佳运行/处理条件。所提出的结果为大型商业和中试规模流化床系统的计算机模拟提供了有价值的参数。
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Computational and Experimental Methods in Multiphase and Complex Flow X
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