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Numerical study of a crossflow heat exchanger to investigate thermal performance using nanofluids 利用纳米流体对横流换热器热性能进行数值研究
Pub Date : 2019-07-18 DOI: 10.1063/1.5115927
Jaed Al Nahian, P. Pandit, M. Mamun
In this study, conjugate heat transfer between solids and fluids has been analyzed for a cross flow rectangular shaped microchannel heat exchanger. Three different nanofluids have been used such as CuO-water, Al2O3-water and Al2O3-ethylene glycol to investigate the effect of changing nanoparticles volume fraction as well as, effect of changing the base fluid at constant temperature. Volume fraction has been varied from 0.5% to 4%. These nanofluids have been widely used in compact heat exchangers, micro reactors, automotive radiators etc. for their exhibition of larger thermos-physical properties than conventional fluids due to presence of nanosized particles in them which enhance heat transfer. It has been observed that changing the base fluid has had a much significant effect than changing the nanoparticle. Heat transfer coefficient, pressure drop and pumping power requirement have been investigated in terms of varying nanoparticles volume fraction and Reynolds number. In addition, different characteristics such as isotherms, channel wall temperature have been graphically shown.In this study, conjugate heat transfer between solids and fluids has been analyzed for a cross flow rectangular shaped microchannel heat exchanger. Three different nanofluids have been used such as CuO-water, Al2O3-water and Al2O3-ethylene glycol to investigate the effect of changing nanoparticles volume fraction as well as, effect of changing the base fluid at constant temperature. Volume fraction has been varied from 0.5% to 4%. These nanofluids have been widely used in compact heat exchangers, micro reactors, automotive radiators etc. for their exhibition of larger thermos-physical properties than conventional fluids due to presence of nanosized particles in them which enhance heat transfer. It has been observed that changing the base fluid has had a much significant effect than changing the nanoparticle. Heat transfer coefficient, pressure drop and pumping power requirement have been investigated in terms of varying nanoparticles volume fraction and Reynolds number. In addition, different characterist...
本文对横流矩形微通道换热器的固液耦合传热进行了分析。采用cuo -水、al2o3 -水和al2o3 -乙二醇三种不同的纳米流体,考察了在恒温条件下改变纳米颗粒体积分数的影响以及改变基液的影响。体积分数从0.5%到4%不等。这些纳米流体被广泛应用于紧凑的热交换器、微反应器、汽车散热器等,因为它们比传统流体具有更大的热物理性质,因为它们中存在纳米级颗粒,可以增强传热。已经观察到,改变基液比改变纳米颗粒有更显著的效果。研究了纳米颗粒体积分数和雷诺数变化对传热系数、压降和泵送功率的影响。此外,还用图形表示了等温线、通道壁温度等不同特性。本文对横流矩形微通道换热器的固液耦合传热进行了分析。采用cuo -水、al2o3 -水和al2o3 -乙二醇三种不同的纳米流体,考察了在恒温条件下改变纳米颗粒体积分数的影响以及改变基液的影响。体积分数从0.5%到4%不等。这些纳米流体被广泛应用于紧凑的热交换器、微反应器、汽车散热器等,因为它们比传统流体具有更大的热物理性质,因为它们中存在纳米级颗粒,可以增强传热。已经观察到,改变基液比改变纳米颗粒有更显著的效果。研究了纳米颗粒体积分数和雷诺数变化对传热系数、压降和泵送功率的影响。此外,不同的特点……
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引用次数: 1
Analysis of wind pressure coefficients on CTBUH standard high-rise buildings in CFD simulations CTBUH标准高层建筑风压系数CFD模拟分析
Pub Date : 2019-07-18 DOI: 10.1063/1.5115953
Tanvir Chowdhury, Quamrul Islam
At present with the fast growth rate of population constructing high-rise buildings has been a common trend for many urban communities, so it is important to analyze wind pressure around and over these high-rise structures. CFD analysis is an effective way to understand this, in which CTBUH (Council on Tall Buildings and Urban Habitat) standard high-rise building has been a recognized model to validate and calibrate high-rise building models. As it may, less work has been directed to study of airflow around CTBUH standard high-rise building to geometric and computational parameters in CFD analysis. In this investigation is therefore intended to fill this gap by analyzing effects of various parameters like turbulence model, approaching-flow speed and grid type on wind pressure coefficients over CTBUH structures. Wind pressure coefficients around CTBUH models subjected to three wind directions were numerically analyzed for validating the correctness and effectiveness of numerical model. In conclusion acquired results can help structural engineers to choose empirical geometric and computational parameters in anticipating wind pressure distribution against high-rise buildings.At present with the fast growth rate of population constructing high-rise buildings has been a common trend for many urban communities, so it is important to analyze wind pressure around and over these high-rise structures. CFD analysis is an effective way to understand this, in which CTBUH (Council on Tall Buildings and Urban Habitat) standard high-rise building has been a recognized model to validate and calibrate high-rise building models. As it may, less work has been directed to study of airflow around CTBUH standard high-rise building to geometric and computational parameters in CFD analysis. In this investigation is therefore intended to fill this gap by analyzing effects of various parameters like turbulence model, approaching-flow speed and grid type on wind pressure coefficients over CTBUH structures. Wind pressure coefficients around CTBUH models subjected to three wind directions were numerically analyzed for validating the correctness and effectiveness of numerical model. In conclusion acquir...
在人口快速增长的今天,建设高层建筑已成为许多城市社区的共同趋势,因此对高层建筑周围和上方的风压进行分析具有重要意义。CFD分析是理解这一点的有效途径,其中CTBUH (Council on Tall Buildings and Urban Habitat)标准高层建筑已成为验证和校准高层建筑模型的公认模型。尽管如此,针对CTBUH标准高层建筑周围气流的CFD分析中几何参数和计算参数的研究较少。因此,本研究旨在通过分析湍流模型、接近流速度和网格类型等各种参数对CTBUH结构风压系数的影响来填补这一空白。通过对三种风向下CTBUH模型周围风压系数的数值分析,验证了数值模型的正确性和有效性。所得结果可以帮助结构工程师在预测高层建筑风压分布时选择经验几何参数和计算参数。在人口快速增长的今天,建设高层建筑已成为许多城市社区的共同趋势,因此对高层建筑周围和上方的风压进行分析具有重要意义。CFD分析是理解这一点的有效途径,其中CTBUH (Council on Tall Buildings and Urban Habitat)标准高层建筑已成为验证和校准高层建筑模型的公认模型。尽管如此,针对CTBUH标准高层建筑周围气流的CFD分析中几何参数和计算参数的研究较少。因此,本研究旨在通过分析湍流模型、接近流速度和网格类型等各种参数对CTBUH结构风压系数的影响来填补这一空白。通过对三种风向下CTBUH模型周围风压系数的数值分析,验证了数值模型的正确性和有效性。总之,获得……
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引用次数: 1
Non-Newtonian shear thinning effect on natural convection flow over an isothermal elliptical cylinder 非牛顿剪切减薄对等温椭圆圆柱自然对流流动的影响
Pub Date : 2019-07-18 DOI: 10.1063/1.5115860
P. Nag, M. Molla, Md.Anwar Hossain
In this paper, laminar natural convection flow of Newtonian and non-Newtonian (shear thinning case only) fluid surround an isothermal horizontal cylinder of elliptic cross section has been studied numerically. To characterize the non-Newtonian fluid, a modified power-law viscosity model has been employed. The boundary layer equations governing the flow are transformed into a non-dimensional form and the resulting equations are reduced to a convenient form which are solved numerically by an efficient implicit finite difference method. Numerical results are presented for two significant physical quantity such as the local skin friction coefficients and the rate of surface heat transfer (i.e. the local Nusselt number) as a function of the eccentric angle of an elliptical configurations with different aspect ratio and for different orientation such as blunt and slender. The local skin friction is found to be higher for Newtonian fluid than that of the shear thinning fluid. Furthermore, the total heat transfer rate becomes higher for elliptical cylinder with slender orientation than that of the blunt orientation in the fluids of interest.In this paper, laminar natural convection flow of Newtonian and non-Newtonian (shear thinning case only) fluid surround an isothermal horizontal cylinder of elliptic cross section has been studied numerically. To characterize the non-Newtonian fluid, a modified power-law viscosity model has been employed. The boundary layer equations governing the flow are transformed into a non-dimensional form and the resulting equations are reduced to a convenient form which are solved numerically by an efficient implicit finite difference method. Numerical results are presented for two significant physical quantity such as the local skin friction coefficients and the rate of surface heat transfer (i.e. the local Nusselt number) as a function of the eccentric angle of an elliptical configurations with different aspect ratio and for different orientation such as blunt and slender. The local skin friction is found to be higher for Newtonian fluid than that of the shear thinning fluid. Furthermore, the total heat transfer...
本文数值研究了牛顿流体和非牛顿流体(仅限剪切变薄情况)围绕等温椭圆横截面水平圆柱体的层流自然对流流动。为了描述非牛顿流体,采用了修正的幂律粘度模型。将控制流动的边界层方程转化为无量纲形式,并将得到的方程简化为方便的形式,用有效的隐式有限差分法进行数值求解。给出了两个重要物理量,如局部表面摩擦系数和表面换热率(即局部努塞尔数)作为不同长径比椭圆构型偏心角和不同取向(如钝型和细长型)的函数的数值结果。发现牛顿流体的局部表面摩擦比剪切稀化流体的高。此外,在所研究的流体中,细长取向的椭圆圆柱体的总换热率比钝取向的总换热率高。本文数值研究了牛顿流体和非牛顿流体(仅限剪切变薄情况)围绕等温椭圆横截面水平圆柱体的层流自然对流流动。为了描述非牛顿流体,采用了修正的幂律粘度模型。将控制流动的边界层方程转化为无量纲形式,并将得到的方程简化为方便的形式,用有效的隐式有限差分法进行数值求解。给出了两个重要物理量,如局部表面摩擦系数和表面换热率(即局部努塞尔数)作为不同长径比椭圆构型偏心角和不同取向(如钝型和细长型)的函数的数值结果。发现牛顿流体的局部表面摩擦比剪切稀化流体的高。此外,总传热…
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引用次数: 3
Process analysis and gasification of rice husk by using downdraft fixed bed gasifier 稻壳下吸式固定床气化工艺分析与研究
Pub Date : 2019-07-18 DOI: 10.1063/1.5115951
M. E. Hoque, F. Rashid, S. Aziz, M. Rahman, P. Das
The use of fossil fuels has great impact on environment and energy security problems. Besides, the rising cost of fuel oil compelled the industry to search for alternative fuels, and biomass in general and rice husks in particular are considered a suitable candidate. Bio energy has significant potential contribution for sustainable energy systems, especially when converted to modern energy carriers such as electricity, gaseous or liquid fuels. Rice is cultivated in more than 75 countries in the world. The rice husk is the outer cover of the rice and on average it accounts for 20% of the paddy produced, on weight basis. The worldwide annual husk is about 80 million tons with an annual energy potential of 1.2∼109 GJ corresponding to a heating value of 15 MJ/kg. Maximum rice husk produced by milling process of rice mills in Bangladesh usually burned in the mill boilers to produce process heat for parboiling of paddy rice and excess husk are sold to the market as fuel for cooking purposes and a considerable portion is misused. Therefore, syngas from rice husk can be produced as an auspicious source of energy. It can be used to generate heat and power like natural gas, synthesize other chemicals and liquid fuels, or produce H2. One of the promising approaches for syngas production from biomass is downdraft fixed bed gasification among the several approaches till developed. Optimization of operating conditions (combustion zone temperature, reaction zone temperature, intake air temperature, humidity of intake air and air flow rate) can give a satisfactory result for the quality syngas production. In this paper rice husk was used as potential biomass feed stocks. The moisture content of the feed material is less than 10% on weight basis and consumption rate of rice husk is 3.62 kg/h. Temperature inside the reaction zone (970∼994) K, primary air flow rate 2.7 m3/h, humidity of outside air (45∼50%) and exit temperature of the producer gas (140∼160)°C were measured. This paper gives an optimistic operating condition for quality syngas production.
化石燃料的使用对环境和能源安全问题产生了巨大的影响。此外,燃料油成本的上升迫使该行业寻找替代燃料,而一般的生物质,特别是稻壳被认为是一个合适的候选者。生物能源对可持续能源系统具有重大的潜在贡献,特别是在转化为电力、气体或液体燃料等现代能源载体时。世界上有超过75个国家种植水稻。稻壳是水稻的外层,按重量计算,它平均占水稻产量的20%。全世界每年的稻壳约为8000万吨,年能量潜力为1.2 ~ 109 GJ,相当于15 MJ/kg的热值。孟加拉国碾米厂碾磨过程产生的最大稻壳通常在碾米厂锅炉中燃烧,以产生用于大米煮熟的过程热量,多余的稻壳作为烹饪燃料出售给市场,其中相当一部分被滥用。因此,从稻壳中提取合成气可以作为一种吉祥的能源。它可以像天然气一样用来产生热量和电力,合成其他化学物质和液体燃料,或者产生氢气。在目前尚未开发的几种方法中,有一种很有前途的生物质合成气生产方法是下吸固定床气化。优化操作条件(燃烧区温度、反应区温度、进气温度、进气湿度和进气流量)可以获得满意的效果,从而保证优质合成气的生产。本文将稻壳作为潜在的生物质原料加以利用。饲料含水率按重量计小于10%,稻壳消耗率为3.62 kg/h。测量了反应区内温度(970 ~ 994)K,一次风流量2.7 m3/h,外部空气湿度(45 ~ 50%)和产气出口温度(140 ~ 160)℃。本文给出了高质量合成气生产的乐观运行条件。
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引用次数: 3
A simplified one-equation elliptic-relaxation model 一个简化的单方程椭圆松弛模型
Pub Date : 2019-07-18 DOI: 10.1063/1.5115888
Xiaoqing Tian, Mizanur Rahman, H. Pan, A. Islam
A simplified version of a one-equation R = Cμk2/ϵ turbulence model with elliptic relaxation, formulated by Elkhoury [4] containing explicitly constant coefficients, is proposed that accounts for the distinct effects of low-Reynolds number (LRN) and near-wall turbulence. In the simplified model, coefficients and functions are constructed such as to preserve the anisotropic characteristics of turbulence encountered in nonequilibrium flows. The constant-dependent sensitivity of characteristic length scale associated with the elliptic relaxation function is reduced to an extent. Unlike the Elkhoury model, it requires the elliptic equation for the elliptic relaxation parameter fR with a source term 1.0 (one) to be solved in conjunction with the R-equation model. A near-wall damping function is introduced to relax the viscous length-scale coefficient of the elliptic relaxation model. This incentive approach stems from the combination of wall-viscous (LRN) and wall-blocking (nonlocal) effects. The simplified mod...
Elkhoury[4]提出了包含显式常系数的单方程R = Cμk2/ λ椭圆松弛湍流模型的简化版本,该模型考虑了低雷诺数(LRN)和近壁湍流的不同影响。在简化模型中,通过构造系数和函数来保持非平衡流动中湍流的各向异性特征。在一定程度上降低了与椭圆松弛函数相关的特征长度尺度的常相关灵敏度。与Elkhoury模型不同的是,它需要结合r方程模型求解源项为1.0(1)的椭圆松弛参数fR的椭圆方程。引入近壁阻尼函数对椭圆松弛模型的粘滞长度尺度系数进行松弛。这种激励方法源于壁面粘性(LRN)和壁面阻塞(非局部)效应的结合。简化的mod…
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引用次数: 3
Towards an improved pyrolysis system: Integrating solar energy based pre-heating system 改进热解系统:集成太阳能预热系统
Pub Date : 2019-07-18 DOI: 10.1063/1.5115931
Md. Washim Akram, T. Mondal, Md. Touhidur Rahman, A. Rahim, R. Mursalin
Thermo-chemical conversion process such as gasification and pyrolysis has proven as a potential option to utilize renewable energy. In conventional pyrolysis process, feed material in the reactor i...
热化学转化过程,如气化和热解,已被证明是利用可再生能源的潜在选择。在传统的热解过程中,进料在反应器中是不可逆的。
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引用次数: 1
Heat transfer enhancement in shell and tube heat exchanger by using Al2O3/water and TiO2/water nanofluid Al2O3/水纳米流体和TiO2/水纳米流体强化管壳式换热器的换热性能
Pub Date : 2019-07-18 DOI: 10.1063/1.5115925
Md. Rahmat Ullah, Tanvir Muhammad Ishtiaq, M. Mamun
Nanofluids, potential heat transfer fluid with enhanced thermophysical properties are recently being experimented in different heat transfer device for better performance. Heat transfer characteristics of γ-Al2O3/water and TiO2/water nanofluids has been numerically investigated in a shell and tube heat exchanger under turbulent flow condition. The effects of Reynolds number, volume concentration of suspended nanoparticles, and particle type on the heat characteristics has been investigated. Based on the results, addition of naoparticles to the base fluid causes the significant enhancement of heat transfer characteristics. For γ-Al2O3/water maximum improvement in convective heat transfer coefficient is 41.8% while TiO2/water shows maximum 37% increment. The introduction of nanoparticle incorporates more viscosity than base fluid which eventually increases the pressure drop, but the drop has not been found to be considerably high.Nanofluids, potential heat transfer fluid with enhanced thermophysical properties are recently being experimented in different heat transfer device for better performance. Heat transfer characteristics of γ-Al2O3/water and TiO2/water nanofluids has been numerically investigated in a shell and tube heat exchanger under turbulent flow condition. The effects of Reynolds number, volume concentration of suspended nanoparticles, and particle type on the heat characteristics has been investigated. Based on the results, addition of naoparticles to the base fluid causes the significant enhancement of heat transfer characteristics. For γ-Al2O3/water maximum improvement in convective heat transfer coefficient is 41.8% while TiO2/water shows maximum 37% increment. The introduction of nanoparticle incorporates more viscosity than base fluid which eventually increases the pressure drop, but the drop has not been found to be considerably high.
纳米流体是一种具有增强热物理特性的潜在传热流体,近年来在不同的传热装置中进行了实验,以获得更好的传热性能。对湍流条件下γ-Al2O3/水和TiO2/水纳米流体在管壳式换热器中的换热特性进行了数值研究。研究了悬浮纳米颗粒的雷诺数、体积浓度和颗粒类型对热特性的影响。结果表明,在基液中加入纳米颗粒可以显著增强传热特性。γ-Al2O3/water的对流换热系数最大提高了41.8%,TiO2/water的对流换热系数最大提高了37%。纳米颗粒的引入比基液具有更高的粘度,这最终会增加压降,但目前还没有发现压降相当高。纳米流体是一种具有增强热物理特性的潜在传热流体,近年来在不同的传热装置中进行了实验,以获得更好的传热性能。对湍流条件下γ-Al2O3/水和TiO2/水纳米流体在管壳式换热器中的换热特性进行了数值研究。研究了悬浮纳米颗粒的雷诺数、体积浓度和颗粒类型对热特性的影响。结果表明,在基液中加入纳米颗粒可以显著增强传热特性。γ-Al2O3/water的对流换热系数最大提高了41.8%,TiO2/water的对流换热系数最大提高了37%。纳米颗粒的引入比基液具有更高的粘度,这最终会增加压降,但目前还没有发现压降相当高。
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引用次数: 9
Temperature dependent mechanical properties of inter-metallic compounds in nano-solder joints 纳米焊点金属间化合物的温度相关力学性能
Pub Date : 2019-07-18 DOI: 10.1063/1.5115965
M. Billah, R. I. Siddiquee, M. Motalab
SnAgCu (SAC) alloys has become the topic of interest in recent days, as it shows great potential to be alternate to lead-based solders, the use of which is being discontinued for environmental issues. Intermetallic compounds (IMC) form in the solder joints which reduces the strength and other properties thus reducing the reliability of microprocessor components. To investigate this behavior, intermetallic compounds were modeled at nanoscale. Properties of three intermetallic compounds were investigated which are Ag3Sn, Cu3Sn and Cu6Sn5. The variation of mechanical properties the ultimate tensile strength, yield strength and Young’s modulus with the change of temperature were thoroughly observed. Also, the coefficient of thermal expansion was determined for these three different compounds. The mechanical properties of these three compounds were compared to find out which of these poses the greater threat to the solder joints. All the simulations were done by molecular dynamics software LAMMPS (Large-scale Atomic/Molecular Massively Parallel Simulator) and the structures of the IMCs were built by VNL (Virtual NanoLab). Molecular dynamics approach was used to model the interaction between molecules under various temperatures.SnAgCu (SAC) alloys has become the topic of interest in recent days, as it shows great potential to be alternate to lead-based solders, the use of which is being discontinued for environmental issues. Intermetallic compounds (IMC) form in the solder joints which reduces the strength and other properties thus reducing the reliability of microprocessor components. To investigate this behavior, intermetallic compounds were modeled at nanoscale. Properties of three intermetallic compounds were investigated which are Ag3Sn, Cu3Sn and Cu6Sn5. The variation of mechanical properties the ultimate tensile strength, yield strength and Young’s modulus with the change of temperature were thoroughly observed. Also, the coefficient of thermal expansion was determined for these three different compounds. The mechanical properties of these three compounds were compared to find out which of these poses the greater threat to the solder joints. All the simulations were done by molecular dynamics software LAMMPS (Large-scale ...
近年来,SnAgCu (SAC)合金已成为人们感兴趣的话题,因为它显示出替代铅基焊料的巨大潜力,铅基焊料的使用因环境问题而被停止使用。金属间化合物(IMC)在焊点中形成,降低了强度和其他性能,从而降低了微处理器组件的可靠性。为了研究这种行为,在纳米尺度上对金属间化合物进行了建模。研究了Ag3Sn、Cu3Sn和Cu6Sn5三种金属间化合物的性质。深入观察了材料力学性能、极限抗拉强度、屈服强度和杨氏模量随温度变化的变化规律。同时测定了这三种不同化合物的热膨胀系数。比较了这三种化合物的力学性能,找出哪一种对焊点构成更大的威胁。所有模拟均采用分子动力学软件LAMMPS (Large-scale Atomic/ molecular Massively Parallel Simulator)完成,IMCs的结构由VNL (Virtual NanoLab)构建。采用分子动力学方法模拟了不同温度下分子间的相互作用。近年来,SnAgCu (SAC)合金已成为人们感兴趣的话题,因为它显示出替代铅基焊料的巨大潜力,铅基焊料的使用因环境问题而被停止使用。金属间化合物(IMC)在焊点中形成,降低了强度和其他性能,从而降低了微处理器组件的可靠性。为了研究这种行为,在纳米尺度上对金属间化合物进行了建模。研究了Ag3Sn、Cu3Sn和Cu6Sn5三种金属间化合物的性质。深入观察了材料力学性能、极限抗拉强度、屈服强度和杨氏模量随温度变化的变化规律。同时测定了这三种不同化合物的热膨胀系数。比较了这三种化合物的力学性能,找出哪一种对焊点构成更大的威胁。所有模拟均由分子动力学软件LAMMPS (Large-scale…
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引用次数: 6
Optimization of sintering profile to achieve highly toughened alumina based ceramic 优化烧结型态,实现高增韧氧化铝基陶瓷
Pub Date : 2019-07-18 DOI: 10.1063/1.5115964
U. Salma, M. Hasanuzzaman
Alumina (Al2O3) based ceramics are widely used for making machine parts, high-temperature components, wear-resistant material and biological ceramic due to their high hardness, strength, wear-resistance, and chemical and thermal stability. However, low fracture toughness (KIC∼3.0 MPa.m1/2) inhibit its usage in other potential applications where high toughness is a pre-requisite (e.g. ceramic engine). In an attempt to improve the strength, particularly the fracture toughness, two step sintering process was used. Sintering temperature was optimized based on the results obtained from dilatometer and DSC-TG analysis. X-ray fluorescence (XRF) was used to make compositional analysis of as received raw powders and X-ray Diffraction (XRD) was used to analysis the phase purity and crystallinity for both powder and sintered samples. Microstructure was investigated by using SEM. Hardness and fracture toughness was measured and its correlation with microstructure was investigated. Density was measured by Archimedes method and crystalline density from XRD. Microhardness diamond indenter was used and the diagonal length of indent and the crack lengths were measured by SEM to calculate the Vickers hardness values and fracture toughness, respectively. The maximum fracture toughness was obtained 4.03 MPa.m1/2 for Al2O3 ceramic and the hardness value was 15.97 GPa. Density was found 99.6% of the relative density of Alumina at optimum sintering cycle and the grain size was found 0.38 µm. Thermal expansion coefficient was measured by dilatometer and the calculated value was 7.9×10-6 K-1. The physical properties of the Alumina were good enough and comparable to withstand high temperature applications.Alumina (Al2O3) based ceramics are widely used for making machine parts, high-temperature components, wear-resistant material and biological ceramic due to their high hardness, strength, wear-resistance, and chemical and thermal stability. However, low fracture toughness (KIC∼3.0 MPa.m1/2) inhibit its usage in other potential applications where high toughness is a pre-requisite (e.g. ceramic engine). In an attempt to improve the strength, particularly the fracture toughness, two step sintering process was used. Sintering temperature was optimized based on the results obtained from dilatometer and DSC-TG analysis. X-ray fluorescence (XRF) was used to make compositional analysis of as received raw powders and X-ray Diffraction (XRD) was used to analysis the phase purity and crystallinity for both powder and sintered samples. Microstructure was investigated by using SEM. Hardness and fracture toughness was measured and its correlation with microstructure was investigated. Density was measured by Archimedes m...
氧化铝(Al2O3)基陶瓷由于具有较高的硬度、强度、耐磨性以及化学和热稳定性,被广泛用于制造机械零件、高温部件、耐磨材料和生物陶瓷。然而,低断裂韧性(KIC ~ 3.0 MPa.m1/2)抑制了其在其他潜在应用中的使用,这些应用需要高韧性作为先决条件(例如陶瓷发动机)。为了提高材料的强度,特别是断裂韧性,采用了两步烧结工艺。根据膨胀仪和DSC-TG分析结果对烧结温度进行了优化。用x射线荧光(XRF)对接收的原料粉末进行成分分析,用x射线衍射(XRD)分析粉末和烧结样品的相纯度和结晶度。利用扫描电镜对其微观结构进行了研究。测定了硬度和断裂韧性,并研究了其与显微组织的关系。用阿基米德法测定密度,用XRD测定结晶密度。采用显微硬度金刚石压头,通过扫描电镜测量压头的对角线长度和裂纹长度,分别计算试样的维氏硬度值和断裂韧性。最大断裂韧性为4.03 MPa。Al2O3陶瓷为m1/2,硬度值为15.97 GPa。在最佳烧结循环下,氧化铝的相对密度为99.6%,晶粒尺寸为0.38µm。热膨胀系数用膨胀仪测量,计算值为7.9×10-6 K-1。氧化铝的物理性能足够好,可以承受高温应用。氧化铝(Al2O3)基陶瓷由于具有较高的硬度、强度、耐磨性以及化学和热稳定性,被广泛用于制造机械零件、高温部件、耐磨材料和生物陶瓷。然而,低断裂韧性(KIC ~ 3.0 MPa.m1/2)抑制了其在其他潜在应用中的使用,这些应用需要高韧性作为先决条件(例如陶瓷发动机)。为了提高材料的强度,特别是断裂韧性,采用了两步烧结工艺。根据膨胀仪和DSC-TG分析结果对烧结温度进行了优化。用x射线荧光(XRF)对接收的原料粉末进行成分分析,用x射线衍射(XRD)分析粉末和烧结样品的相纯度和结晶度。利用扫描电镜对其微观结构进行了研究。测定了硬度和断裂韧性,并研究了其与显微组织的关系。密度是用阿基米德测量的。
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引用次数: 1
Investigation of ferroelastic mechanical behavior of lanthanum ferrite, LaFeO3 铁酸镧LaFeO3的铁弹性力学行为研究
Pub Date : 2019-07-18 DOI: 10.1063/1.5115956
M. Islam, W. Araki, Y. Arai
The present study investigates the deformation behavior of lanthanum ferrite, LaFeO3 under uniaxial compression. Ferroelastic domains were observed in samples at high temperature etching which was confirmed by scanning electron microscopic observation. XRD patterns of all samples showed characteristics reflection with orthorhombic crystal structure. Uniaxial compression tests were carried out at temperature of 93K, 193K, 293K, 393K, and 553K, at a constant loading rate of 1.0 MPa/s. All samples exhibited non-elastic stress-strain behavior during loading- unloading cycles owing to ferroelasticity. The slope of the stress-strain curves increased with increasing the temperature as well as ferroelastic parameters, initial modulus and loading modulus were increased due to ferroelastic domain switching.
本文研究了铁素体镧LaFeO3在单轴压缩下的变形行为。在高温刻蚀过程中,样品中存在铁弹性畴,并通过扫描电镜观察得到了证实。所有样品的XRD谱图均显示出具有正交晶型结构的特征反射。分别在93K、193K、293K、393K和553K温度下进行单轴压缩试验,加载速率为1.0 MPa/s。由于铁弹性的存在,所有样品在加载-卸载过程中均表现出非弹性应力-应变行为。应力应变曲线的斜率随温度和铁弹性参数的增加而增大,初始模量和加载模量因铁弹性畴切换而增大。
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8TH BSME INTERNATIONAL CONFERENCE ON THERMAL ENGINEERING
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