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The Structural Examination of Fe/(Cu/Nb)/MgB2 Multifilament Wires During Cold Forming Process 铁/(铜/铌)/MgB2 多丝在冷成型过程中的结构检验
Pub Date : 2024-05-06 DOI: 10.61326/jaasci.v3i1.127
D. Avcı, H. Yetiş, F. Karaboğa, I. Belenli
In this study, we have successfully produced a Fe-sheathed 6+1 multifilament wire using Cu/Nb/MgB2 monocore wires. The mono filament wire was prepared using Mg+2B powder mixture by powder-in-tube method without any intermediate heat treatment. The powder mixture of the amorphous nano boron (PVZ Nano Boron, purity of 98.5%, particle sizes < 250 nm) and high purity Mg powder (PVZ Mg, purity of 99%, particle size 74µm) were used. The multifilament wire was produced using groove rolling and cold drawing machines. The geometrical form of the filaments was examined using wire pieces taken from the wire at different steps throughout the production process. Finally, the multifilament wires produced in two different diameters of 1.02 mm and 0.82 mm were investigated in terms of filament uniformity, crack formation, surface roughness, and electrical transport properties. The structural examination was done on Nb filaments after the Fe and Cu sheaths were etched using HCl and HNO3 solution. The I – V measurements of the multifilament wires heat treated at 650 °C for 15, 30, 45, 60, and 240 minutes, and 700 °C for 60 minutes were carried out for the applied current up to 1 A at 25 K under various external magnetic field.
在这项研究中,我们利用铜/铌/镁硼单芯线成功制备出了铁护套 6+1 多丝线材。单丝是用管内粉末法制备 Mg+2B 混合粉末的,没有经过任何中间热处理。使用的粉末混合物包括无定形纳米硼(PVZ 纳米硼,纯度 98.5%,粒径小于 250 纳米)和高纯度镁粉(PVZ 镁,纯度 99%,粒径 74 微米)。多丝金属丝是通过轧槽机和冷拔机生产出来的。在整个生产过程的不同阶段,使用从金属丝上截取的金属丝片对金属丝的几何形状进行了检测。最后,研究了以 1.02 毫米和 0.82 毫米两种不同直径生产的多丝金属丝的长丝均匀性、裂纹形成、表面粗糙度和电气传输特性。在使用 HCl 和 HNO3 溶液蚀刻铁和铜外鞘后,对铌丝进行了结构检查。在不同的外磁场条件下,将多丝线材在 650 °C 下热处理 15、30、45、60 和 240 分钟,以及在 700 °C 下热处理 60 分钟,并在 25 K 下施加最大 1 A 的电流,对其进行了 I - V 测量。
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引用次数: 0
Purity Detection of Some Liquids by Using Reflection Values Based on Metamaterial 利用基于超材料的反射值检测某些液体的纯度
Pub Date : 2024-05-06 DOI: 10.61326/jaasci.v3i1.108
Sanam Movazzafgharehbagh, Faruk Karadağ
The aim of this work is to design and fabricate a type of sensor based on Metamaterials. This structure determines the purity of Methanol and Ethanol mixture in the water by using the Octagonal form of a resonator and sample holder. The proposed structure has been employed in the 8-12 GHZ frequency band. The important thing in the work is the changes of the waveform at the resonance frequency. The output waveform of materials (reflection coefficient S11 or transmission coefficient S12) must be changed in the liner figure by considering the dielectric coefficient. We use copper for the metal layer and resonator and Isola IS680 (3.2DK) (lossy) for substrate layer. We simulate one unit cell of this Meta-material sensor by CST microwave software and then achieve the results and evaluate them. Both the numerical and experimental tests, give the same outcomes and results and they will be in good agreement with each other. The proposed structure can be used in many applications where purity and determining of some materials might be necessary.
这项工作的目的是设计和制造一种基于超材料的传感器。这种结构通过使用八角形谐振器和样品架来确定水中甲醇和乙醇混合物的纯度。所提议的结构被用于 8-12 GHZ 频段。工作中最重要的是共振频率下的波形变化。材料的输出波形(反射系数 S11 或透射系数 S12)必须通过考虑介电系数来改变衬图。我们使用铜作为金属层和谐振器,使用 Isola IS680 (3.2DK)(有损耗)作为基底层。我们用 CST 微波软件模拟了这种元材料传感器的一个单元,然后得出了结果并进行了评估。数值测试和实验测试都得出了相同的结果和结果,而且它们之间的吻合度很高。所提出的结构可用于许多需要确定某些材料纯度的应用领域。
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引用次数: 0
Theoretical Investigation of Mechanical and Electronic Properties of Hexagonal BaB2 六方 BaB2 机械和电子特性的理论研究
Pub Date : 2024-05-06 DOI: 10.61326/jaasci.v3i1.100
C. Parlak
A comprehensive investigation of the electronic and mechanical properties in the hexagonal BaB2 binary system using state of the art first-principles computational techniques is critical for an in-depth understanding of the fundamental properties unique to this binary system. In this context, we derived elastic constants using the metric-tensor formulation, which allowed us to find important mechanical properties such as Bulk Modulus, Shear Modulus, and Vickers's hardness which are fundamental mechanical quantities. Also, this research includes a detailed analysis of the electronic band structures and a study comparison of Fermi surface topologies. The charge density at the Fermi level (N(EF)), which is very important in superconductivity theories, was found to be 1.43 states/eV.uc. Furthermore, we have explored whether there exists a close relationship between these properties and the superconducting behavior of the BaB2 material. Nevertheless, our calculations unequivocally demonstrate that the information derived from electronic band structures and Fermi surfaces alone is insufficient for a comprehensive explanation of the superconductivity phenomenon observed in such materials.
利用最先进的第一原理计算技术对六方 BaB2 双元体系的电子和机械特性进行全面研究,对于深入了解该双元体系的独特基本特性至关重要。在此背景下,我们利用度量张量公式推导出了弹性常数,从而找到了重要的力学性能,如体积模量、剪切模量和维氏硬度等基本力学量。此外,这项研究还包括对电子带结构的详细分析和对费米面拓扑结构的研究比较。研究发现,在超导理论中非常重要的费米级电荷密度(N(EF))为 1.43 个态/eV.uc。此外,我们还探讨了这些特性与 BaB2 材料的超导行为之间是否存在密切关系。尽管如此,我们的计算明确证明,仅从电子能带结构和费米面获得的信息不足以全面解释在这类材料中观察到的超导现象。
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引用次数: 0
Deuteron Optical Model Calculations for Elastic and Inelastic Reactions on 14N, 16O, 27Al Target Nuclei 关于 14N、16O、27Al 靶核弹性和非弹性反应的氘核光学模型计算
Pub Date : 2023-12-18 DOI: 10.61326/jaasci.v2i2.112
H. Büyükuslu
Nuclear reaction cross sections have a key role in nuclear radioisotope production research. It is also an important part of applied fields such as energy production and experimental nuclear studies. It has been the subject of theoretical studies such as elucidating the nuclear structure and preparing and testing nuclear reaction models. It has become a very useful tool, especially for determining nuclear optical model parameters. In this study differential cross sections were calculated for elastic and inelastic scattering of 14-15 MeV energy range deuterons from 14N, 16O and 27Al. Calculation were carried out with TALYS 1.96/2.0 nuclear reaction code. Calculations include determining the deuteron optical model that match the experimental data.  The values calculated with theoretical models were compared with experimental data obtained from the literature. While such studies are important for testing nuclear reaction models, they are also important for encouraging the preparation of nuclear reaction codes.
核反应截面在核放射性同位素生产研究中起着关键作用。它也是能源生产和核实验研究等应用领域的重要组成部分。它一直是理论研究的主题,如阐明核结构以及准备和测试核反应模型。它已成为一种非常有用的工具,尤其是在确定核光学模型参数方面。本研究计算了 14N、16O 和 27Al 的 14-15 MeV 能量范围氘核的弹性和非弹性散射的差分截面。计算使用 TALYS 1.96/2.0 核反应代码进行。计算包括确定与实验数据相匹配的氘核光学模型。 用理论模型计算出的数值与从文献中获得的实验数据进行了比较。这些研究对测试核反应模型非常重要,同时对鼓励编制核反应代码也很重要。
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引用次数: 0
New Crystal Photodiode Combination for Environmental Radiation Measurement 用于环境辐射测量的新型晶体光电二极管组合
Pub Date : 2023-12-18 DOI: 10.61326/jaasci.v2i2.103
I. Tapan, Fatma Kocak
Here, a new design will be introduced to detect radiation in the environment with high efficiency. The designed structure consists of placing ZnS–Si APD and PIN photodiodes at the ends of conventional crystals such as NaI(Tl) and CsI(Tl). Since ZnS is transparent to photons with wavelengths between 340 and 10000 nm, photons coming from the crystals are absorbed directly in the depletion region and generate primary particles. With an increase in the number of generated primary particles, a stronger and cleaner signal is obtained. In the simulation work, the light generated by 30 keV–3 MeV gamma rays in the crystals was obtained using the Geant4 simulation code. The single-particle Monte Carlo technique was used to calculate the photodiode output signal for the crystal emission spectrum. The simulation results showed that the crystals and ZnS–Si photodiode structures formed a good combination. The high quantum efficiency and low excess noise factor make the ZnS–Si structure an excellent choice for scintillating light detection.
这里将介绍一种新的设计,用于高效探测环境中的辐射。所设计的结构包括在 NaI(Tl)和 CsI(Tl)等传统晶体的两端放置 ZnS-Si APD 和 PIN 光电二极管。由于 ZnS 对波长介于 340 纳米和 10000 纳米之间的光子是透明的,因此来自晶体的光子会被耗尽区直接吸收并产生原生粒子。随着产生的原生粒子数量的增加,会获得更强、更纯净的信号。在模拟工作中,使用 Geant4 模拟代码获得了 30 keV-3 MeV 伽马射线在晶体中产生的光。利用单粒子蒙特卡洛技术计算了晶体发射光谱的光电二极管输出信号。模拟结果表明,晶体和 ZnSi-Si 光电二极管结构形成了良好的组合。高量子效率和低过量噪声系数使 ZnS-Si 结构成为闪烁光探测的最佳选择。
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引用次数: 0
Non-Destructive Testing Using Transmission Line-Based Microwave Sensors 使用基于传输线的微波传感器进行无损检测
Pub Date : 2023-12-18 DOI: 10.61326/jaasci.v2i2.109
Sanam Movazzafgharehbagh, Faruk Karadağ
In this study, some types of antennas and metamaterial structures have been designed and produced with the aim of determining and detecting ionized chlorine of sea sand in concrete. The first structure has a Loop-like resonator with the sample, the second structure has a Bowtie-shaped resonator with the sample and the third structure has double loop resonators on both sides of concrete samples also non-destructive method is applied for all structures. Different samples of concrete are produced with different proportions of ionized sea sand. Electrical properties of concrete samples for all structures are investigated in the frequency range of 1-9 GHz. The structures are designed in the CST Microwave Studio program. Also, the simulation study of the designed structures shows that the most important resonance frequency changes, considering the dielectric constant of concrete samples, for the Loop-like structure occur in the 1-8 GHz, Bowtie-shaped structure in 1-4 GHz and double Loop structure in 1-9 GHz of frequency band. The important point in this study is the changes of the waveform at the resonance frequency. The output waveform (reflection coefficient S11/ transmission coefficient S12) should change in linear form by considering the dielectric coefficient. We have used copper for the resonators and also the material with ℇ value of 3 as the substrate layers of the structures. We have simulated three types of designed structures with CST Microwave Software and then achieve the results and evaluate them. Both numerical and experimental tests have given approximately same results and are in good agreement with each other. These proposed structures can be used in many applications where it is necessary to determine the rate of ionized sea sand in cement-based composites such as concrete.
本研究设计并制作了一些类型的天线和超材料结构,旨在确定和检测混凝土中海砂的电离氯。第一种结构是带有样品的环状谐振器,第二种结构是带有样品的弓形谐振器,第三种结构是混凝土样品两侧的双环谐振器,所有结构都采用了非破坏性方法。使用不同比例的电离海砂制作不同的混凝土样品。在 1-9 GHz 的频率范围内,对所有结构的混凝土样品的电特性进行了研究。这些结构是在 CST Microwave Studio 程序中设计的。对所设计结构的模拟研究还表明,考虑到混凝土样品的介电常数,环状结构最重要的共振频率变化发生在 1-8 GHz,弓形结构发生在 1-4 GHz,双环结构发生在 1-9 GHz 频段。本研究的重点是共振频率下的波形变化。考虑到介电系数,输出波形(反射系数 S11/ 传输系数 S12)应呈线性变化。我们使用铜作为谐振器,并使用ℇ 值为 3 的材料作为结构的基底层。我们用 CST 微波软件模拟了三种设计结构,然后对结果进行了评估。数值测试和实验测试得出的结果大致相同,并且相互吻合。这些建议的结构可用于许多需要确定水泥基复合材料(如混凝土)中电离海砂比率的应用中。
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引用次数: 0
Design of Voltage Transducer for Digital Signal Processing Development Kit in Implementation of a High Step-up DC-DC Converter 为数字信号处理开发套件设计电压传感器以实现高升压直流-直流转换器
Pub Date : 2023-12-18 DOI: 10.61326/jaasci.v2i2.99
Yavuz Koç
High step-up DC-DC converters are used in many industrial applications Especially, renewable energy systems that have a low output voltage and high output current need DC-DC converters with high voltage gain to meet the requirements of the grid-connected systems for a high output voltage. This study is aimed to design an implementation of hardware of the high step-up DC-DC converter’s measurement board prototype for digital signal processing (DSP) TMS320F28335 development kits. The vital parameter to detect for high step-up application systems is a sampling output voltage. This sample of output voltage is produced by using the voltage transducer (LV 25-P) with hall effect sensor in this research.  A signal conditioning circuit includes an operational amplifier featuring unity gain buffer for the protection ADC of the DSP and a low pass filter circuit. Therefore, the requirements of the ADC of EZDSP TMS320F28335 development kit can be met by using this voltage transducer sensor and the signal conditioning circuit.
高升压直流-直流转换器广泛应用于工业领域,特别是输出电压低、输出电流大的可再生能源系统需要高电压增益的直流-直流转换器,以满足并网系统对高输出电压的要求。本研究旨在为数字信号处理(DSP)TMS320F28335 开发套件设计高升压 DC-DC 转换器测量板原型的硬件实现。高升压应用系统的重要检测参数是输出电压采样。在本研究中,输出电压采样是通过使用带有霍尔效应传感器的电压传感器(LV 25-P)产生的。 信号调节电路包括一个运算放大器,其特点是为 DSP 的保护 ADC 提供统一增益缓冲器,以及一个低通滤波器电路。因此,通过使用该电压传感器和信号调节电路,可以满足 EZDSP TMS320F28335 开发套件 ADC 的要求。
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引用次数: 0
Investigation of Optical and Structural Properties of VO2 Thin Films by Thermal Treatment 通过热处理研究 VO2 薄膜的光学和结构特性
Pub Date : 2023-12-18 DOI: 10.61326/jaasci.v2i2.101
Gökhan Ekinci, Bünyamin Özkal, Nora Ali A. S. Al-Jawfi, S. Kazan
In this study, VO2 thin films were grown on SiO2 substrate using the PLD method. Then the grown VO2 thin films were subjected to heat treatments at different temperatures and times in the atmosphere environment. The structural properties of the heat-treated films were investigated using X-ray diffraction (XRD) technique and Raman spectroscopy techniques. The surface microstructures of these films were investigated by Scanning Electron Microscope (SEM) technique, and their optical properties and bond structures were investigated by Photoluminescence (PL) spectra and Fourier Transform Infrared Spectroscopy (FTIR) measurements, respectively. Especially XRD and Raman results revealed that heat treatments with high temperature values transformed the films into VO2 and V2O5 mixed-phase crystal structures. Due to the heat treatment carried out in the atmosphere and the high oxygen affinity of the vanadium metal, crystallization took place in both VO2 and V2O5 forms. In order to obtain homogeneous crystalline VO2 structures, heat treatments should be carried out for a long time in oxygen-limited environments.
本研究采用 PLD 方法在二氧化硅基底上生长出 VO2 薄膜。然后在大气环境中对生长的 VO2 薄膜进行不同温度和时间的热处理。使用 X 射线衍射 (XRD) 技术和拉曼光谱技术研究了热处理薄膜的结构特性。扫描电子显微镜(SEM)技术研究了这些薄膜的表面微观结构,光致发光(PL)光谱和傅立叶变换红外光谱(FTIR)测量分别研究了它们的光学性质和键合结构。尤其是 XRD 和拉曼结果显示,高温热处理使薄膜转变为 VO2 和 V2O5 混相晶体结构。由于热处理是在大气中进行的,而且金属钒与氧的亲和性很高,因此结晶以 VO2 和 V2O5 两种形式出现。为了获得均匀的 VO2 晶体结构,应在限氧环境中进行长时间的热处理。
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引用次数: 0
Synthesis of NiSe2 Materials Directly on Ni Foam using Microwave-Assisted Technique and Employing as Electrode Material in Supercapacitors 利用微波辅助技术在镍泡沫上直接合成 NiSe2 材料并将其用作超级电容器的电极材料
Pub Date : 2023-12-18 DOI: 10.61326/jaasci.v2i2.98
R. Taş, Ebru Köroğlu, Vedat Emin Ayaz
As the world’s population grows, the energy crisis is becoming an increasingly severe problem, driving the need for energy storage. This demand is a significant driver for innovation and development in the energy sector. Clean and sustainable energy research focuses on two areas: renewable resources and high-performance energy storage systems. Today’s energy systems provide large amounts of electricity generation, but the desired results cannot be achieved in the energy storage process. There is an urgent need for high-capacity and efficient energy storage devices. Supercapacitors are one of the most promising technologies for energy storage. They have competitive features such as high power density, excellent cycle stability, and short charge/discharge time. This study demonstrates the potential usage of NiSe2 in supercapacitor applications as cathode material. In an experimentally novel approach, NiSe2 on nickel foam was synthesized by a fast, simple, and inexpensive microwave-assisted method in the presence of selenium salt. In this route, nickel foam was employed as both nickel source and substrate. Furthermore, the electrochemical properties of the prepared NiSe2 cathodes were investigated in three electrodes system. As a result, NiSe2 obtained in 45 minutes delivers a high capacitance of 3.3 F/cm2 at a high current density of 5 mA/cm2.
随着世界人口的增长,能源危机正成为一个日益严重的问题,从而推动了对能源储存的需求。这种需求是能源领域创新和发展的重要驱动力。清洁和可持续能源研究主要集中在两个领域:可再生资源和高性能储能系统。当今的能源系统提供了大量的发电量,但在储能过程中却无法达到预期效果。我们迫切需要大容量、高效率的储能设备。超级电容器是最有前途的储能技术之一。超级电容器具有高功率密度、出色的循环稳定性和较短的充放电时间等优势。本研究证明了 NiSe2 作为阴极材料在超级电容器应用中的潜在用途。通过一种新颖的实验方法,在硒盐的存在下,采用快速、简单、廉价的微波辅助方法合成了泡沫镍上的 NiSe2。在该方法中,泡沫镍既是镍源又是基底。此外,还在三电极系统中研究了制备的 NiSe2 阴极的电化学特性。结果表明,在 5 mA/cm2 的高电流密度下,45 分钟内获得的 NiSe2 可提供 3.3 F/cm2 的高电容。
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引用次数: 0
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Journal of Advanced Applied Sciences
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