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Challenges in Rietveld Refinement and Structure Visualization in Ceramics 陶瓷中Rietveld细化和结构可视化的挑战
Pub Date : 2021-02-12 DOI: 10.5772/INTECHOPEN.96065
T. A. Para, S. Sarkar
The most common and basic characterization in the field of material science is the almighty X-ray diffraction (XRD). In every institute, every research report and every manuscript, concerning material properties, the X-ray diffraction pattern is essentially found. Although the basis of these works relies on the fact that X-ray diffraction pattern was found to be matching with some structure in a database, the in depth significance of the various characteristic diffraction manifestations of various physical characters are rarely discussed. Most of the researchers (especially beginners) are either not aware of the prowess of X-ray based characterizations, or have not been introduced to it properly or may be sometimes they are not interested in its results at all. The decreased interest (later) in the results from such studies might be for not being productive enough for time spending or non-effectiveness in justifying the motivation of the work. The former two are more related to the availability and accessibility of study material for the development of core concepts. Most of the institutes always do not have access to the span-wide scientific literature and the researchers joining these institutions are partly affected. In this context the effective open-access and free availability of intech-open, it is prudent to at least attempt to accumulate, assimilated and aggregate the concepts related to X-ray diffraction in a single package. The chapter is an attempt in the path of this route.
在材料科学领域最常见和最基本的表征是全能的x射线衍射(XRD)。在每一个研究所、每一份研究报告和每一份手稿中,关于材料的性质,基本上都能找到x射线衍射图。虽然这些工作的基础是在数据库中发现x射线衍射图与某些结构相匹配,但很少讨论各种物理特性的各种特征衍射表现的深入意义。大多数研究人员(尤其是初学者)要么没有意识到基于x射线的表征的威力,要么没有正确地介绍它,或者有时他们对它的结果根本不感兴趣。对这些研究结果的兴趣降低(后来)可能是因为没有足够的时间花费或在证明工作动机方面没有有效性。前两者更多地与核心概念发展的学习材料的可获得性和可及性有关。大多数研究机构总是无法获得广泛的科学文献,而加入这些机构的研究人员在一定程度上受到影响。在有效的开放获取和免费获取技术的背景下,至少尝试将与x射线衍射有关的概念积累、吸收和汇总在一个单一的包中是谨慎的。本章是在这条道路上的一次尝试。
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引用次数: 7
Ferroelectric Glass-Ceramic Systems for Energy Storage Applications 用于储能应用的铁电玻璃陶瓷系统
Pub Date : 2020-11-27 DOI: 10.5772/intechopen.93855
Abdulkarim Z. Khalf
An overview of ferroelectric glass ceramics, some literature review and some of the important previous studies were focused in this chapter. Nanocrystalline glass–ceramics containing ferroelectric perovskite-structured phases have been included. All modified glasses having ferroelectric ceramics which prepared by different methods are discussed, that producing nanocrystalline glass–ceramics. Then particular tested to their use as dielectric energy storage materials. These materials exhibit promising dielectric properties, indicating good potential for high energy density capacitors as a result of their nanocrystalline microstructures. The results of the analysis are summarised in this chapter to provide an overview of the energy storage characteristics of the different materials produced during the study.
本章主要介绍了铁电玻璃陶瓷的研究概况、相关文献综述以及一些重要的前人研究成果。含有铁电钙钛矿结构相的纳米晶微晶玻璃已被包括在内。讨论了用不同方法制备的铁电陶瓷改性玻璃,从而制备出纳米微晶玻璃。然后特别测试了它们作为电介质储能材料的用途。这些材料表现出良好的介电性能,由于其纳米晶微观结构,表明高能量密度电容器具有良好的潜力。本章总结了分析结果,概述了研究过程中产生的不同材料的储能特性。
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引用次数: 1
New Bismuth Sodium Titanate Based Ceramics and Their Applications 新型钛酸铋钠基陶瓷及其应用
Pub Date : 2020-10-14 DOI: 10.5772/intechopen.93921
Hengchang Nie, Genshui Wang, Xianlin Dong
Ferroelectric materials are widely investigated due to their excellent properties and versatile applications. At present, the dominant materials are lead-containing materials, such as Pb (Zr,Ti)O3 solid solutions. However, the use of lead gives rise to environmental concerns, which is the driving force for the development of alternative lead-free ferroelectric materials. (Bi0.5Na0.5)TiO3-based ceramics are considered to be one of the most promising lead-free materials to replace lead-containing ferroelectric ceramics due to their excellent ferroelectric properties, relaxation characteristics, and high Curie point. After decades of efforts, great progress has been made in the phase structure characterization and properties improvement of BNT based ceramics. However, most of the studies on BNT system mainly focuses on its piezoelectric properties and application of piezoelectric sensors and strain actuators, little attention is paid to its ferroelectric properties and related applications. In this chapter, new BNT-based ceramics via composition modification and special focuses on the ferroelectric properties, phase transition behaviors under external fields and related applications, such as application in energy storage, pulsed power supply and pyroelectric detection were proposed.
铁电材料因其优异的性能和广泛的应用而受到广泛的研究。目前,主导材料是含铅材料,如Pb (Zr,Ti)O3固溶体。然而,铅的使用引起了环境问题,这是发展替代无铅铁电材料的动力。(Bi0.5Na0.5) tio3基陶瓷由于其优异的铁电性能、弛豫特性和较高的居里点,被认为是取代含铅铁电陶瓷的无铅材料之一。经过几十年的努力,在BNT基陶瓷的相结构表征和性能改善方面取得了很大进展。然而,目前对BNT系统的研究大多集中在其压电特性及压电传感器和应变执行器的应用上,对其铁电特性及相关应用关注较少。在本章中,提出了通过成分改性的新型bnt基陶瓷,重点研究了其铁电性能、外场下的相变行为及其在储能、脉冲电源和热释电检测等方面的应用。
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引用次数: 0
Ceramic Materials: Science and Engineering 陶瓷材料:科学与工程
Pub Date : 2013-01-01 DOI: 10.1007/978-1-4614-3523-5
B. Carter, M. G. Norton, L. Wang
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引用次数: 752
Ceramics Process Engineering 陶瓷工艺工程
Pub Date : 1991-01-01 DOI: 10.1016/B978-0-08-034720-2.50029-0
D. Perduijn
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引用次数: 0
Insulators, Low-Voltage 绝缘体,低压
Pub Date : 1991-01-01 DOI: 10.1016/B978-0-08-034720-2.50072-1
E. Smoke
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引用次数: 0
Directed Metal Oxidation 定向金属氧化
Pub Date : 1991-01-01 DOI: 10.1016/B978-0-08-034720-2.50043-5
N. Claussen, A. Urquhart
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引用次数: 2
Cold Isostatic Pressing 冷等静压
Pub Date : 1991-01-01 DOI: 10.1016/B978-0-08-034720-2.50031-9
K. J. Morris
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引用次数: 1
Refractory Materials, Specialty 耐火材料,特种
Pub Date : 1991-01-01 DOI: 10.1016/B978-0-08-034720-2.50110-6
D. F. Beal
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引用次数: 0
NTC Thermistor Materials NTC热敏电阻材料
Pub Date : 1991-01-01 DOI: 10.1016/B978-0-08-034720-2.50091-5
E. Macklen
{"title":"NTC Thermistor Materials","authors":"E. Macklen","doi":"10.1016/B978-0-08-034720-2.50091-5","DOIUrl":"https://doi.org/10.1016/B978-0-08-034720-2.50091-5","url":null,"abstract":"","PeriodicalId":7260,"journal":{"name":"Advanced Ceramic Materials","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"1991-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80511177","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
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Advanced Ceramic Materials
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