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Short-Range Order and the Nucleation of Long-Range Order in Ni-Rich Nickel-Niobium Alloys 富镍镍铌合金的近程有序与远程有序形核
Pub Date : 1900-01-01 DOI: 10.1179/030634571790439487
C. V. D. Wekken, R. Taggart, D. H. Polonis
AbstractThe changes in the electrical resistivity of nickel-rich Ni-Nb alloys due to the formation of short-range order exhibit an anomalous dependence on the solute concentration. This anomaly can be explained by the formation of embryos of long-range order of the type Ni8Nb in alloys approaching the NisNb composition and near the critical temperature for long-range order. In the absence of a critical concentration of quenched-in vacancies, short-range-order formation only has been detected during ageing below the critical temperature.
摘要富镍Ni-Nb合金的电阻率变化与溶质浓度有异常的关系。这种异常现象可以解释为,在接近NisNb成分的合金中,在接近长程临界温度时,形成了长程Ni8Nb型胚。在没有临界淬火空位浓度的情况下,只有在低于临界温度的时效过程中才检测到短程阶的形成。
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引用次数: 15
Widmanstätten Precipitation from Non-Ideal Solid Solution: αinβ-CuZn Widmanstätten非理想固溶体的沉淀:αinβ-CuZn
Pub Date : 1900-01-01 DOI: 10.1179/030634571790439685
G. Purdy
AbstractThe diffusional growth of Widmanstatten α rods from ordered β-brass has been studied by means of deep-etching techniques and scanning electron microscopy. Slow-growing rods have large tip radii. The lengthening rates and tip radii of fast-growing rods are in good accord with a local-equilibrium model in which account is taken of non-ideal thermodynamic behaviour.
摘要采用深度刻蚀技术和扫描电镜研究了有序β-黄铜中维氏α棒的扩散生长。生长缓慢的杆有大的尖端半径。速生棒的延长速率和尖端半径符合考虑非理想热力学行为的局部平衡模型。
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引用次数: 43
On the Formation of Internal Fatigue Damage in Association with Twins in α-Titanium α-钛中孪晶内部疲劳损伤的形成
Pub Date : 1900-01-01 DOI: 10.1179/MSC.1969.3.1.74
C. Beevers, M. Halliday
AbstractCoarse-grained (∼0·3 mm) α-titanium has been fatigued in tension/compression about a zero mean load at a frequency of ∼ 100 Hz at room temperature. A combined metallographic and microbeam X-ray analysis revealed the presence of { 10 1 ¯ 2 } -, { 11 2 ¯ 1 } -, and { 11 2 ¯ 2 } - type twins. In internal grains, i.e. grains completely constrained by surrounding material, fatigue _damage was observed to be associated with the { 11 2 ¯
粗晶(~ 0.3 mm) α-钛在室温下以~ 100 Hz的频率在平均载荷为零的拉伸/压缩下疲劳。结合金相和微束x射线分析,发现存在{10¯2}-,{11¯1}-和{11¯2}-型双胞胎。在内部晶粒中,即完全受周围材料约束的晶粒,观察到疲劳损伤与{11.2¯有关
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引用次数: 20
The Surface Energy of Iron-3% Silicon by Surface-Relaxation Measurements 用表面弛豫测量铁-3%硅的表面能
Pub Date : 1900-01-01 DOI: 10.1179/MSC.1967.1.1.9
B. Mills, H. Jones, G. Leak
AbstractThe surface energy of iron-3% silicon alloy has been determined as 1940 ± 600 erg. cm−2 for the range 1075–1325° C by measuring the decay kinetics of multiple scratches on single crystals near (110) orientation during vacuum annealing. Mass transport occurred mainly by volume diffusion in the alloy. Surface-energy values from single scratches were higher by ∼ 20% than those from multiple scratches, probably because of inadequacies in the single-scratch analysis. Facets formed where the smoothed scratch profile contained the (110) plane at the highest temperature (1300° C) only and for the crystal nearest to (110) orientation. It was noted that extended striations formed on a single crystal near (100) orientation on annealing at 1200° C, in the direction for which a small surface tilt would expose the (100) plane. These observations suggest that the γ-plot has a deeper cusp at (100) than at (110) under the annealing conditions prevailing.
摘要测定了铁-3%硅合金的表面能为1940±600 erg。在1075-1325°C范围内,通过测量真空退火过程中单晶在(110)取向附近的多重划痕的衰减动力学。在合金中主要通过体积扩散进行传质。单次划痕的表面能值比多次划痕的表面能值高约20%,这可能是因为单次划痕分析的不足。在最高温度(1300°C)下,光滑的划痕轮廓包含(110)平面,并且最接近(110)方向的晶体形成切面。注意到,在1200℃退火时,单晶在(100)取向附近形成了延伸的条纹,其方向是表面轻微倾斜会暴露(100)平面。这些观测结果表明,在普遍的退火条件下,γ-图在(100)处比在(110)处有更深的尖点。
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引用次数: 6
Stress Relaxation in Single Crystals of Copper and α-Brasses 铜和α-黄铜单晶的应力松弛
Pub Date : 1900-01-01 DOI: 10.1179/030634568790443189
P. Feltham, C. J. Spears
AbstractStress relaxation at constant strains has been studied in crystals of copper and α-brasses containing 10, 20, or 30 at.-% zinc at 77,200, and 291° K after consecutive small plastic deformations. Close to the yield point the relaxation was generally within 1% of the applied stress, but at large deformations, notably within the third stage of work-hardening, it attained ∼ 10%. Any given relaxation was observed for ∼ 1000 sec, over most of which period the decay of the stress was logarithmic in time. Energy barriers of the activated process were from ∼ 0.08 eV for copper and 0.2–0.3 eV for brasses. Their significance is discussed in terms of a model in which unpinning of dislocations from rows of solute atoms is the principal process determining the relaxation rate.
摘要本文研究了含10、20、30 at的铜和α-黄铜晶体在恒应变下的应力松弛。-%锌在77,200和291°K连续小塑性变形后。在接近屈服点时,松弛通常在施加应力的1%以内,但在大变形时,特别是在加工硬化的第三阶段,松弛达到了~ 10%。任何给定的松弛被观察到~ 1000秒,在大部分时间内,应力的衰减是对数的。激活过程的能垒为铜的~ 0.08 eV和黄铜的0.2 ~ 0.3 eV。它们的意义是根据一个模型来讨论的,在这个模型中,从一排排的溶质原子中解除位错是决定弛豫速率的主要过程。
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引用次数: 11
Deviations from Linearity in Creep-Rupture Curves 蠕变-破裂曲线的线性偏差
Pub Date : 1900-01-01 DOI: 10.1179/MSC.1967.1.1.172
R. Lagneborg
AbstractBreaks in the stress/rupture time and stress/creep rate relation are known to occur during high-temperature creep. In the present work these deflections are explained in terms of different stress-dependences of the intracrystalline deformation rate and the rate of grain-boundary sliding. The transition from trans- to intercrystalline fracture, which coincides, at least approximately, with these breaks, is suggested to be due to the increased grain-boundary sliding at stresses below the break.
摘要高温蠕变过程中,应力/断裂时间和应力/蠕变速率关系出现断裂。在本工作中,这些偏转被解释为不同应力依赖的晶内变形速率和晶界滑动速率。从跨晶断裂到晶间断裂的转变,至少近似地与这些断裂相吻合,被认为是由于在断裂以下的应力下晶界滑动的增加。
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引用次数: 5
The Effects of Load Ratio, Interstitial Content, and Grain Size on Low-Stress Fatigue-Crack Propagation in α-Titanium 载荷比、间隙含量和晶粒尺寸对α-钛合金低应力疲劳裂纹扩展的影响
Pub Date : 1900-01-01 DOI: 10.1179/030634573790445550
J. Robinson, C. Beevers
AbstractLow-stress fatigue-crack-propagation tests have been carried out on three commercially pure α-titaniumalloys. It was found that decreasing load ratio (R), increasing grain size, and increasing interstitial alloying content could all produce significant reductions in growth rate over the ∆K range studied (4–20 MN/m2). The conclusion was reached that the fatigue-fracture process comprised two stages: (1) the formation of relatively planar facets (primarily ∆K-controlled) and (2) their interconnection by a mechanism involving plastic tearing (primarily K max-controlled). Scanning electron microscope examination of the fatigue-fracture surfaces revealed that the orientations of individual grains exerted a considerable influence on fracture-surface morphology. This effect occurred when the scale of reversed plasticity at the crack tip was of the order of, or less than, the grain size. A transition in fracturesurface appearance occurred in all specimens at an approximately constant value of growth rate ...
摘要对三种市售纯α-钛合金进行了低应力疲劳裂纹扩展试验。在研究的∆K范围内(4 ~ 20 MN/m2),减小载荷比(R)、增大晶粒尺寸和增加间隙合金含量均能显著降低合金的生长率。得出的结论是,疲劳断裂过程包括两个阶段:(1)相对平面切面的形成(主要由∆K控制)和(2)它们通过塑性撕裂机制相互连接(主要由K最大值控制)。对疲劳断口表面的扫描电镜检查表明,单个晶粒的取向对断口表面形貌有相当大的影响。当裂纹尖端的反向塑性规模等于或小于晶粒尺寸时,就会出现这种效应。所有试样的断口表面形貌都以近似恒定的生长速率发生转变。
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引用次数: 93
Extrinsic Stacking-Fault Energies in F.C.C. Materials fcc材料的外部堆叠故障能
Pub Date : 1900-01-01 DOI: 10.1179/MSC.1967.1.1.198
P. Goodhew, P. Dobson, R. Smallman
AbstractThe extrinsic stacking-fault energy of aluminium has been determined from the isothermal annealing of double-faulted dislocation loops in the electron microscope and found to be 30% greater than the intrinsic energy. The observed rarity of extrinsic faulting in thin foils is accounted for in terms of a nucleation barrier to the formation of an extrinsic fault. Several previous observations of extrinsic faults, some of which have been taken to imply a higher extrinsic stacking-fault energy, are re-examined in the light of this barrier.
摘要通过对双错位错环的等温退火,在电镜下测定了铝的本征叠错能,发现其比本征叠错能大30%。在薄箔中观察到的外部断层的罕见性是根据外部断层形成的成核屏障来解释的。在这个势垒的基础上,我们重新检查了以前对外部断层的一些观测,其中一些观测被认为意味着更高的外部堆叠断层能量。
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引用次数: 12
Correlation of Magnetic Permeability and Microstructure in Cupro-Nickel Alloys 铜镍合金磁导率与显微组织的关系
Pub Date : 1900-01-01 DOI: 10.1179/030634573790445361
M. Vowles, J. Billingham, E. Culpan
AbstractThe magnetic permeability of a series of complex, high-strength cupro-nickel alloys is shown to be strongly dependent on the composition and degree of order of the strengthening γ′ (Ni3Al-type) precipitate. Electron metallography and X-ray-diffraction techniques were used to study the precipitation occurring in such alloys in the quenched, slowly cooled, and aged conditions. The composition of the γ′ precipitate varied with both alloy content and heat-treatment but was of the general form (NiCuh)3(AlFeMn). The effect of precipitate composition and degree of order on magnetic permeability was examined in a number of synthetic alloys with compositions similar to those of precipitates extracted from the original alloys. A direct correlation of magnetic permeability with the ordered state of these precipitates was possible by means of dark-field microscopy. The alloys have high magnetic permeability when ordered ferromagnetic precipitates are formed within a limited composition range. Magnetic permeab...
摘要一系列复杂的高强铜镍合金的磁导率与强化γ′(ni3al型)析出相的组成和有序程度密切相关。利用电子金相和x射线衍射技术研究了在淬火、慢冷和时效条件下合金中的析出现象。γ′析出物的组成随合金含量和热处理的不同而变化,但均为一般形式(NiCuh)3(AlFeMn)。用与原合金析出相成分相近的合成合金,研究了析出相组成和有序度对磁导率的影响。磁导率与这些沉淀物的有序状态之间的直接关系可以通过暗场显微镜得到。当在有限的成分范围内形成有序的铁磁沉淀时,合金具有较高的磁导率。磁permeab……
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引用次数: 1
The Effect of Hydrogen on the Work-Hardening and Fracture Behaviour of Titanium–Low-Aluminium–Low-Manganese Alloys 氢对钛-低铝-低锰合金加工硬化和断裂行为的影响
Pub Date : 1900-01-01 DOI: 10.1179/MSC.1969.3.1.190
R. Haynes, P. Maddocks
Abstract True stress/true strain curves have been determined for two fine-grained (α + β) titanium alloys containing various amounts of hydrogen, which was present either in solid solution or in solid solution and as a film-like hydride precipitate. In hydride-free specimens three stages, with high, low, and intermediate work-hardening exponents, are identified in the work-hardening of the alloys. The three stages, in order of occurrence, are attributed to partial plastic deformation, easy glide, and parabolic hardening. The presence of hydride lowers the initial flow stress, extends the first stage, eliminates the second stage, and lowers the work-hardening exponent of the third stage of work-hardening. These changes are believed to be caused by the hydride particles acting as stress concentrators, thus enabling localized plastic deformation to occur at low macroscopic stress levels and inducing complex slip at an early stage in work-hardening. Hydride precipitate also causes loss of ductility by markedl...
摘要:测定了两种细晶(α + β)钛合金的真应力/真应变曲线,分别以固溶体和固溶形式存在,并以膜状氢化物析出。在无氢化物试样中,合金的加工硬化分为高、低和中等加工硬化阶段。这三个阶段按发生的先后顺序分别为部分塑性变形、易滑动和抛物线硬化。氢化物的存在降低了初始流动应力,延长了第一阶段,消除了第二阶段,降低了第三阶段的加工硬化指数。这些变化被认为是由氢化物颗粒作为应力集中剂引起的,从而使局部塑性变形在低宏观应力水平下发生,并在加工硬化的早期阶段诱发复杂滑移。氢化物析出物也会造成市场上的延展性损失。
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引用次数: 4
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Metal Science Journal
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