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Storage Temperature Effect on Shelf Life Characteristics of Roasted Coffee Beans Packaged in Metalized Bag With a Pressure Releasing Valve 温度对带减压阀金属袋装烘培咖啡豆保质期特性的影响
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-16 DOI: 10.1111/jfpe.70288
Su Chan Kim, Gyu Ri Kim, Dong Sun Lee, Jung Hee Woo, Duck Soon An

The effect of storage temperature on moderately dark roasted coffee beans packaged in Al-metallized bags was investigated focusing on the package atmospheric change and the product quality deterioration. Al-vacuum metallized bag packages of 100 g product attached with a pressure-releasing valve were stored at 15°C, 25°C, 35°C, and 45°C, with measurements in changes of package gas composition, package volume, and product quality attributes. Package atmospheric and volumetric change behavior was examined in relation to the product's carbon dioxide production measured in a separate experiment. The CO2 production was characterized using the Weibull function form, which effectively quantified the influence of temperature: higher storage temperatures resulted in increased and faster CO2 production with activation energy of 17–18 kJ/mol as described by the Arrhenius dependence. The headspace, originally containing ambient air, transitioned to and maintained the high CO2 partial pressures mostly exceeding 0.7 atm, alongside reduced O2 and N2 partial pressures of 0.01–0.02 and 0.07–0.11 atm, respectively, due to flushing by CO2 gas released from the coffee beans. This initial shift in gas concentration was more pronounced at higher temperatures. While temperature exhibited no significant effect on pH and titratable acidity changes of the product except at the later stage at 45°C, oxidation measured in peroxide value increase was found to be a primary quality degradation factor. This oxidation process showed clear dependence on temperature, following the Arrhenius equation with an activation energy of 42.5 kJ/mol, suggesting its suitability as a model for accelerated shelf life testing.

研究了贮存温度对铝金属袋装中度深焙咖啡豆的影响,重点研究了包装气氛的变化和产品质量的恶化。将100g产品的铝真空金属化袋包装连接减压阀,分别在15℃、25℃、35℃、45℃下保存,测量包装气体成分、包装体积和产品质量属性的变化。包装大气和体积变化的行为进行了检查,关系到产品的二氧化碳产量测量在一个单独的实验。CO2产率采用Weibull函数形式进行表征,该函数有效地量化了温度的影响:较高的储存温度导致CO2产率增加和加快,活化能为17-18 kJ/mol,符合Arrhenius依赖性。最初含有环境空气的顶空过渡到并保持了高CO2分压,大部分超过0.7 atm,同时由于咖啡豆释放的CO2气体的冲刷,O2和N2分压分别降低了0.01-0.02和0.07-0.11 atm。这种气体浓度的初始变化在较高的温度下更为明显。温度对产品的pH和可滴定酸度变化没有显著影响,但在45℃的后期,通过过氧化值增加测量的氧化被发现是主要的质量退化因素。该氧化过程具有明显的温度依赖性,符合Arrhenius方程,活化能为42.5 kJ/mol,表明其适合作为加速货架期测试的模型。
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引用次数: 0
Assessment of the In Vitro Glycemic Index, Content of Bioactive Compounds, and Their In Vitro Bioaccessibility in White Bread Enriched With Pinus nigra Ten. Bark Extract 黑松白面包体外升糖指数、生物活性化合物含量及其体外生物可及性的研究树皮中提取
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-16 DOI: 10.1111/jfpe.70267
Kubra Feyza Erol, Gozde Kutlu, Necattin Cihat Icyer, Fatih Tornuk

Pinus nigra Ten. (black pine) bark, a by-product of the timber industry, is rich in bioactive compounds with high antioxidant activity and various health benefits. This study investigated the effects of the addition of pine bark extract (PBE) into bread at different concentrations (0%, 0.25%, 0.50%, and 1.00%; w/w) on the hydrolysis index (HI), predicted glycemic index (pGI), antioxidant activity (DPPH and FRAP), total phenolic content (TPC), in vitro phenolic digestibility, mineral composition, textural properties, and sensory attributes. Bioaccessibility levels of the control bread were 6.79% for TPC, 8.99% for FRAP activity, and 6.44% for DPPH radical scavenging activity, whereas 1.00% PBE-enriched bread exhibited significantly higher values of 28.63%, 30.14%, and 22.75%, respectively. Incorporation of 0.50% and 1.00% of PBE into bread also reduced their pGI significantly; thereby these breads were classified as medium (pGI = 66.28 and 59.29, respectively) glycemic index. A strong linear correlation was observed between TPC and antioxidant activities. Mineral analysis (mg/100 g) confirmed the presence of essential macro- (Ca [19.79–38.95], K [4.80–25.72], Mg [5.78–12.38], Na [7.12–28.29]) and microelements (Zn [2.62–3.61], Cu [< 2.5], Fe [< 2.5], Mn [< 2.5]) in especially PBE-enriched breads. Texture analysis showed that the breads became softer (304.43–394.09 N) in proportion to the PBE level while sensory evaluations did not show any negative effect of PBE addition. Overall, these findings highlighted the potential of PBE as a valuable functional ingredient for enhancing the nutritional and technological properties of bakery products.

黑松(黑松)树皮是木材工业的副产品,含有丰富的生物活性化合物,具有高抗氧化活性和各种健康益处。研究了在面包中添加不同浓度(0%、0.25%、0.50%和1.00%;w/w)的松皮提取物(PBE)对面包水解指数(HI)、预测升糖指数(pGI)、抗氧化活性(DPPH和FRAP)、总酚含量(TPC)、体外酚消化率、矿物质组成、质地特性和感官特性的影响。对照面包的TPC、FRAP和DPPH自由基清除活性的生物可及性分别为6.79%、8.99%和6.44%,而富含1.00% pbe的面包的生物可及性分别为28.63%、30.14%和22.75%。面包中添加0.50%和1.00%的PBE也显著降低了pGI;因此,这些面包被归类为中等(pGI分别为66.28和59.29)血糖指数。TPC与抗氧化活性呈显著的线性相关。矿物质分析(mg/100 g)证实,在富含pbe的面包中存在必需的宏量元素(Ca [19.79-38.95], K [4.80-25.72], mg [5.78-12.38], Na[7.12-28.29])和微量元素(Zn [2.62-3.61], Cu [< 2.5], Fe [< 2.5], Mn [< 2.5])。质地分析表明,添加PBE后,面包的柔软度(304.43 ~ 394.09 N)与添加PBE成比例,而感官评价没有显示PBE的负面影响。总的来说,这些发现突出了PBE作为一种有价值的功能成分的潜力,可以提高烘焙产品的营养和技术特性。
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引用次数: 0
Recent Advances in Electronic Eye, Electronic Nose, and Electronic Tongue in Sensory Evaluation of Food: A Review 电子眼、电子鼻、电子舌在食品感官评价中的研究进展
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-15 DOI: 10.1111/jfpe.70281
Samuel Ayofemi Olalekan Adeyeye, Blessing Rachael Adeyeye

This study reviewed recent advances in electronic eye, electronic nose and electronic tongue in sensory evaluation of food. Significant progress has been made in using electronic eyes, noses, and tongues for objective food sensory evaluation, but research gaps include improving sensor technology for stability and selectivity, standardizing testing protocols, and developing more robust, low-cost portable devices. The novelty lies in the move from single-device applications to integrated, multisensory systems (e-nose, e-tongue, e-eye) that provide a more holistic and accurate picture of sensory properties. A novel approach is to combine the data from multiple artificial senses (electronic nose, tongue, and eye) to create a more comprehensive and reliable evaluation, often resulting in 8%–25% higher accuracy than a single instrument. The application of more advanced AI and machine learning techniques beyond traditional chemometrics like principal component analysis (PCA) will be a novel approach. This includes deep learning, neural networks, and specialized algorithms that can process high-dimensional sensor data more efficiently and accurately for tasks such as food authentication and quality prediction. Novel sensor designs, such as ratiometric electrochemical sensors, offer improved signal stability and noise cancelation. These dual-signal processing capabilities provide more accurate and reproducible measurements by internally correcting for background interference. Future outlooks point toward advanced data processing with deep learning, real-time online quality control in production, and a greater role in rapid food safety analysis. Although electronic senses are effective for many food types, their performance is still limited by complex food matrices. Factors like water vapor, high fat content, and complex volatile profiles can interfere with electronic nose sensors, requiring more research to enhance selectivity. While portable options exist, making electronic sensors affordable for widespread consumer and small-business use requires significant progress in cost-effective manufacturing and miniaturization. Incorporating biological recognition elements, such as enzymes and antibodies, into electronic sensor platforms allows for highly specific detection of complex analytes like pathogenic microorganisms and mycotoxins. The future will see electronic senses integrated into smart systems for real-time, remote monitoring throughout the food supply chain.

本文综述了电子眼、电子鼻和电子舌在食品感官评价中的最新进展。在使用电子眼、电子鼻和电子舌进行客观食物感官评估方面已经取得了重大进展,但研究差距包括提高传感器技术的稳定性和选择性,标准化测试协议,以及开发更坚固、低成本的便携式设备。新颖之处在于从单一设备应用到集成的多感官系统(电子鼻、电子舌、电子眼)的转变,这些系统提供了更全面、更准确的感官特性图像。一种新颖的方法是将来自多个人工感官(电子鼻、舌头和眼睛)的数据结合起来,以创建更全面、更可靠的评估,通常比单一仪器的准确度高8%-25%。除了主成分分析(PCA)等传统化学计量学之外,更先进的人工智能和机器学习技术的应用将是一种新颖的方法。这包括深度学习、神经网络和专门的算法,这些算法可以更有效、更准确地处理高维传感器数据,用于食品认证和质量预测等任务。新型传感器设计,如比例电化学传感器,提供了更好的信号稳定性和噪声消除。这些双信号处理能力通过内部校正背景干扰提供更准确和可重复的测量。未来的展望指向深度学习的先进数据处理,生产中的实时在线质量控制,以及在快速食品安全分析中发挥更大作用。虽然电子感官对许多食物类型都是有效的,但它们的性能仍然受到复杂食物基质的限制。水蒸气、高脂肪含量和复杂的挥发性特征等因素会干扰电子鼻传感器,需要更多的研究来提高选择性。虽然存在便携式选择,但要使电子传感器能够为广大消费者和小型企业使用,需要在成本效益制造和小型化方面取得重大进展。将酶和抗体等生物识别元素整合到电子传感器平台中,可以对病原微生物和真菌毒素等复杂分析物进行高度特异性的检测。未来将看到电子传感器集成到智能系统中,用于整个食品供应链的实时远程监控。
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引用次数: 0
Extended Release Ethyl Cellulose-Coated Eugenol-Loaded Puffed Rice Matrix for Quality Preservation of Dairy Sweets 缓释乙基纤维素包被负载丁香酚的膨化大米基质用于乳制品糖果的品质保存
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-15 DOI: 10.1111/jfpe.70298
Shipra Jha, Anupam Roy

Traditional dairy sweets are highly perishable due to their high moisture content (~36%), moderate pH (5.5–6.5), and nutrient-rich composition, which leads to rapid microbial spoilage. This study aimed to develop a natural, extended-release vapor-phase antimicrobial system using eugenol as an antimicrobial agent and an expanded porous starch matrix of puffed rice (EPSMPR) as a carrier matrix to preserve the quality of such perishable products. This study investigates the vapor-phase antimicrobial efficacy of eugenol and extends its applications as a food preservation option to extend the shelf life of dairy-based sweets through the development of an ethyl cellulose-coated eugenol-loaded EPSMPR (ELEPSMPR). Eugenol exhibited broad-spectrum vapor-phase antimicrobial activity against Gram-positive, Gram-negative, and fungal strains, with minimum inhibitory concentration, minimum bactericidal concentration, and minimum inhibitory dose values in the ranges of 0.195–1.56 μg/mL, 0.39–3.12 μg/mL, and 100–171.42 mL/L, respectively. ELEPSMPR was developed through the vacuum impregnation process (encapsulation efficiency 82.64%), and it offered sustained release of eugenol vapors (30.22% release at 36 h compared to 40% in the uncoated control sample). ELEPSMPR was placed on the top inner surface of rectangular storage packets (Kraft paper, volume 500 cm3) of dairy sweets, ensuring the eugenol release without direct product contact at ambient storage. The ELEPSMPR modified the headspace environment of the storage packets, effectively suppressing microbial growth while maintaining the physicochemical quality of dairy sweet—Sandesh (pH, moisture content, and lipid stability). The ELEPSMPR system represents a sustainable food preservation technology that can be a safe, natural, and contactless strategy for dairy sweets and similar foods.

传统的乳制品糖果由于其高水分含量(~36%),中等pH值(5.5-6.5)和丰富的营养成分,导致微生物迅速变质,因此极易变质。本研究旨在开发一种以丁香酚为抗菌剂,膨化大米膨胀多孔淀粉基质(EPSMPR)为载体基质的天然、缓释气相抗菌体系,以保持易腐烂产品的质量。本研究研究了丁香酚的气相抗菌效果,并通过开发乙基纤维素包被丁香酚负载的EPSMPR (ELEPSMPR),扩展了其作为食品保存选择的应用,以延长乳制品糖果的保质期。丁香酚对革兰氏阳性、革兰氏阴性和真菌均表现出广谱的气相抑菌活性,最小抑菌浓度、最小杀菌浓度和最小抑菌剂量分别在0.195 ~ 1.56 μg/mL、0.39 ~ 3.12 μg/mL和100 ~ 171.42 mL/L范围内。ELEPSMPR采用真空浸渍法制备,包封率为82.64%,具有良好的丁香酚蒸气缓释效果(36 h缓释率为30.22%,未包覆对照样品为40%)。ELEPSMPR放置在乳制品糖果的矩形存储包(牛皮纸,体积500 cm3)的顶部内表面,确保在环境储存中不直接接触产品的情况下释放丁香酚。ELEPSMPR修改了存储包的顶空环境,有效抑制微生物生长,同时保持乳制品甜味的理化品质(pH值、水分含量和脂质稳定性)。ELEPSMPR系统代表了一种可持续的食品保存技术,对于乳制品、糖果和类似的食品来说,这是一种安全、自然、无接触的策略。
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引用次数: 0
Comparative Assessment of Indirect Solar Dryer and Screw Conveyor-Based Solar Dryer During Drying Ivy Gourd: A Techno-Economic Analysis 间接太阳能干燥机与螺旋输送机太阳能干燥机在冬瓜干燥过程中的技术经济比较分析
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-12 DOI: 10.1111/jfpe.70296
R. Karthikeyan, P. Thangavel, P. Saji Raveendran

This experimental study compares the performance and cost-effectiveness of an indirect solar dryer (ISD) with a Screw Conveyor Based Solar Dryer (SBSD) used to dry ivy gourd. The drying procedure is followed at temperatures between 33°C and 49°C, with each dryer requiring 16 h to attain the necessary moisture reduction. Moreover, the average drying efficiency for ISD and SBSD is 7.82% and 7.48%, respectively. The final moisture content in ISD is measured at 8%, while SBSD is 15.97%, thereby demonstrating the superior moisture removal capabilities of ISD. Besides, the average drying rates of ISD and SBSD are 1.16 and 1.05 kg/h, respectively. The average heat supply of ISD and SBSD is determined to be 0.88 and 0.80 kW, respectively, with ISD providing 9.09% more heat than SBSD. The average mass transfer coefficient (hm) for ISD is 0.0049 m/s, while it is 0.0036 m/s for SBSD, showing that ISD has a 26.53% higher hm value. The specific energy consumption (SEC) values of SBSD and ISD are 0.931 and 0.924 kWh/kg, respectively. The Payback Period (PBP) for ISD is 2.16 and 7.45 years for SBSD, indicating a faster return on investment for ISD. Therefore, from the study, the findings show that the ISD has improved the drying efficiency, energy utilization, and economic feasibility for small-scale farmers in rural areas.

本实验研究比较了间接太阳能干燥机(ISD)与螺旋输送机太阳能干燥机(SBSD)用于干燥常青藤葫芦的性能和成本效益。干燥过程在33°C和49°C之间的温度下进行,每个干燥机需要16小时才能达到必要的减湿。ISD和SBSD的平均干燥效率分别为7.82%和7.48%。ISD的最终含水率为8%,而SBSD的最终含水率为15.97%,可见ISD具有较好的除湿能力。ISD和SBSD的平均干燥速率分别为1.16和1.05 kg/h。确定了ISD和SBSD的平均发热量分别为0.88和0.80 kW,其中ISD比SBSD多出9.09%的热量。ISD的平均传质系数(hm)为0.0049 m/s,而SBSD的平均传质系数(hm)为0.0036 m/s,表明ISD的hm值高出26.53%。SBSD和ISD的比能耗(SEC)值分别为0.931和0.924 kWh/kg。ISD的投资回收期(PBP)为2.16年,SBSD为7.45年,表明ISD的投资回报更快。因此,从研究结果来看,ISD提高了农村小农的干燥效率、能源利用率和经济可行性。
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引用次数: 0
Development of Milk Quality Index and Its Prediction Using Regression and Artificial Neural Network Approach 基于回归和人工神经网络方法的牛奶品质指标及其预测研究
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-12 DOI: 10.1111/jfpe.70287
Suruthi Muthusamy, Chandrasekar Veerapandian, Subhasri Dharmaraj, Eyarkai Nambi Vijayaram

Milk is one of the nutritious foods consumed regularly by people. It is highly perishable and prone to spoilage quickly after milking from animals. The study aimed to develop a Milk Quality Index (MQI) comprising physicochemical, microbiological, and volatile parameters and to create a predictive model based on this index for evaluating milk quality. In this study, milk was stored for 0–240 min, and its physicochemical properties (fat, SNF, protein, lactose, density, color, and pH), microbial analysis (MBRT and TPC), and volatile compounds were assessed using an E-nose at 30-min intervals. The major volatile compounds responsible for spoilage were identified using the Partial Least Squares regression—Variable Importance in Projection method. Furthermore, Principal Component Analysis was performed on physicochemical, microbial, and volatile compounds obtained from the VIP score to group the milk samples based on spoilage. The MQI was developed for grouped milk samples and found that an MQI ≤ 3.0 indicates a fresh sample, an MQI between 3 and 6 indicates the beginning of spoilage and requires heat treatment for consumption, and an MQI ≥ 6 indicates spoiled. Multiple linear regression and Artificial Neural Network models were developed by relating physicochemical and microbial analysis to MQI to predict milk quality. This study provides insight into the development of MQI models for real-time milk spoilage prediction and decision-making in the dairy industry.

牛奶是人们经常食用的营养食品之一。它极易腐烂,从动物身上挤奶后很快就会变质。本研究旨在建立由理化、微生物学和挥发性参数组成的牛奶品质指数(MQI),并建立基于该指数的牛奶品质评价预测模型。在本研究中,将牛奶储存0-240分钟,并每隔30分钟使用电子鼻评估其理化性质(脂肪、SNF、蛋白质、乳糖、密度、颜色和pH)、微生物分析(MBRT和TPC)和挥发性化合物。采用偏最小二乘回归-变量重要性投影法确定了主要挥发性变质化合物。此外,对VIP评分获得的理化、微生物和挥发性化合物进行主成分分析,根据腐败程度对牛奶样品进行分组。对分组牛奶样品开发了MQI,发现MQI≤3.0表示新鲜样品,MQI在3到6之间表示开始变质,需要热处理才能食用,MQI≥6表示变质。将理化和微生物分析与MQI相关联,建立多元线性回归和人工神经网络模型来预测牛奶品质。本研究为乳品行业实时牛奶变质预测和决策的MQI模型的发展提供了见解。
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引用次数: 0
The Detailed Comparison of the Effect of Optimum Thermosonication and Potash Solution Pretreatments on Quality Attributes of Dried Black Grapes 最佳热超声处理和钾盐溶液预处理对黑葡萄干品质特性影响的详细比较
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-11 DOI: 10.1111/jfpe.70290
Erdal Ağçam, Burcu Dündar Kırıt, Asiye Akyildiz

This study evaluated the impact of optimized thermosonication pretreatment (UT) (743.1 J/g, 16.6°C) on the physical and chemical quality of dried black grapes, comparing it with the traditional potash treatment. Dried grapes showed high dry matter (89.53%–91.41%) and controlled water activity (0.415–0.467), with significant changes in color parameters. Thermosonication pretreatment significantly reduced rehydration capacity, unlike potash. Potash increased sucrose content and negatively impacted fructose, while UT significantly reduced sucrose. UT-treated samples retained the highest organic acid contents and exhibited the lowest HMF and furfural contents, demonstrating an advantage over potash in minimizing these undesirable compounds. Potash enhanced total phenolic content (TPC) and total monomeric anthocyanin content (TMAC), whereas UT only increased antioxidant activity. Untreated control samples generally scored highest in sensory attributes, particularly appearance and overall acceptability. This research indicates that optimized thermosonication offers specific benefits like HMF/furfural reduction and organic acid preservation, though its overall quality impact varies compared to conventional treatments.

本研究评价了优化后的热超声预处理(UT) (743.1 J/g, 16.6℃)对黑葡萄干理化品质的影响,并与传统的钾肥处理进行了比较。干葡萄干物质含量高(89.53% ~ 91.41%),水分活性受控(0.415 ~ 0.467),颜色参数变化显著。与钾肥不同,热超声预处理显著降低了再水化能力。钾肥增加了蔗糖含量并对果糖产生负面影响,而UT显著降低了蔗糖含量。ut处理的样品保留了最高的有机酸含量,并表现出最低的HMF和糠醛含量,在减少这些不需要的化合物方面显示出比钾肥的优势。钾肥提高了总酚含量(TPC)和总单体花青素含量(TMAC),而UT仅提高了抗氧化活性。未经处理的对照样品通常在感官属性,特别是外观和整体可接受性方面得分最高。这项研究表明,优化的热超声处理具有特定的好处,如HMF/糠醛还原和有机酸保存,尽管其整体质量影响与传统处理相比有所不同。
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引用次数: 0
Detection of Peanut Contamination in Wheat Flour Using a Digital Light Processing (DLP) Based Near-Infrared Spectrometer and Ensemble Machine Learning 基于数字光处理(DLP)的近红外光谱仪和集成机器学习检测小麦粉中的花生污染
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-10 DOI: 10.1111/jfpe.70286
Siva Peddareddigari, Sindhu Chaudhary, Annamalai Manickavasagan

Peanut flour contamination poses significant health and regulatory challenges within food production systems, often originating from adulterated raw materials or cross-contamination during processing. Rapid and non-destructive detection methods are essential for real-time monitoring and mitigation. This study aimed to develop a non-destructive detection system using a portable digital light processing (DLP) based near-infrared (NIR) spectrometer integrated with machine learning (ML) models to identify and quantify peanut adulteration in wheat flour. Samples were systematically prepared by blending wheat flour with peanut flour at six contamination levels: 0%, 2%, 4%, 6%, 8%, and 10% (w/w). Spectral data were acquired using a handheld DLP-NIR device operating in the 900–1700 nm range. Due to limited separability among contamination levels, a binary classification framework was adopted to distinguish pure wheat flour (0%) from contaminated samples (≥ 2%) using models such as Linear Discriminant Analysis, Logistic Regression, and boosted tree ensembles. Regression models including Extra Trees, Random Forest, and LightGBM were trained to estimate contamination levels. Spectral preprocessing involved normalization and Yeo-Johnson transformation, while model evaluation employed stratified K-fold cross-validation with Optuna-based hyperparameter tuning. The top five performing classifiers were selected for ensemble learning to enhance predictive performance. The final ensemble classifier achieved accuracy, precision, recall, and F1-score values of 0.9937, 0.9976, 0.9948, and 0.9962, respectively. Ensemble regressors yielded R2 = 0.7477, RMSE = 1.7157, and MAE = 1.148, demonstrating promising semi-quantitative estimation capabilities. These results highlight the feasibility of combining portable NIR spectroscopy with ensemble ML for rapid, in-line detection of peanut contamination in wheat flour.

花生粉污染对食品生产系统的健康和监管构成重大挑战,通常源于掺假的原材料或加工过程中的交叉污染。快速和非破坏性检测方法对于实时监测和缓解至关重要。本研究旨在开发一种基于便携式数字光处理(DLP)的近红外(NIR)光谱仪与机器学习(ML)模型相结合的无损检测系统,以识别和定量小麦粉中的花生掺假。通过将小麦粉与花生粉混合,在6种污染水平(0%、2%、4%、6%、8%和10% (w/w))下系统制备样品。光谱数据是使用手持式DLP-NIR设备在900-1700 nm范围内获得的。由于污染水平之间的可分性有限,采用二元分类框架,使用线性判别分析、逻辑回归和增强树集成等模型来区分纯小麦粉(0%)和污染样品(≥2%)。包括Extra Trees、Random Forest和LightGBM在内的回归模型被训练来估计污染水平。光谱预处理包括归一化和Yeo-Johnson变换,而模型评估采用分层K-fold交叉验证和基于optuna的超参数调谐。选择表现最好的五个分类器进行集成学习以提高预测性能。最终的集成分类器的准确率、精密度、召回率和f1得分分别为0.9937、0.9976、0.9948和0.9962。集合回归得到R2 = 0.7477, RMSE = 1.7157, MAE = 1.148,显示出有希望的半定量估计能力。这些结果强调了将便携式近红外光谱与集合ML相结合用于快速、在线检测小麦粉中花生污染的可行性。
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引用次数: 0
Kinetic and Thermodynamic Studies of Yacon Juice Extraction Under Thermosonication Treatment 热超声法提取雪莲汁的动力学和热力学研究
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-09 DOI: 10.1111/jfpe.70293
Puja Das, Prakash Kumar Nayak, Radha krishnan Kesavan

Building on previous research that optimized thermosonication (TS) conditions to enhance the functional compounds of yacon (Smallanthus sonchifolius) tuber juice, this study explores the underlying extraction kinetics and thermodynamic mechanisms governing the process. Following the determination of optimal TSYJ processing parameters using the integrated ANN-GA model (50% amplitude, 40°C, and 45 min), responses were evaluated across a temperature range of 30°C–50°C, with measurements recorded at 5-min intervals during sonication. By evaluating the release patterns of functional compounds such as total phenolic content (TPC), total flavonoid content (TFC), antioxidant activity (AOA), ascorbic acid (AA), and total carotenoid content (TCC), the study applies kinetic modeling to identify the most suitable mathematical fit. The pseudo second-order model was identified as the most suitable model with the highest R2 (0.999) and lower χ2 (0.072) value obtained for all five responses. Additionally, key thermodynamic parameters, including activation energy (Ea: 24.89–28.23), enthalpy (ΔH: 14.86–27.44 kJ/mol), entropy (ΔS: 22.27–58.42 J/mol·K), and Gibbs free energy (ΔG: −6.73 to 18.86 kJ/mol), were obtained to understand the energy requirements and feasibility of thermosonication-assisted extraction.

本研究在优化热超声(TS)条件以提高雪莲块茎汁中功能化合物含量的基础上,探讨了热超声提取过程的动力学和热力学机制。在使用集成的ANN-GA模型(50%振幅,40°C和45分钟)确定最佳TSYJ处理参数后,在30°C - 50°C的温度范围内评估响应,并在超声期间每隔5分钟记录一次测量结果。通过评价总酚含量(TPC)、总黄酮含量(TFC)、抗氧化活性(AOA)、抗坏血酸(AA)和总类胡萝卜素含量(TCC)等功能化合物的释放模式,应用动力学模型确定最合适的数学拟合。伪二阶模型是最合适的模型,5个响应的R2最高(0.999),χ2最低(0.072)。此外,还获得了关键热力学参数,包括活化能(Ea: 24.89 ~ 28.23)、焓(ΔH: 14.86 ~ 27.44 kJ/mol)、熵(ΔS: 22.27 ~ 58.42 J/mol·K)和吉布斯自由能(ΔG:−6.73 ~ 18.86 kJ/mol),以了解热超声辅助提取的能量需求和可行性。
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引用次数: 0
Unraveling the Interplay: Nutrigenomics in Gut Microbiome 揭示相互作用:肠道微生物组的营养基因组学
IF 2.9 3区 农林科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2025-12-09 DOI: 10.1111/jfpe.70278
Sankarganesh Palaniyandi, Adeyeye Samuel Ayofemi Olalekan, Sumit Kumar Rawat, Prem Shankar Pandey

The human gut microbiome plays a crucial role in synthesizing immune-modulating metabolites, such as short-chain fatty acids (SCFAs), which offer multiple health benefits, including fuelling gut cells and modulating the immune system. Individual variations in nutrition, diet, and genetics significantly influence the body's response to various foods, affecting digestion, absorption, and metabolism processes. These factors, in turn, impact the accessibility of nutrients to the gut microbiota. Recent studies have elucidated diet-microbiome interaction mechanisms, demonstrating how gut microbiota respond to dietary changes, with specific nutrients selectively promoting the growth of certain microbial species. The emerging field of nutrigenomics examines the effects of genetic variants on nutritional responses, eating habits, and overall health. This discipline enhances our understanding of how diet influences the composition and activities of gut microbes. The interplay between genes, gut microbiomes, and host physiology forms a complex, highly interconnected network. Nutrigenomics research focuses on personalized nutrition, aiming to develop diets tailored to an individual's genetic profile and gut bacterial composition. This approach may unlock potential treatments for metabolically associated disorders in the future. This research aims to explore the role of nutrigenomics in identifying genetic variables that influence an individual's susceptibility to certain illnesses and how dietary choices can modulate these risks through interactions with the gut flora. Additionally, the review addresses the challenges associated with microbial dynamics, ethical and privacy concerns, and practical applications of this emerging field.

人体肠道微生物群在合成免疫调节代谢物方面起着至关重要的作用,如短链脂肪酸(SCFAs),它提供多种健康益处,包括为肠道细胞提供能量和调节免疫系统。营养、饮食和遗传的个体差异显著影响身体对各种食物的反应,影响消化、吸收和代谢过程。这些因素反过来又影响营养物质对肠道微生物群的可及性。最近的研究已经阐明了饮食与微生物群相互作用的机制,展示了肠道微生物群如何对饮食变化做出反应,特定的营养物质选择性地促进某些微生物物种的生长。营养基因组学这一新兴领域研究基因变异对营养反应、饮食习惯和整体健康的影响。这门学科增强了我们对饮食如何影响肠道微生物组成和活动的理解。基因、肠道微生物群和宿主生理之间的相互作用形成了一个复杂的、高度互联的网络。营养基因组学研究的重点是个性化营养,旨在开发适合个人遗传特征和肠道细菌组成的饮食。这种方法可能在未来开启代谢相关疾病的潜在治疗方法。这项研究旨在探索营养基因组学在确定影响个体对某些疾病易感性的遗传变量方面的作用,以及饮食选择如何通过与肠道菌群的相互作用来调节这些风险。此外,该综述还讨论了与微生物动力学、伦理和隐私问题以及这一新兴领域的实际应用相关的挑战。
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引用次数: 0
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Journal of Food Process Engineering
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