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Comparative evaluation of mechanical properties between dual-layer and bonded three-dimensional printed denture base materials: An in vitro study. 双层与粘结三维打印义齿基托材料力学性能的体外比较研究。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2026-01-01 DOI: 10.4103/jips.jips_403_25
Naveen Gopi Chander, Aryan Shivaji Deshmukh, Harini Gnana Prakash, Vigneshvar Kandaswamy Srinivasan

Aim: The study aimed to compare the flexural strength, fracture toughness, and impact strength of the denture base materials fabricated using dual-layer and bonded 3D printing techniques.

Settings and design: In vitro comparative study.

Materials and methods: Seventy-two bar-shaped samples were fabricated using a digital light processing 3D printer and were divided into 2 groups (n = 36 each). Group I samples were fabricated by dual-layer technique, with the denture base and tooth-colored resins were printed sequentially in a single print cycle. Group II samples were printed separately and bonded with denture base resin. Flexural strength and fracture toughness were tested according to ISO 20795-1:2013, and impact strength was evaluated using ASTM D-256.Statistical Analysis Used: Statistical analysis comprised Shapiro-Wilk for normality, t-test for flexural strength, and Mann-Whitney U-test for fracture toughness and impact strength (α = 0.05).

Results: Group I exhibited significantly higher flexural strength (82.78 ± 2.02 MPa) and fracture toughness (89.91 ± 0.53 MPa) compared to Group II (80.01 ± 2.69 MPa and 86.93 ± 2.29 MPa, respectively). Conversely, impact strength was greater in Group II (4.17 ± 0.39 J) than in Group I (3.00 ± 1.04 J) (P < .05).

Conclusion: The dual-layer printing technique improved the flexural and fracture resistance of denture base materials by eliminating interfacial weaknesses. Although bonded resins exhibited higher impact strength, the structural advantages of dual-printing support its application in clinical prosthodontics.

目的:比较采用双层和粘结3D打印技术制备的义齿基托材料的弯曲强度、断裂韧性和冲击强度。设置和设计:体外比较研究。材料与方法:采用数字光处理3D打印机制作72个条形样品,分为2组,每组36个。第一组采用双层打印技术,在一个打印周期内依次打印义齿基托和牙色树脂。第二组样品单独打印,与义齿基托树脂粘接。弯曲强度和断裂韧性按照ISO 20795-1:2013进行测试,冲击强度按照ASTM D-256进行评估。统计学方法:正态性采用Shapiro-Wilk检验,弯曲强度采用t检验,断裂韧性和冲击强度采用Mann-Whitney u检验(α = 0.05)。结果:ⅰ组的抗折强度(82.78±2.02 MPa)和断裂韧性(89.91±0.53 MPa)明显高于ⅱ组(80.01±2.69 MPa和86.93±2.29 MPa)。相反,II组的冲击强度(4.17±0.39 J)大于I组(3.00±1.04 J) (P < 0.05)。结论:双层打印技术通过消除界面缺陷,提高了义齿基托材料的抗折性和抗折性。虽然结合树脂具有较高的冲击强度,但双打印的结构优势支持其在临床修复中的应用。
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引用次数: 0
Survival rate of immediate functionally loaded ball-attachment mini-implants retaining mandibular overdentures: A systematic review. 即时功能负荷球附着型微型种植体固位下颌覆盖义齿的存活率:一项系统回顾。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2026-01-01 DOI: 10.4103/jips.jips_361_25
Heba M Moftah, Mohannad H Al-Saadi

Aim: Immediate loading protocols are frequently applied when placing mini-implants (MIs), although many of these may not be functional loading. Data on immediately functionally loaded MIs are limited. Therefore, this systematic review aimed to answer the question: What is the survival rate (SR) of immediately functionally loaded MIs placed in the edentulous mandible to retain a complete mandibular overdenture?

Settings and design: Studies published in peer-reviewed journals up to April 2025 were considered.

Material and methods: An electronic search was conducted using MeSH terms and free-text search in April 2025 across Web of Science, PubMed, Cochrane Central, EBSCOhost, and ScienceDirect. Eligible criteria included case-control studies, retrospective and prospective case series, cohort studies, clinical trials, and randomized controlled trials.

Statistical analysis used: Not applicable.

Results: Out of 1854 identified references, seven studies met the inclusion criteria, three randomized controlled and four prospective case series. A total of 496 immediately functionally loaded MIs were placed in 124 patients. The diameters of MIs were 1.8, 2.0, 2.1, 2.2, and 2.4 mm. Within the 1st year, 16 out of 495 MIs failed, resulting in a 1-year SR of 96.77%. A 24-month SR of 94.4% was reported by three studies, and a 36-month rate of 94.77% was reported by two studies.

Conclusions: Current evidence indicates that immediately functionally loaded MIs are a promising option for retaining mandibular overdentures, with a high 1-year SR of 96.77%. However, the limited number of included studies and relatively short follow-up periods highlight the need for further well-designed, long-term research to validate these findings.

目的:在放置微型植入物(MIs)时,经常采用即时加载协议,尽管其中许多可能不是功能性加载。立即功能加载的mi上的数据是有限的。因此,本系统综述旨在回答这个问题:在无牙下颌骨放置立即功能加载的MIs以保留完整的下颌覆盖义齿的存活率(SR)是多少?环境和设计:考虑到2025年4月之前在同行评审期刊上发表的研究。材料和方法:于2025年4月在Web of Science、PubMed、Cochrane Central、EBSCOhost和ScienceDirect上使用MeSH术语和自由文本检索进行电子检索。入选标准包括病例对照研究、回顾性和前瞻性病例系列研究、队列研究、临床试验和随机对照试验。使用的统计分析:不适用。结果:在1854篇文献中,7篇研究符合纳入标准,3篇随机对照研究和4篇前瞻性病例研究。124名患者共植入了496个立即功能加载的MIs。直径分别为1.8、2.0、2.1、2.2和2.4 mm。在第一年,495名MIs中有16名失败,导致1年SR为96.77%。3项研究报告了24个月的SR为94.4%,2项研究报告了36个月的SR为94.77%。结论:目前的证据表明,即刻功能加载的MIs是下颌覆盖义齿固位的一种很有希望的选择,其1年的SR高达96.77%。然而,纳入的研究数量有限,随访期相对较短,因此需要进一步精心设计的长期研究来验证这些发现。
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引用次数: 0
Evaluation of wear resistance in 3D printed temporary restorative material using two different printing technologies" - An in vitro study. 使用两种不同的打印技术评估3D打印临时修复材料的耐磨性”——一项体外研究。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2026-01-01 DOI: 10.4103/jips.jips_305_25
Srilekha Daripalli, Mahendranadh Reddy Kareti, Y Mahadev Shastry, S Venkat Aditya, Sai Akhil Khadkekar, Divya Dubey

Aim: This study aimed to assess and compare the wear resistance of 3D printable crown and bridge interim resin material with two different 3D printers.

Settings and design: In vitro comparative study.

Materials and methods: 60 specimens were divided into 2 groups and designed using nx12 (Unigraphics) software. This Standard Tessellation Language file was used to print the specimens. Specimens fabricated using Phrozen Sonic Mini 3D printer of LCD software were grouped as Group A (n = 30), and specimens fabricated using Asiga Max 3D printer of DLP software were grouped as Group B (n = 30). Surface micro roughness measurements (Ra) were noted with a profilometer prior to and following toothbrush wear simulation. The collected data were tabulated to facilitate statistical analysis.

Statistical analysis used: Student's t-test and Mann-Whitney U-test was employed for multiple comparisions.

Results: The Student's t-test was employed to compare the mean surface micro-roughness of Group A and Group B specimens before and after toothbrush wear simulation. The test indicated that there was no significant difference.

Conclusion: Within the scope of this study, both groups underwent wear and were statistically insignificant.

目的:通过两种不同的3D打印机,评估和比较3D打印冠桥中间树脂材料的耐磨性。设置和设计:体外比较研究。材料与方法:60例标本分为2组,采用nx12 (Unigraphics)软件进行设计。这个标准镶嵌语言文件用于打印标本。采用LCD软件的Phrozen Sonic Mini 3D打印机制作的标本作为A组(n = 30),采用DLP软件的Asiga Max 3D打印机制作的标本作为B组(n = 30)。在牙刷磨损模拟之前和之后,用轮廓仪记录表面微粗糙度测量(Ra)。收集到的数据被制成表格,以便于统计分析。采用统计学分析:多重比较采用Student’st检验和Mann-Whitney u检验。结果:采用Student’st检验比较A组和B组牙体在牙刷磨损模拟前后的平均表面微粗糙度。经检验无显著性差异。结论:在本研究范围内,两组患者均出现磨损,差异无统计学意义。
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引用次数: 0
Effect of build position on the accuracy and flexural properties of resin model materials for three-dimensional printing technologies. 构建位置对三维打印树脂模型材料精度和弯曲性能的影响。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2026-01-01 DOI: 10.4103/jips.jips_106_25
Xiao-Mei Tang, Na-Yu, Bin-Ding Bai, Peng-Wang, Lu-Liu, Fa-Bing Tan

Aim: This study aimed to evaluate the effects of build position (rows or columns) on the accuracy and flexural properties of three-dimensional printing resin model materials.

Settings and design: This was a comparative experimental study.

Materials and methods: Three additive manufacturing technologies - digital light processing (DLP), stereolithography (SLA), and polymer jetting printing (PJP) - were employed to fabricate resin model specimens (2 mm × 2 mm × 25 mm), arranged evenly in 7 rows and 7 columns on the build platform. Dimensional trueness was assessed by measuring deviations in length (X-axis), width (Y-axis), and height (Z-axis) using a digital micrometer. Triplicate printing runs were performed to determine precision, quantified using intraclass correlation coefficient analysis. Flexural properties were evaluated through three-point bending tests.

Statistical analysis used: Data were analyzed using one-way ANOVA followed by Tukey post hoc tests.

Results: The PJP group exhibited deviations in length (0.18-0.25 mm) and height (0.18-0.22 mm) at several column positions, exceeding 0.1 mm, whereas the DLP and SLA groups showed deviations in all dimensions within 0.1 mm. At different row positions, PJP length (0.20-0.24 mm) and height (0.17-0.22 mm) deviations also exceeded 0.1 mm. Precision in height was lower than in length or width across both rows and columns (P = 0.000). Compared with the DLP and PJP groups, the SLA group demonstrated larger deviations in flexural modulus at column positions (P = 0.003, H = 19.730) and greater variations (95% confidence interval) in flexural strength and modulus at column and row positions.

Conclusion: Build position had a greater influence on trueness in the PJP group, while precision was lowest for height across all three groups. Furthermore, the flexural strength and modulus of the SLA group varied more significantly with build position. Thus, meticulous selection of the build position is essential to achieve improved accuracy and flexural properties in resin models.

目的:本研究旨在评估构建位置(行或列)对三维打印树脂模型材料精度和弯曲性能的影响。环境与设计:本研究为比较实验研究。材料和方法:采用数字光处理(DLP)、立体光刻(SLA)和聚合物喷射打印(PJP)三种增材制造技术制作树脂模型标本(2mm × 2mm × 25mm),在构建平台上均匀排列7排7列。通过使用数字千分尺测量长度(x轴),宽度(y轴)和高度(z轴)的偏差来评估尺寸真实性。进行三次印刷以确定精密度,用类内相关系数分析进行量化。通过三点弯曲试验评估弯曲性能。采用统计分析:数据分析采用单因素方差分析,随后采用Tukey事后检验。结果:PJP组在多个柱位出现长度偏差(0.18 ~ 0.25 mm)和高度偏差(0.18 ~ 0.22 mm),偏差均超过0.1 mm,而DLP组和SLA组在各维度的偏差均在0.1 mm以内。不同排位的PJP长度(0.20 ~ 0.24 mm)和高度(0.17 ~ 0.22 mm)偏差均超过0.1 mm。高度的精度低于行和列的长度或宽度(P = 0.000)。与DLP和PJP组相比,SLA组在柱位置的弯曲模量偏差更大(P = 0.003, H = 19.730),柱和行位置的弯曲强度和模量变化更大(95%置信区间)。结论:在PJP组中,体位对准确率的影响较大,而身高对准确率的影响最低。此外,SLA组的抗弯强度和模量随构建位置的变化更为显著。因此,精心选择的构建位置是必不可少的,以实现提高精度和弯曲性能的树脂模型。
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引用次数: 0
Effect of cathodic arc plasma spraying on shear bond strength between polyether ether ketone and maxillofacial silicone after accelerated aging - An in vitro study. 阴极电弧等离子喷涂对加速老化后聚醚醚酮与颌面硅胶剪切结合强度的影响——体外研究。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-10-01 Epub Date: 2025-10-20 DOI: 10.4103/jips.jips_203_25
Ganesh Ramkumar Rajapandi, Ahila Singaravel Chidambaranathan, Muthukumar Balasubramanium

Aim: To evaluate and compare the shear bond strength between polyether ether ketone (PEEK) and maxillofacial silicone after cathodic arc plasma spraying and accelerated aging.

Settings and design: An in vitro study.

Materials and methods: According to ISO 10477:2020, 72 PEEK specimens were fabricated using computer-aided design/computer-aided manufacturing with 10-mm diameter and 3-mm thickness, and the silicone specimens were made with 5-mm diameter with 2.5-mm height. The specimens were categorized into Group 1 - No surface treatment, Group 2 - Cathodic arc plasma spraying, and Group 3 - Primer application. The silicone specimens were bonded to PEEK and subjected to accelerated aging for 252 and 504 h. The shear bond strength was performed using a universal testing machine at 1 mm/min crosshead speed.

Statistical analysis used: One-way ANOVA, Tukey HSD test, and Student's t-test, where P < 0.5 was set as significant.

Results: PEEK specimens subjected to primer application exhibited highest shear bond strength of 19.22 ± 0.35 Mpa, 18.55 ± 0.60 Mpa, 18.14 ± 0.65 Mpa, followed by cathodic arc plasma spraying 14.71 ± 0.28 Mpa, 13.54 ± 0.42 Mpa, 12.46 ± 0.48 Mpa after 24 h of fabrication, 252 h, and 504 h of aging and the least shear bond strength exhibited by control 4.98 ± 0.32, Mpa, 4.52 ± 0.33 Mpa, 4.2 ± 0.39 Mpa, respectively. The significance value P = 0.0001, which was <0.05. Hence, the results were found to be statistically significant.

Conclusion: The maximum shear bond strength between PEEK and maxillofacial silicone was seen after primer application, followed by cathodic arc plasma surface treatment. Increasing the aging hours from 252 to 504 h, the shear bond strength was relatively reduced between PEEK and maxillofacial silicone.

目的:评价和比较聚醚醚酮(PEEK)与颌面部硅胶经阴极电弧等离子喷涂和加速老化后的剪切结合强度。设置和设计:一项体外研究。材料与方法:根据ISO 10477:2020,采用计算机辅助设计/计算机辅助制造方法制作72个直径为10mm、厚度为3mm的PEEK试件,制作直径为5mm、高度为2.5 mm的硅胶试件。试样分为三组,第一组为无表面处理,第二组为阴极电弧等离子喷涂,第三组为底漆。将硅胶试件与PEEK粘结,分别进行252和504 h的加速老化。在万能试验机上以1 mm/min的十字速度进行剪切粘结强度测试。统计分析采用单因素方差分析、Tukey HSD检验和学生t检验,其中P < 0.5为显著性。结果:涂底漆的PEEK试样在制备24 h、时效252 h和504 h后的剪切强度最高,分别为19.22±0.35 Mpa、18.55±0.60 Mpa和18.14±0.65 Mpa,阴极电弧等离子喷涂次之,分别为14.71±0.28 Mpa、13.54±0.42 Mpa、12.46±0.48 Mpa,对照组的剪切强度最低,分别为4.98±0.32 Mpa、4.52±0.33 Mpa和4.2±0.39 Mpa。结论:聚醚醚酮与颌面部有机硅的剪切结合强度在涂底漆后最大,其次为阴极电弧等离子体表面处理。老化时间从252小时增加到504小时,PEEK与颌面硅胶的剪切结合强度相对降低。
{"title":"Effect of cathodic arc plasma spraying on shear bond strength between polyether ether ketone and maxillofacial silicone after accelerated aging - An in vitro study.","authors":"Ganesh Ramkumar Rajapandi, Ahila Singaravel Chidambaranathan, Muthukumar Balasubramanium","doi":"10.4103/jips.jips_203_25","DOIUrl":"https://doi.org/10.4103/jips.jips_203_25","url":null,"abstract":"<p><strong>Aim: </strong>To evaluate and compare the shear bond strength between polyether ether ketone (PEEK) and maxillofacial silicone after cathodic arc plasma spraying and accelerated aging.</p><p><strong>Settings and design: </strong>An in vitro study.</p><p><strong>Materials and methods: </strong>According to ISO 10477:2020, 72 PEEK specimens were fabricated using computer-aided design/computer-aided manufacturing with 10-mm diameter and 3-mm thickness, and the silicone specimens were made with 5-mm diameter with 2.5-mm height. The specimens were categorized into Group 1 - No surface treatment, Group 2 - Cathodic arc plasma spraying, and Group 3 - Primer application. The silicone specimens were bonded to PEEK and subjected to accelerated aging for 252 and 504 h. The shear bond strength was performed using a universal testing machine at 1 mm/min crosshead speed.</p><p><strong>Statistical analysis used: </strong>One-way ANOVA, Tukey HSD test, and Student's t-test, where P < 0.5 was set as significant.</p><p><strong>Results: </strong>PEEK specimens subjected to primer application exhibited highest shear bond strength of 19.22 ± 0.35 Mpa, 18.55 ± 0.60 Mpa, 18.14 ± 0.65 Mpa, followed by cathodic arc plasma spraying 14.71 ± 0.28 Mpa, 13.54 ± 0.42 Mpa, 12.46 ± 0.48 Mpa after 24 h of fabrication, 252 h, and 504 h of aging and the least shear bond strength exhibited by control 4.98 ± 0.32, Mpa, 4.52 ± 0.33 Mpa, 4.2 ± 0.39 Mpa, respectively. The significance value P = 0.0001, which was <0.05. Hence, the results were found to be statistically significant.</p><p><strong>Conclusion: </strong>The maximum shear bond strength between PEEK and maxillofacial silicone was seen after primer application, followed by cathodic arc plasma surface treatment. Increasing the aging hours from 252 to 504 h, the shear bond strength was relatively reduced between PEEK and maxillofacial silicone.</p>","PeriodicalId":22669,"journal":{"name":"The Journal of Indian Prosthodontic Society","volume":"25 4","pages":"305-311"},"PeriodicalIF":1.0,"publicationDate":"2025-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145329797","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
In vitro evaluation of the dispersion of nano-polylactic acid and nano-zinc oxide fillers in denture base resins using spectroscopic modalities. 用光谱方法体外评价纳米聚乳酸和纳米氧化锌填料在义齿基托树脂中的分散性。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-10-01 Epub Date: 2025-10-20 DOI: 10.4103/jips.jips_142_25
Nikita Parasrampuria, N Gopi Chander, Jayanta Chattopadhyay

Aim: Polymethyl methacrylate (PMMA) is a widely used denture base material, but its mechanical and antimicrobial properties require further improvement to the diverse clinical situations. Nanoparticles such as zinc oxide (ZnO) and polylactic acid (PLA) offer promising enhancements through improved structural and functional integration. The aim of the study was to assess the molecular characterization and structural integration of PMMA modified with nano-ZnO and nano-PLA.

Settings and design: This was an in vitro material characterization study.

Materials and methods: Forty samples were fabricated and divided into two groups: control (n = 20, unmodified PMMA) and test (n = 20, PMMA reinforced with 10% nano-PLA and 3% ZnO). A high-shear mixing technique was used. Molecular interactions were evaluated using Fourier-transform infrared spectroscopy (FTIR), and energy-dispersive X-ray spectroscopy (EDS) estimated the nanoparticle dispersion and elemental composition.

Statistical analysis used: Qualitative analysis was used for statistical analysis.

Results: FTIR confirmed the inclusion of nano-PLA and nano-ZnO, with a broad absorption peak at 3500 cm-1 indicating increased polarity and hydrogen bonding. EDS analysis verified the presence of carbon, oxygen, and zinc, with uniform nanoparticle dispersion. Nano-PLA addition reduced crystallinity and nano-ZnO promoted crystal formation, indicating their functions in structural modification.

Conclusion: The study confirmed molecular interactions and uniform elemental dispersion, with indications of reduced crystallinity. These findings suggest potential for further investigations into the mechanical and antimicrobial properties of this modified resin for clinical applications.

目的:聚甲基丙烯酸甲酯(PMMA)是一种广泛应用的义齿基托材料,但由于临床情况的多样化,其力学性能和抗菌性能有待进一步提高。纳米颗粒如氧化锌(ZnO)和聚乳酸(PLA)通过改善结构和功能集成提供了有希望的增强。研究了纳米氧化锌和纳米聚乳酸改性PMMA的分子特性和结构集成度。设置和设计:这是一项体外材料表征研究。材料和方法:制作40个样品,分为对照组(n = 20,未改性PMMA)和试验组(n = 20,添加10%纳米pla和3% ZnO的PMMA)。采用了高剪切混合技术。利用傅里叶变换红外光谱(FTIR)评估分子相互作用,利用能量色散x射线光谱(EDS)评估纳米颗粒的色散和元素组成。采用的统计分析:采用定性分析进行统计分析。结果:FTIR证实了纳米pla和纳米zno的包合,在3500 cm-1处有一个宽的吸收峰,表明极性和氢键增强。能谱分析证实了碳、氧和锌的存在,纳米颗粒分散均匀。纳米pla的加入降低了结晶度,纳米zno的加入促进了晶体的形成,说明了纳米pla在结构修饰中的作用。结论:该研究证实了分子相互作用和均匀的元素分散,具有结晶度降低的迹象。这些发现为进一步研究这种改性树脂的机械和抗菌性能提供了潜在的临床应用。
{"title":"In vitro evaluation of the dispersion of nano-polylactic acid and nano-zinc oxide fillers in denture base resins using spectroscopic modalities.","authors":"Nikita Parasrampuria, N Gopi Chander, Jayanta Chattopadhyay","doi":"10.4103/jips.jips_142_25","DOIUrl":"https://doi.org/10.4103/jips.jips_142_25","url":null,"abstract":"<p><strong>Aim: </strong>Polymethyl methacrylate (PMMA) is a widely used denture base material, but its mechanical and antimicrobial properties require further improvement to the diverse clinical situations. Nanoparticles such as zinc oxide (ZnO) and polylactic acid (PLA) offer promising enhancements through improved structural and functional integration. The aim of the study was to assess the molecular characterization and structural integration of PMMA modified with nano-ZnO and nano-PLA.</p><p><strong>Settings and design: </strong>This was an in vitro material characterization study.</p><p><strong>Materials and methods: </strong>Forty samples were fabricated and divided into two groups: control (n = 20, unmodified PMMA) and test (n = 20, PMMA reinforced with 10% nano-PLA and 3% ZnO). A high-shear mixing technique was used. Molecular interactions were evaluated using Fourier-transform infrared spectroscopy (FTIR), and energy-dispersive X-ray spectroscopy (EDS) estimated the nanoparticle dispersion and elemental composition.</p><p><strong>Statistical analysis used: </strong>Qualitative analysis was used for statistical analysis.</p><p><strong>Results: </strong>FTIR confirmed the inclusion of nano-PLA and nano-ZnO, with a broad absorption peak at 3500 cm-1 indicating increased polarity and hydrogen bonding. EDS analysis verified the presence of carbon, oxygen, and zinc, with uniform nanoparticle dispersion. Nano-PLA addition reduced crystallinity and nano-ZnO promoted crystal formation, indicating their functions in structural modification.</p><p><strong>Conclusion: </strong>The study confirmed molecular interactions and uniform elemental dispersion, with indications of reduced crystallinity. These findings suggest potential for further investigations into the mechanical and antimicrobial properties of this modified resin for clinical applications.</p>","PeriodicalId":22669,"journal":{"name":"The Journal of Indian Prosthodontic Society","volume":"25 4","pages":"346-352"},"PeriodicalIF":1.0,"publicationDate":"2025-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145329798","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Comparative evaluation of fracture toughness and antifungal properties of polymethyl methacrylate and polyetheretherketone incorporated with titanium dioxide nanoparticles in different concentrations - An in vitro study. 不同浓度的二氧化钛纳米颗粒掺入聚甲基丙烯酸甲酯和聚醚醚酮的断裂韧性和抗真菌性能的比较评价-一项体外研究。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-10-01 Epub Date: 2025-10-20 DOI: 10.4103/jips.jips_253_25
S S Sivananda Narasimha Teja Vetsa, Peter John, Muthukumar Balasubramaniam

Aim: This study aimed to compare and evaluate the fracture toughness and antifungal properties of polymethyl methacrylate (PMMA) and polyether etherketone (PEEK) materials incorporated with titanium dioxide nanoparticles at two different concentrations (2% and 3%).

Settings and design: A total of 42 PMMA specimens and 42 PEEK specimens were fabricated, with each group consisting of 7 specimens and a total of 6 groups, and each group was subjected to tests for fracture toughness and antifungal property.

Materials and methods: The PMMA specimens were fabricated by incorporating TiO2 nanoparticles in 2 and 3 percentages into the polymer, followed by making the specimens in the lost wax technique, and PEEK specimens were fabricated by incorporating the nanoparticles into the pellets in 2 and 3 percentages, followed by filament extrusion, and this filament was used for three-dimensional printing the specimens in required dimensions. Once the specimens were fabricated, these were tested for fracture toughness using urinary tract mycosis and antifungal properties using the green synthesis method. Later, statistical analysis was performed to determine the significance.

Statistical analysis used: Statistical analysis was done using IBM SPSS Statistics for Windows, Version 20.0. The Shapiro-Wilk test was applied to each group for assessment of data normality. One-way analysis of variance followed by Tukey's post hoc test was done.

Results: Fracture toughness of PMMA with 3% of TiO2 was highest among the PMMA group, being 1.62 ± 0.64 MPa m1/2 and PEEK with 3% of TiO2 is highest among the PEEK group being 4.91 ± 0.30 MPa m1/2 when compared to 0% and 2% groups. Similarly, for anti-Candida, the results were better in the group with 3% of TiO2 PMMA (154.86 ± 3.13 CFU/100 mL) and 3% of TiO2 PEEK (131.14 ± 2.73 CFU/100 mL) compared to other groups.

Conclusion: Both fracture toughness and anti-Candida properties were improved when incorporated with TiO2 nanoparticles, these properties enhanced as the concentration of nanoparticles increased within the limitations of the study.

目的:比较和评价不同浓度(2%和3%)二氧化钛纳米粒子对聚甲基丙烯酸甲酯(PMMA)和聚醚酮(PEEK)材料的断裂韧性和抗真菌性能。设置与设计:共制作42个PMMA和42个PEEK样品,每组7个,共6组,对每组进行断裂韧性和抗真菌性能测试。材料与方法:将2、3%的TiO2纳米颗粒掺入聚合物中制备PMMA样品,然后采用失蜡技术制备样品;将2、3%的TiO2纳米颗粒掺入球团中制备PEEK样品,然后采用挤出长丝的方法,用该长丝进行所需尺寸的三维打印。一旦标本被制造,这些测试断裂韧性使用尿路真菌和抗真菌性能使用绿色合成方法。随后进行统计学分析,确定显著性。采用的统计分析:采用IBM SPSS Statistics for Windows, Version 20.0进行统计分析。各组采用Shapiro-Wilk检验评估数据的正态性。进行单因素方差分析,并进行Tukey事后检验。结果:添加3% TiO2的PMMA的断裂韧性在PMMA组中最高,为1.62±0.64 MPa m1/2;添加3% TiO2的PEEK的断裂韧性在PEEK组中最高,为4.91±0.30 MPa m1/2。同样,对于抗念珠菌,3% TiO2 PMMA组(154.86±3.13 CFU/100 mL)和3% TiO2 PEEK组(131.14±2.73 CFU/100 mL)的效果优于其他组。结论:TiO2纳米颗粒掺入后,材料的断裂韧性和抗念珠菌性能均有所提高,且在研究范围内,随着纳米颗粒浓度的增加,材料的断裂韧性和抗念珠菌性能均有所增强。
{"title":"Comparative evaluation of fracture toughness and antifungal properties of polymethyl methacrylate and polyetheretherketone incorporated with titanium dioxide nanoparticles in different concentrations - An in vitro study.","authors":"S S Sivananda Narasimha Teja Vetsa, Peter John, Muthukumar Balasubramaniam","doi":"10.4103/jips.jips_253_25","DOIUrl":"https://doi.org/10.4103/jips.jips_253_25","url":null,"abstract":"<p><strong>Aim: </strong>This study aimed to compare and evaluate the fracture toughness and antifungal properties of polymethyl methacrylate (PMMA) and polyether etherketone (PEEK) materials incorporated with titanium dioxide nanoparticles at two different concentrations (2% and 3%).</p><p><strong>Settings and design: </strong>A total of 42 PMMA specimens and 42 PEEK specimens were fabricated, with each group consisting of 7 specimens and a total of 6 groups, and each group was subjected to tests for fracture toughness and antifungal property.</p><p><strong>Materials and methods: </strong>The PMMA specimens were fabricated by incorporating TiO2 nanoparticles in 2 and 3 percentages into the polymer, followed by making the specimens in the lost wax technique, and PEEK specimens were fabricated by incorporating the nanoparticles into the pellets in 2 and 3 percentages, followed by filament extrusion, and this filament was used for three-dimensional printing the specimens in required dimensions. Once the specimens were fabricated, these were tested for fracture toughness using urinary tract mycosis and antifungal properties using the green synthesis method. Later, statistical analysis was performed to determine the significance.</p><p><strong>Statistical analysis used: </strong>Statistical analysis was done using IBM SPSS Statistics for Windows, Version 20.0. The Shapiro-Wilk test was applied to each group for assessment of data normality. One-way analysis of variance followed by Tukey's post hoc test was done.</p><p><strong>Results: </strong>Fracture toughness of PMMA with 3% of TiO2 was highest among the PMMA group, being 1.62 ± 0.64 MPa m1/2 and PEEK with 3% of TiO2 is highest among the PEEK group being 4.91 ± 0.30 MPa m1/2 when compared to 0% and 2% groups. Similarly, for anti-Candida, the results were better in the group with 3% of TiO2 PMMA (154.86 ± 3.13 CFU/100 mL) and 3% of TiO2 PEEK (131.14 ± 2.73 CFU/100 mL) compared to other groups.</p><p><strong>Conclusion: </strong>Both fracture toughness and anti-Candida properties were improved when incorporated with TiO2 nanoparticles, these properties enhanced as the concentration of nanoparticles increased within the limitations of the study.</p>","PeriodicalId":22669,"journal":{"name":"The Journal of Indian Prosthodontic Society","volume":"25 4","pages":"340-345"},"PeriodicalIF":1.0,"publicationDate":"2025-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145329779","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Role of prosthodontists in managing peri-implantitis. 修复医师在处理种植体周围炎中的作用。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-10-01 Epub Date: 2025-10-20 DOI: 10.4103/jips.jips_476_25
Shilpa R Shetty
{"title":"Role of prosthodontists in managing peri-implantitis.","authors":"Shilpa R Shetty","doi":"10.4103/jips.jips_476_25","DOIUrl":"10.4103/jips.jips_476_25","url":null,"abstract":"","PeriodicalId":22669,"journal":{"name":"The Journal of Indian Prosthodontic Society","volume":"25 4","pages":"283-284"},"PeriodicalIF":1.0,"publicationDate":"2025-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145329810","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of photofunctionalization with and without vibration on osseointegration of titanium implants: A comparative in vitro study. 有振动和无振动的光功能化对钛种植体骨整合的影响:体外比较研究。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-10-01 Epub Date: 2025-10-20 DOI: 10.4103/jips.jips_194_25
Priyanka Patra, Rajyalakshmi Ravuri, Praveen Mamidi, Gautam Kumar Annojjula, Tejaswi Manasa Emany, Chittaranjan Bogishetty

Aim: Enhancing early cell-implant interaction is vital for successful osseointegration. This in vitro study aimed to evaluate the combined effect of photofunctionalization and low-frequency mechanical vibration on osteoblast cells derived from human placental tissue cultured on titanium surfaces.

Settings and design: Following approval from the Institutional Ethics Committee and informed consent, a controlled in vitro experimental study was conducted in the Department of Prosthodontics in collaboration with a certified cell culture laboratory.

Materials and methods: Osteoblast cells were isolated and cultured. Titanium implant surface was photofunctionalized using ultraviolet C (UV-C) light (254 nm) for 48 h. Cells were seeded onto the implant surface and divided into three groups: Group 1: Control (untreated titanium), Group 2: UV-treated titanium, and Group 3: UV-treated titanium implant with mechanical vibration (20 Hz for 3 min/day for 3 days) to osteoblast cells. Cell proliferation was assessed using MTT assay, mineralization via Alizarin Red S staining, and osteogenic gene expression (runt-related transcription factor-2, Alkaline phosphatase, OCN) through reverse transcription polymerase chain reaction.

Statistical analysis used: Data were analyzed using analysis of variance with Tukey's post hoc test (P < 0.05).

Results: The combination of photofunctionalization and mechanical vibration (Group 3) significantly enhanced cell proliferation, mineral deposition, and osteogenic gene expression compared to Groups 1 and 2 (P < 0.05). While photofunctionalization alone improved osteoblast activity, the synergistic application of mechanical vibration further amplified the response.

Conclusion: The combination of photofunctionalization and low-frequency vibration significantly enhances the osteogenic response of osteoblast cells to titanium, indicating its potential to improve implant osseointegration.

目的:增强早期细胞-种植体相互作用对骨整合的成功至关重要。本实验旨在探讨光功能化和低频机械振动对钛表面培养的人胎盘组织成骨细胞的联合作用。环境和设计:经机构伦理委员会批准并获得知情同意后,在口腔修复科与经认证的细胞培养实验室合作进行了一项对照体外实验研究。材料与方法:分离培养成骨细胞。采用UV-C光(254 nm)对钛种植体表面进行48 h的光功能化。将细胞播种于种植体表面,分为三组:1组:对照(未处理的钛),2组:紫外线处理的钛,3组:紫外线处理的钛种植体通过机械振动(20 Hz, 3分钟/天,3天)对成骨细胞。MTT法检测细胞增殖,茜素红S染色检测矿化,逆转录聚合酶链反应检测成骨基因(矮子相关转录因子-2,碱性磷酸酶,OCN)表达。采用统计学分析:采用Tukey事后检验方差分析(P < 0.05)。结果:与1、2组相比,光功能化与机械振动联合作用(3组)显著增强了细胞增殖、矿物质沉积和成骨基因表达(P < 0.05)。光功能化可以提高成骨细胞的活性,而机械振动的协同应用进一步放大了这种反应。结论:光功能化与低频振动结合可显著增强成骨细胞对钛的成骨反应,提示其具有改善种植体骨整合的潜力。
{"title":"Effect of photofunctionalization with and without vibration on osseointegration of titanium implants: A comparative in vitro study.","authors":"Priyanka Patra, Rajyalakshmi Ravuri, Praveen Mamidi, Gautam Kumar Annojjula, Tejaswi Manasa Emany, Chittaranjan Bogishetty","doi":"10.4103/jips.jips_194_25","DOIUrl":"https://doi.org/10.4103/jips.jips_194_25","url":null,"abstract":"<p><strong>Aim: </strong>Enhancing early cell-implant interaction is vital for successful osseointegration. This in vitro study aimed to evaluate the combined effect of photofunctionalization and low-frequency mechanical vibration on osteoblast cells derived from human placental tissue cultured on titanium surfaces.</p><p><strong>Settings and design: </strong>Following approval from the Institutional Ethics Committee and informed consent, a controlled in vitro experimental study was conducted in the Department of Prosthodontics in collaboration with a certified cell culture laboratory.</p><p><strong>Materials and methods: </strong>Osteoblast cells were isolated and cultured. Titanium implant surface was photofunctionalized using ultraviolet C (UV-C) light (254 nm) for 48 h. Cells were seeded onto the implant surface and divided into three groups: Group 1: Control (untreated titanium), Group 2: UV-treated titanium, and Group 3: UV-treated titanium implant with mechanical vibration (20 Hz for 3 min/day for 3 days) to osteoblast cells. Cell proliferation was assessed using MTT assay, mineralization via Alizarin Red S staining, and osteogenic gene expression (runt-related transcription factor-2, Alkaline phosphatase, OCN) through reverse transcription polymerase chain reaction.</p><p><strong>Statistical analysis used: </strong>Data were analyzed using analysis of variance with Tukey's post hoc test (P < 0.05).</p><p><strong>Results: </strong>The combination of photofunctionalization and mechanical vibration (Group 3) significantly enhanced cell proliferation, mineral deposition, and osteogenic gene expression compared to Groups 1 and 2 (P < 0.05). While photofunctionalization alone improved osteoblast activity, the synergistic application of mechanical vibration further amplified the response.</p><p><strong>Conclusion: </strong>The combination of photofunctionalization and low-frequency vibration significantly enhances the osteogenic response of osteoblast cells to titanium, indicating its potential to improve implant osseointegration.</p>","PeriodicalId":22669,"journal":{"name":"The Journal of Indian Prosthodontic Society","volume":"25 4","pages":"334-339"},"PeriodicalIF":1.0,"publicationDate":"2025-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145329787","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Immediate complete denture rehabilitation using combined digital-functional impression technique and three-dimensional-printed occlusal templates. 结合数字功能印模技术和三维打印咬合模板的即刻全口义齿修复。
IF 1 Q3 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-10-01 Epub Date: 2025-10-20 DOI: 10.4103/jips.jips_353_25
Dhitika Handa, Abhijit Ashok Patil, Ajay Sabane, Rupali Patil

Integration of digital technology in prosthodontics enables precise and predictable outcomes. A hybrid digital-conventional workflow combines the accuracy of digital protocols with the reliability of traditional techniques. A 46-year-old male with generalized aggressive periodontitis required full-mouth extraction and immediate dentures. Intraoral scans were captured at the existing vertical dimension and used to design custom trays in EXOCAD. The trays, three-dimensional-printed with windows for natural teeth, facilitated border molding and final impressions for soft tissue capture. These impressions were digitized, superimposed on intraoral scans, and used to create a virtual model, perform virtual extractions, and fabricate definitive dentures. The digital approach improved patient comfort, accelerated planning, and enhanced accuracy, while conventional steps ensured an optimal peripheral seal in scanner-inaccessible areas. The technique delivered a functionally stable and esthetically satisfactory outcome.

数字技术在口腔修复中的集成可以实现精确和可预测的结果。数字-传统混合工作流结合了数字协议的准确性和传统技术的可靠性。一位46岁男性,患有广泛性侵袭性牙周炎,需要全口拔牙和即时义齿。在现有的垂直尺寸上捕获口内扫描,并用于在EXOCAD中设计定制托盘。托盘,三维打印的窗口自然牙齿,促进边界成型和软组织捕获的最终印象。这些印象被数字化,叠加在口腔内扫描上,用于创建虚拟模型,进行虚拟拔牙,并制造最终假牙。数字方法提高了患者的舒适度,加速了计划,提高了准确性,而传统步骤确保了扫描仪无法到达区域的最佳外围密封。该技术提供了功能稳定和美观满意的结果。
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引用次数: 0
期刊
The Journal of Indian Prosthodontic Society
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