In this work two new alloys were obtained by extrapolation from a wellknown high entropy alloy, the equimolar CoNiFeMnCr one. This was doneby the addition of carbon and of tantalum, Ta being one of the strongestMC-former elements. They were produced by conventional casting underinert atmosphere. The obtained microstructures were characterized by X-raydiffraction, metallography, electron microscopy, and energy dispersionspectrometry. Their hardness was also measured by hardness indentation.In parallel, the original CoNiFeMnCr alloy was also synthesized andcharacterized for comparison. The reference HEA alloy is single-phasedwith an austenitic structure, while the two {Ta, C}-added alloys aredouble-phased, with an austenitic matrix and interdendritic script-likeTaC carbides. The matrixes of these HEA/TaC alloy are equivalent toan equimolar CoNiFeMnCr alloy to which 2 wt.% Ta is present in solidsolution. The presence of the TaC carbides caused a significant increase inhardness which suggests that the HEA/TaC alloys may be mechanicallystronger than the HEA reference alloy at high temperature.
{"title":"As-Cast Microstructures of High Entropy Alloys Designed to Be TaC-Strengthened","authors":"P. Berthod","doi":"10.30564/jmmr.v5i2.4685","DOIUrl":"https://doi.org/10.30564/jmmr.v5i2.4685","url":null,"abstract":"In this work two new alloys were obtained by extrapolation from a wellknown high entropy alloy, the equimolar CoNiFeMnCr one. This was doneby the addition of carbon and of tantalum, Ta being one of the strongestMC-former elements. They were produced by conventional casting underinert atmosphere. The obtained microstructures were characterized by X-raydiffraction, metallography, electron microscopy, and energy dispersionspectrometry. Their hardness was also measured by hardness indentation.In parallel, the original CoNiFeMnCr alloy was also synthesized andcharacterized for comparison. The reference HEA alloy is single-phasedwith an austenitic structure, while the two {Ta, C}-added alloys aredouble-phased, with an austenitic matrix and interdendritic script-likeTaC carbides. The matrixes of these HEA/TaC alloy are equivalent toan equimolar CoNiFeMnCr alloy to which 2 wt.% Ta is present in solidsolution. The presence of the TaC carbides caused a significant increase inhardness which suggests that the HEA/TaC alloys may be mechanicallystronger than the HEA reference alloy at high temperature.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"322 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-06-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"115840771","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Oman Sea is connecting belt between the Indian Ocean and PersianGulf. Because it strategic and environmental aim, presence of naturalradionuclide 226Ra, 232Th, 40K and 137Cs as man-made element is considered.Water samples were taken from 36 marine spots at the coastal strip fromHormoz canyon to Goatr seaport in the northern coast of Oman Sea.Correspondence analysis is used to identify variation and relationshipbetween samples (Q-mood analysis) and variable (R-mood analysis) basedon approximate χ2 distances. Radioactive elements (226Ra, 232Th and 40K),physical (temperature, pH, turbidity, conductivity, special density) andchemical (salinity, oxygen and chlorophyll) parameters of water for 36samples handled by correspondence analysis, there are two outstandingresult, 1) Radioactive elements show high correlation in factors by greatereigenvalue, and 2) some of the samples such as W13, W24 and rather W02,W05 and W12 show highest activity from Radioactive elements and alsotemperature and conductivity show nearest relation with them in manyfactors.
{"title":"Interpretation of Water Samples by Correspondence Analysis for Radioactive Elements in the Northern Coast of Oman Sea","authors":"Farshad Darab-Golestan, M. R. Zare","doi":"10.30564/jmmr.v5i1.4571","DOIUrl":"https://doi.org/10.30564/jmmr.v5i1.4571","url":null,"abstract":"Oman Sea is connecting belt between the Indian Ocean and PersianGulf. Because it strategic and environmental aim, presence of naturalradionuclide 226Ra, 232Th, 40K and 137Cs as man-made element is considered.Water samples were taken from 36 marine spots at the coastal strip fromHormoz canyon to Goatr seaport in the northern coast of Oman Sea.Correspondence analysis is used to identify variation and relationshipbetween samples (Q-mood analysis) and variable (R-mood analysis) basedon approximate χ2 distances. Radioactive elements (226Ra, 232Th and 40K),physical (temperature, pH, turbidity, conductivity, special density) andchemical (salinity, oxygen and chlorophyll) parameters of water for 36samples handled by correspondence analysis, there are two outstandingresult, 1) Radioactive elements show high correlation in factors by greatereigenvalue, and 2) some of the samples such as W13, W24 and rather W02,W05 and W12 show highest activity from Radioactive elements and alsotemperature and conductivity show nearest relation with them in manyfactors.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"7 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-05-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126852718","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The hydrodynamic characteristics of bimetallic Ag/Cu and Co/Ag nanoparticles stabilized by chitosan were determined. The polydispersity indexand the diameter of nanoparticles were observed to decrease in contrast tothe original polymer during the creation of chitosan stabilized bimetallicnanoparticles, decreasing from 0.342 to 0.12±0.04 and 2.5 micron to 180nm, respectively. However, the diffusion coefficient of chitosan was increased from 0.2 cm2 /s to 2.71 cm2 /s during the production of stable bimetallic nanoparticles. The lack of absorption bands at 500 nm and 700 nm-900 nm in the UV spectra of the samples suggests that in the presence ofa reducing agent, copper (II) and cobalt (II) ions undergo full reduction.The relationship between the synthesis conditions and the kind of structureof bimetallic nanoparticles “core-shell” has been discovered. Silver atomshave been shown to be both a core and a shell, depending on the synthesisconditions and chemical nature of metal ions.
{"title":"Determination of Hydrodynamic Parameters of Chitosan Stabilized Bimetallic Nanoparticles","authors":"Vokhidova N. R., Rashidova S. Sh.","doi":"10.30564/jmmr.v5i1.4566","DOIUrl":"https://doi.org/10.30564/jmmr.v5i1.4566","url":null,"abstract":"The hydrodynamic characteristics of bimetallic Ag/Cu and Co/Ag nanoparticles stabilized by chitosan were determined. The polydispersity indexand the diameter of nanoparticles were observed to decrease in contrast tothe original polymer during the creation of chitosan stabilized bimetallicnanoparticles, decreasing from 0.342 to 0.12±0.04 and 2.5 micron to 180nm, respectively. However, the diffusion coefficient of chitosan was increased from 0.2 cm2 /s to 2.71 cm2 /s during the production of stable bimetallic nanoparticles. The lack of absorption bands at 500 nm and 700 nm-900 nm in the UV spectra of the samples suggests that in the presence ofa reducing agent, copper (II) and cobalt (II) ions undergo full reduction.The relationship between the synthesis conditions and the kind of structureof bimetallic nanoparticles “core-shell” has been discovered. Silver atomshave been shown to be both a core and a shell, depending on the synthesisconditions and chemical nature of metal ions.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"25 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-04-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"132980895","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The efficiency and irreversibility defined based on the second law ofthermodynamics provide a new path for heat exchangers design and makeperformance analysis more straightforward and elegant. The second lawof thermodynamics is applied in a Straight Microchannel Printed Circuitheat exchanger to determine the thermal performance of different shapes ofBoehmite Alumina compared to Al2O3 aluminum oxide. The various formsof non-spherical Boehmite Alumina are characterized dynamically andthermodynamically through dynamic viscosity and thermal conductivity,using empirical coefficients. The non-spherical shape includes platelet,cylindrical, blades, and bricks forms. Graphical results are presented forthermal efficiency, thermal irreversibility, heat transfer rate, and nanofluidexit temperature. The non-spherical shapes of Boehmite Alumina showdifferent thermal characteristics concerning the spherical shape whenthere are variations in fluid flow rates and the nanoparticles fraction.Furthermore, it was theoretically demonstrated that non-spherical particleshave higher heat transfer rates than spherical particles, emphasizingplatelets and cylindrical shapes for the low volume fraction of nanoparticlesand bricks and blades for high volume fraction.
{"title":"Influence of Nanoparticle Shapes of Boehmite Alumina on the Thermal Performance of a Straight Microchannel Printed Circuit Heat Exchanger","authors":"E. Nogueira","doi":"10.30564/jmmr.v5i1.4364","DOIUrl":"https://doi.org/10.30564/jmmr.v5i1.4364","url":null,"abstract":"The efficiency and irreversibility defined based on the second law ofthermodynamics provide a new path for heat exchangers design and makeperformance analysis more straightforward and elegant. The second lawof thermodynamics is applied in a Straight Microchannel Printed Circuitheat exchanger to determine the thermal performance of different shapes ofBoehmite Alumina compared to Al2O3 aluminum oxide. The various formsof non-spherical Boehmite Alumina are characterized dynamically andthermodynamically through dynamic viscosity and thermal conductivity,using empirical coefficients. The non-spherical shape includes platelet,cylindrical, blades, and bricks forms. Graphical results are presented forthermal efficiency, thermal irreversibility, heat transfer rate, and nanofluidexit temperature. The non-spherical shapes of Boehmite Alumina showdifferent thermal characteristics concerning the spherical shape whenthere are variations in fluid flow rates and the nanoparticles fraction.Furthermore, it was theoretically demonstrated that non-spherical particleshave higher heat transfer rates than spherical particles, emphasizingplatelets and cylindrical shapes for the low volume fraction of nanoparticlesand bricks and blades for high volume fraction.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"27 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-02-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"121395815","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The welding of dissimilar materials is one of the challenging issues in thefabrication industry to obtain required quality welds using fusion weldingmethods. However, some processes recently improved interface bondingwith low joint strength. Unfortunately, the major intermetallic compoundscould not alleviate from the joint interface. Alternatively, solid-statewelding methods revealed fewer intermetallics at the joint interface fordissimilar material welds. Among them, friction welding was chosen to joinincompatible materials with the necessary properties successfully. Frictiontime is a critical parameter for obtaining strong welds through frictionwelding, apart from friction pressure, forging pressure, forging time, androtational speed. Variability of friction time can change the strength offriction by changing mechanical properties such as tensile strength. Thischange of tensile strength is typically influenced by the intermixing region,dependent on friction time. In this experiment, carbon steel and stainlesssteel have been friction welded to test the impact of friction time on thejoint interface where the substrate’s faying surface meets. This interfaceconsists of the intermixing region of the two materials on which the frictionwelding is performed. The results showed an interesting variation in tensilestrength, with varying friction time. The width of the intermixing zoneincreased gradually with friction time until and decreased with the furtherincreasing. The strength of the welds obtained was the highest of 730 MPaat a friction time of 4 s and fell as friction time’s increased value after 4 s.
{"title":"The Influence of Friction Time on the Joint Interface and Mechanical Properties in Dissimilar Friction Welds","authors":"Venkata Charan Kantumuchu, Muralimohan Cheepu","doi":"10.30564/jmmr.v5i1.4209","DOIUrl":"https://doi.org/10.30564/jmmr.v5i1.4209","url":null,"abstract":"The welding of dissimilar materials is one of the challenging issues in thefabrication industry to obtain required quality welds using fusion weldingmethods. However, some processes recently improved interface bondingwith low joint strength. Unfortunately, the major intermetallic compoundscould not alleviate from the joint interface. Alternatively, solid-statewelding methods revealed fewer intermetallics at the joint interface fordissimilar material welds. Among them, friction welding was chosen to joinincompatible materials with the necessary properties successfully. Frictiontime is a critical parameter for obtaining strong welds through frictionwelding, apart from friction pressure, forging pressure, forging time, androtational speed. Variability of friction time can change the strength offriction by changing mechanical properties such as tensile strength. Thischange of tensile strength is typically influenced by the intermixing region,dependent on friction time. In this experiment, carbon steel and stainlesssteel have been friction welded to test the impact of friction time on thejoint interface where the substrate’s faying surface meets. This interfaceconsists of the intermixing region of the two materials on which the frictionwelding is performed. The results showed an interesting variation in tensilestrength, with varying friction time. The width of the intermixing zoneincreased gradually with friction time until and decreased with the furtherincreasing. The strength of the welds obtained was the highest of 730 MPaat a friction time of 4 s and fell as friction time’s increased value after 4 s.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"60 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"123915231","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Natural organic matter affect water environmental security and posed a potential threat to human health, and thus it has long been considered as a key index to evaluate water treatment performance. Dissolved organic nitrogen is one of the NOM, which produces some disinfection byproducts having more toxic than those carbon-based materials. Coagulation is a key unit of drinking water purification and has received wide attention. However, conventional flocculation technology on removal of DON is so poor that we have to seek more effective improving measurement. The combined use of conventional flocculant and organic polymer can improve treatment efficiency to a certain extent, and enhanced coagulation can also improve the DON removal rate, but their DON removal performance is still not dreamful. At present, there is a lack of systematic research on flocculation to remove DON. Although some achievements have been made, there is still a big gap between the preparation technology of flocculant and the goal of efficient removal of DON in water.For treatment of secondary effluent of industrial wastewater, some studies show that the use of Fe3O4 mainly has the effect of accelerating separation, but the adsorption effect is not good. However, with the synergistic flocculation of amino functionalized Fe3O4 it has a good effect on removing water protein, polysaccharide and humic acid, which can meet the water quality discharge standard and reduce the dosage of flocculant. The above results show that functional nanoparticle materials are of great significance to improve the adsorption and flocculation performance. Therefore, the functional modification of magnetic nanoparticles plays an important role.
{"title":"Developing Magnetic Material for Remediation of Aquatic Nitrogen Pollution in Water Facilities","authors":"G. Zhu, Junming Chen","doi":"10.30564/jmmr.v4i2.4231","DOIUrl":"https://doi.org/10.30564/jmmr.v4i2.4231","url":null,"abstract":"Natural organic matter affect water environmental security and posed a potential threat to human health, and thus it has long been considered as a key index to evaluate water treatment performance. Dissolved organic nitrogen is one of the NOM, which produces some disinfection byproducts having more toxic than those carbon-based materials. Coagulation is a key unit of drinking water purification and has received wide attention. However, conventional flocculation technology on removal of DON is so poor that we have to seek more effective improving measurement. The combined use of conventional flocculant and organic polymer can improve treatment efficiency to a certain extent, and enhanced coagulation can also improve the DON removal rate, but their DON removal performance is still not dreamful. At present, there is a lack of systematic research on flocculation to remove DON. Although some achievements have been made, there is still a big gap between the preparation technology of flocculant and the goal of efficient removal of DON in water.For treatment of secondary effluent of industrial wastewater, some studies show that the use of Fe3O4 mainly has the effect of accelerating separation, but the adsorption effect is not good. However, with the synergistic flocculation of amino functionalized Fe3O4 it has a good effect on removing water protein, polysaccharide and humic acid, which can meet the water quality discharge standard and reduce the dosage of flocculant. The above results show that functional nanoparticle materials are of great significance to improve the adsorption and flocculation performance. Therefore, the functional modification of magnetic nanoparticles plays an important role.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-12-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130159454","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The work done in this work deals with the efficacy of cutting parameters on surface of EN-8 alloy steel. For knowing the optimal effects of cutting parameters response surface methodology was practiced subjected to central composite design matrix. The motive was to introduce an interaction among input parameters, i.e., cutting speed, feed and depth of cut and output parameter, surface roughness. For this, second order response surface model was modeled. The foreseen values obtained were found to be fairly close to observed values, showed that the model could be practiced to forecast the surface roughness on EN-8 within the range of parameter studied. Contours and 3-D plots are generated to forecast the value of surface roughness. It was revealed that surface roughness decreases with increases in cutting speed and it increases with feed. However, there were found negligible or almost no implication of depth of cut on surface roughness whereas feed rate affected the surface roughness most. For lower surface roughness, the optimum values of each one were also evaluated.
{"title":"Investigation and Mathematical Modelling of Optimized Cutting Parameters for Surface Roughness of EN-8 Alloy Steel","authors":"A. Saraswat, Dipak Kumar","doi":"10.30564/jmmr.v4i2.4094","DOIUrl":"https://doi.org/10.30564/jmmr.v4i2.4094","url":null,"abstract":"The work done in this work deals with the efficacy of cutting parameters on surface of EN-8 alloy steel. For knowing the optimal effects of cutting parameters response surface methodology was practiced subjected to central composite design matrix. The motive was to introduce an interaction among input parameters, i.e., cutting speed, feed and depth of cut and output parameter, surface roughness. For this, second order response surface model was modeled. The foreseen values obtained were found to be fairly close to observed values, showed that the model could be practiced to forecast the surface roughness on EN-8 within the range of parameter studied. Contours and 3-D plots are generated to forecast the value of surface roughness. It was revealed that surface roughness decreases with increases in cutting speed and it increases with feed. However, there were found negligible or almost no implication of depth of cut on surface roughness whereas feed rate affected the surface roughness most. For lower surface roughness, the optimum values of each one were also evaluated.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"65 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-12-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"121602537","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
As an emerging alloy material, high-entropy alloy has potential applications that distinguish it from traditional alloys due to its special physicochemical properties. In this work, a low melting point GaInSnBiZn high-entropy alloy was designed based on Miedema model, and its surface tension was measured by the continuous pendant-drop method. The results show that the intrinsic surface tension of GaInSnBiZn high-entropy alloy at 80 °C is 545±5 mN/m, and the surface tension of the liquid alloy is significantly reduced by the formation of surface oxide film. The surface tension of GaInSnBiZn high-entropy alloy was analyzed by using theoretical models (Guggenheim model, GSM (general solution) model and Butler model), and the thermodynamic characteristics of the surface tension formation were further verified by combining with thermodynamic calculations, among which the calculated results of Butler model were in good agreement with the experimental data. Meanwhile, it is found that the surface concentration of Bi in the alloy is much larger than the nominal concentration of its bulk phase, which contributes the most to the surface tension of the alloy, however, it contributes the least to the entropy of the alloy formation in combination with the Butler model.
{"title":"Surface Tension of GaInSnBiZn Liquid High-entropy Alloy","authors":"S. Zhu, Lu Liu, Q. Lin","doi":"10.30564/jmmr.v4i2.4091","DOIUrl":"https://doi.org/10.30564/jmmr.v4i2.4091","url":null,"abstract":"As an emerging alloy material, high-entropy alloy has potential applications that distinguish it from traditional alloys due to its special physicochemical properties. In this work, a low melting point GaInSnBiZn high-entropy alloy was designed based on Miedema model, and its surface tension was measured by the continuous pendant-drop method. The results show that the intrinsic surface tension of GaInSnBiZn high-entropy alloy at 80 °C is 545±5 mN/m, and the surface tension of the liquid alloy is significantly reduced by the formation of surface oxide film. The surface tension of GaInSnBiZn high-entropy alloy was analyzed by using theoretical models (Guggenheim model, GSM (general solution) model and Butler model), and the thermodynamic characteristics of the surface tension formation were further verified by combining with thermodynamic calculations, among which the calculated results of Butler model were in good agreement with the experimental data. Meanwhile, it is found that the surface concentration of Bi in the alloy is much larger than the nominal concentration of its bulk phase, which contributes the most to the surface tension of the alloy, however, it contributes the least to the entropy of the alloy formation in combination with the Butler model.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"18 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-12-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"115249846","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
The effect of microcosmic morphologies of textured Cu surface by nanosecond laser on the inert wetting and reactive wetting, i.e., ethylene glycol/copper and tin/copper wetting systems, was studied by using modified sessile drop methods. To create different surface roughness, the microcosmic morphologies with different spacing of grooves were constructed by nanosecond laser. The results showed that the inert wetting (ethylene glycol/copper) was consistent with Wenzel model, while the reactive wetting results deviated from the model. In Sn/Cu reactive wetting system, the interfacial evolution in the early stage and the pinning of triple line by the precipitated h-Cu6Sn5 caused the rougher surface and the worse final wettability. When the scale of artificial roughness exceeded the roughness that was caused by interfacial reaction after reaching the quasi-equilibrium state at interface, the final wettability could be improved.
{"title":"Wetting of Laser Textured Cu Surface by Ethylene Glycol and Sn","authors":"Q. Lin, Kaibin Xie, Yu jie Ge","doi":"10.30564/JMMR.V4I1.3427","DOIUrl":"https://doi.org/10.30564/JMMR.V4I1.3427","url":null,"abstract":"The effect of microcosmic morphologies of textured Cu surface by nanosecond laser on the inert wetting and reactive wetting, i.e., ethylene glycol/copper and tin/copper wetting systems, was studied by using modified sessile drop methods. To create different surface roughness, the microcosmic morphologies with different spacing of grooves were constructed by nanosecond laser. The results showed that the inert wetting (ethylene glycol/copper) was consistent with Wenzel model, while the reactive wetting results deviated from the model. In Sn/Cu reactive wetting system, the interfacial evolution in the early stage and the pinning of triple line by the precipitated h-Cu6Sn5 caused the rougher surface and the worse final wettability. When the scale of artificial roughness exceeded the roughness that was caused by interfacial reaction after reaching the quasi-equilibrium state at interface, the final wettability could be improved.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"140 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-07-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"127519745","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Nguiamba Ngiongboung, Celestine Asobo Yanu, P. D. B. Bélibi, J. Sieliechi, M. Ngassoum
This paper deals with the formulation of ceramic filters having the porosity adapted to domestic potable water treatment. The filters were made from clays and rice husk obtained from the Far North region of Cameroon (Logone Valley). Nine formulations were investigated to choose those that might have the porosity standing between 35 and 50% (the ideal porosity adapted for water treatment) [1]. The nine formulations investigated were as follow: clay:rice husk mixture weight ratio 0.7:0.3; 0.8:0.2 and 0.9:0.1 with the particle size of 100:100 microns. The sintering temperatures of 900°C, 950°C and 1000°C were applied for each of the mixtures. The results showed that only filters with weight ratio 0.7:0.3 sintered at 900°C, 950°C and 1000°C had porosity between 35 and 50% with values of 39.41±0.96; 40.15±1.59; 40.14±1.31 respectively. Mechanical strength, permeability and iron leaching behavior were investigated for these three formulations. The formulation 0.7:0.3 with sintering temperature of 1000°C had the higher permeability and was the more stable for iron leaching so it is the more adapted for water treatment in terms of flow rate and iron leaching behavior, pore size distribution showed that these filters were macroporous and designed for microfiltration with average pore diameter of 0.46µm.
{"title":"Identification of an Appropriate Formulation for Domestic Water Ceramic Filters from Soukamna Clay (Cameroon)","authors":"Nguiamba Ngiongboung, Celestine Asobo Yanu, P. D. B. Bélibi, J. Sieliechi, M. Ngassoum","doi":"10.30564/JMMR.V4I1.3462","DOIUrl":"https://doi.org/10.30564/JMMR.V4I1.3462","url":null,"abstract":"This paper deals with the formulation of ceramic filters having the porosity adapted to domestic potable water treatment. The filters were made from clays and rice husk obtained from the Far North region of Cameroon (Logone Valley). Nine formulations were investigated to choose those that might have the porosity standing between 35 and 50% (the ideal porosity adapted for water treatment) [1]. The nine formulations investigated were as follow: clay:rice husk mixture weight ratio 0.7:0.3; 0.8:0.2 and 0.9:0.1 with the particle size of 100:100 microns. The sintering temperatures of 900°C, 950°C and 1000°C were applied for each of the mixtures. The results showed that only filters with weight ratio 0.7:0.3 sintered at 900°C, 950°C and 1000°C had porosity between 35 and 50% with values of 39.41±0.96; 40.15±1.59; 40.14±1.31 respectively. Mechanical strength, permeability and iron leaching behavior were investigated for these three formulations. The formulation 0.7:0.3 with sintering temperature of 1000°C had the higher permeability and was the more stable for iron leaching so it is the more adapted for water treatment in terms of flow rate and iron leaching behavior, pore size distribution showed that these filters were macroporous and designed for microfiltration with average pore diameter of 0.46µm.","PeriodicalId":232294,"journal":{"name":"Journal of Metallic Material Research","volume":"34 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2021-07-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"131926995","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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