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Synthesis and crystal structure of 2-(3-oxo-3-phenylpropyl)isoindoline-1,3-dione, C17H13NO3 2-（3-氧代-3-苯基丙基）异吲哚啉-1,3-二酮，C17H13NO3的合成及晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-05 DOI: 10.1515/ncrs-2023-0342
Junguo Shi, Yongjia Hao, Lian-Hua Xu, Ying Zhou, Hua-Bin Wang
Abstract C17H13NO3, monoclinic, P21/c (no. 14), a = 9.5306(2) Å, b = 6.1971(2) Å, c = 23.3849(7) Å, β = 101.445(3)°, V = 1353.70(7) Å3, Z = 4, Rgt(F) = 0.0644, wR ref (F2) = 0.1909, T = 120 K.
摘要C17H13NO3，单斜晶系，P21/c（编号14），a=9.5306（2） Å，b=6.1971（2） Å，c=23.3849（7） Å，β=101.445（3）°，V=1353.70（7） Å3，Z=4，Rgt（F）=0.0644，wR ref（F2）=0.1909，T=120 K
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引用次数: 0
Crystal structure of 7-hydroxy-3,4-dihydronaphthalen-1(2H)-one, C10H10O2 7-羟基-3,4-二氢萘-1（2H）-酮C10H10O2的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-05 DOI: 10.1515/ncrs-2023-0353
Boye Jiang, Yun Hou, Feng-Lan Zhao, Qing-Guo Meng
Abstract C10H10O2, monoclinic, C2/c (no. 15), a = 16.6341(14) Å, b = 7.4319(4) Å, c = 14.8943(10) Å, β = 123.243(8)°, V = 1540.0(2) Å3, Z = 8, Rgt(F) = 0.0371, wRref(F2) = 0.0997, T = 293 K.
摘要C10H10O2，单斜晶系，C2/c（编号15），a=16.6341（14）Oh，b=7.4319（4）Oh，c=14.8943（10）To，β=132.243（8）°，V为1540.0（2）Å3，Z=8，Rgt（F）=0.0371，wRref（F2）=0.0097，T=293。
{"title":"Crystal structure of 7-hydroxy-3,4-dihydronaphthalen-1(2H)-one, C10H10O2","authors":"Boye Jiang, Yun Hou, Feng-Lan Zhao, Qing-Guo Meng","doi":"10.1515/ncrs-2023-0353","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0353","url":null,"abstract":"Abstract C10H10O2, monoclinic, C2/c (no. 15), a = 16.6341(14) Å, b = 7.4319(4) Å, c = 14.8943(10) Å, β = 123.243(8)°, V = 1540.0(2) Å3, Z = 8, Rgt(F) = 0.0371, wRref(F2) = 0.0997, T = 293 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":" ","pages":""},"PeriodicalIF":0.3,"publicationDate":"2023-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"43690227","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of 6,6a,7,8,9,10-hexahydro-5H-pyrazino [2,3-e]pyrido[1,2-a]pyrazine, C10H14N4 6,6a，7,8,9,10-六氢-5H-吡嗪并[2,3-e]吡啶并[1,2-a]吡嗪，C10H14N4的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-05 DOI: 10.1515/ncrs-2023-0363
Yu Yu, Zhu Dali
Abstract C10H14N4, orthorhombic, Pbca (no. 61), a = 15.5356(2) Å, b = 9.8551(2) Å, c = 25.5551(4) Å, V = 3912.61(11) Å3, Z = 16, R gt (F) = 0.0873, wR ref (F2) = 0.2481, T = 150 K.
摘要C10H14N4，正交晶系，Pbca（编号61），a=15.5356（2） Å，b=9.8551（2） Å，c=25.5551（4） Å，V=3912.61（11） Å3，Z=16，R gt（F）=0.0873，wR ref（F2）=0.2481，T=150 K
{"title":"Crystal structure of 6,6a,7,8,9,10-hexahydro-5H-pyrazino [2,3-e]pyrido[1,2-a]pyrazine, C10H14N4","authors":"Yu Yu, Zhu Dali","doi":"10.1515/ncrs-2023-0363","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0363","url":null,"abstract":"Abstract C10H14N4, orthorhombic, Pbca (no. 61), a = 15.5356(2) Å, b = 9.8551(2) Å, c = 25.5551(4) Å, V = 3912.61(11) Å3, Z = 16, R gt (F) = 0.0873, wR ref (F2) = 0.2481, T = 150 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":" ","pages":""},"PeriodicalIF":0.3,"publicationDate":"2023-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48086629","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The crystal structure of catena-poly[(μ2-2H-1,2,3-triazole-4,5-dicarboxylato-κ2O, O′)-(μ2-1,3-bis((1H-imidazol-1-yl)methyl)benzene-κ2N,N′) zinc(II)], C18H15N7O4Zn 链式聚[(μ2- 2h -1,2,3-三唑-4,5-二羧基lato-κ 2o, O ')-(μ2-1,3-双((1h -咪唑-1-基)甲基)苯-κ 2n,N ')锌(II)]， c18h15n704zn的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-05 DOI: 10.1515/ncrs-2023-0323
Qian Mao, Yanfei Wang, Zhonghua Zhang, Jinlan Ji
Abstract C18H15N7O4Zn, triclinic, P 1 ‾ $overline{1}$ (no. 2), a = 9.1100(8) Å, b = 10.6451(7) Å, c = 12.0479(8) Å, α = 95.238(5)∘, β = 112.154(7)∘, γ = 112.971(7)∘, V = 956.56(13) Å3, Z = 2, R gt (F) = 0.0264, wR ref (F2) = 0.0731, T = 298 K.
摘要C18H15N7O4Zn，三斜晶系，P 1‾$overline｛1｝$（编号2），a.9.1100（8）Å，b10.6451（7）Å、c.12.0479（8）å、a.95.238（5）112.154（7）112.971（7）å，V956.56（13）Å3，Z2，Rgt（F）=0.0264，wR ref=0.0731，T82298ÅK。
{"title":"The crystal structure of catena-poly[(μ2-2H-1,2,3-triazole-4,5-dicarboxylato-κ2O, O′)-(μ2-1,3-bis((1H-imidazol-1-yl)methyl)benzene-κ2N,N′) zinc(II)], C18H15N7O4Zn","authors":"Qian Mao, Yanfei Wang, Zhonghua Zhang, Jinlan Ji","doi":"10.1515/ncrs-2023-0323","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0323","url":null,"abstract":"Abstract C18H15N7O4Zn, triclinic, P 1 ‾ $overline{1}$ (no. 2), a = 9.1100(8) Å, b = 10.6451(7) Å, c = 12.0479(8) Å, α = 95.238(5)∘, β = 112.154(7)∘, γ = 112.971(7)∘, V = 956.56(13) Å3, Z = 2, R gt (F) = 0.0264, wR ref (F2) = 0.0731, T = 298 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":" ","pages":""},"PeriodicalIF":0.3,"publicationDate":"2023-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46263708","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of poly[diaqua-(bis(m2-1,4-bis(imidazol-1-ylmethyl)benzene)-κ2N,N′-manganese] dichloride, C28H32MnN8O2Cl2 聚[双水-(双(m2-1,4-双(咪唑-1-甲基)苯)-κ 2n,N ' -锰]二氯化合物C28H32MnN8O2Cl2的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-05 DOI: 10.1515/ncrs-2023-0326
Si-Na Gu, Zhi-Ying Ou, Ting-Ting Wu, Ting Nie, Yang Liu
Abstract C28H32MnN8O2Cl2, triclinic, P 1 ‾ $Poverline{1}$ (no. 2), a = 8.987(4) Å, b = 9.061(3) Å, c = 10.706(2) Å, α = 88.65(2)°, β = 66.12(2)°, γ = 89.89(2)°, V = 796.9(5) Å3, Z = 1, R gt (F) = 0.1033, wRref(F2) = 0.2218, T = 293(2) K.
摘要C28H32MnN8O2Cl2，三斜晶系，P1‾$Poverline｛1｝$（编号2），a=8.987（4） Å，b=9.061（3） Å，c=10.706（2） Å，α=88.65（2）°，β=66.12（2）℃，γ=89.89（2）℉，V=796.9（5） Å3，Z=1，Rgt（F）=0.1033，wRref（F2）=0.2218，T=293（2） K
{"title":"Crystal structure of poly[diaqua-(bis(m2-1,4-bis(imidazol-1-ylmethyl)benzene)-κ2N,N′-manganese] dichloride, C28H32MnN8O2Cl2","authors":"Si-Na Gu, Zhi-Ying Ou, Ting-Ting Wu, Ting Nie, Yang Liu","doi":"10.1515/ncrs-2023-0326","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0326","url":null,"abstract":"Abstract C28H32MnN8O2Cl2, triclinic, P 1 ‾ $Poverline{1}$ (no. 2), a = 8.987(4) Å, b = 9.061(3) Å, c = 10.706(2) Å, α = 88.65(2)°, β = 66.12(2)°, γ = 89.89(2)°, V = 796.9(5) Å3, Z = 1, R gt (F) = 0.1033, wRref(F2) = 0.2218, T = 293(2) K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":" ","pages":""},"PeriodicalIF":0.3,"publicationDate":"2023-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44536506","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The crystal structure of catena-poly[(4-iodopyridine-2,6-dicarboxylato-κ4O,N,O′,O′′)(4-imidazol-1-yl-pyridine-κN)copper(II)], C15H9N4O4ICu 链状聚[（4-碘吡啶-2,6-二羧酸-κ4O，N，O′，O′′）（4-咪唑-1-基-吡啶-κN）铜（II）]，C15H9N4O4ICu的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-05 DOI: 10.1515/ncrs-2023-0302
Yang Kong, YiXuan Dang, Bin Tian, Chang-Zhao Wang, ZiHao Han, ChenFei Lu
Abstract C15H9N4O4ICu, monoclinic, P21/c (no. 14), a = 13.6216(4) Å, b = 13.4754(4) Å, c = 8.5023(3) Å, β = 102.610(3)°, V = 1522.99(9) Å3, Z = 4, Rgt(F) = 0.0297, wRref(F2) = 0.0781, T = 293 K.
摘要C15H9N4O4ICu，单斜晶系，P21/c（编号14），a=13.6216（4）Oh，b=13.4754（4）Oh，c=8.5023（3）To，β=102.610（3）°，V为1522.99（9）Å3，Z=4，Rgt（F）=0.0297，wRref（F2）=0.0781，T=293K。
{"title":"The crystal structure of catena-poly[(4-iodopyridine-2,6-dicarboxylato-κ4O,N,O′,O′′)(4-imidazol-1-yl-pyridine-κN)copper(II)], C15H9N4O4ICu","authors":"Yang Kong, YiXuan Dang, Bin Tian, Chang-Zhao Wang, ZiHao Han, ChenFei Lu","doi":"10.1515/ncrs-2023-0302","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0302","url":null,"abstract":"Abstract C15H9N4O4ICu, monoclinic, P21/c (no. 14), a = 13.6216(4) Å, b = 13.4754(4) Å, c = 8.5023(3) Å, β = 102.610(3)°, V = 1522.99(9) Å3, Z = 4, Rgt(F) = 0.0297, wRref(F2) = 0.0781, T = 293 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":" ","pages":""},"PeriodicalIF":0.3,"publicationDate":"2023-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44039197","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of polybis(μ4-3,5-dicarboxylatopyrazol-1-yl)-bis(N,N-dimethylformamide)tri-copper(II)–acetonitrile (1/2), C20H22Cu3N8O10 聚双（μ4-3,5-二羧基吡唑-1-基）-双（N，N-二甲基甲酰胺）三铜（II）-乙腈（1/2），C20H22Cu3N8O10的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-05 DOI: 10.1515/ncrs-2023-0308
Yan-Qing Wang, Wen-Qing Yan, Li-Xue Nie, Ping-Ping Luan, Chaomin Li
Abstract C20H22Cu3N8O10, monoclinic, C2/c (no. 15), a = 12.0766(11) Å, b = 16.2778(14) Å, c = 14.7605(13) Å, β = 97.8580(10)∘, V = 2874.4(4) Å3, Z = 4, Rgt(F) = 0.0420, wRref (F2) = 0.0988, T = 298.15 K.
Abstract C20H22Cu3N8O10, monoclinic, C2/c (no. 15), a = 12.0766(11) Å, b = 16.2778(14) Å, c = 14.7605(13) Å, β = 97.8580(10)∘, V = 2874.4(4) Å3, Z = 4, Rgt(F) = 0.0420, wRref (F2) = 0.0988, T = 298.15 K.
{"title":"Crystal structure of polybis(μ4-3,5-dicarboxylatopyrazol-1-yl)-bis(N,N-dimethylformamide)tri-copper(II)–acetonitrile (1/2), C20H22Cu3N8O10","authors":"Yan-Qing Wang, Wen-Qing Yan, Li-Xue Nie, Ping-Ping Luan, Chaomin Li","doi":"10.1515/ncrs-2023-0308","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0308","url":null,"abstract":"Abstract C20H22Cu3N8O10, monoclinic, C2/c (no. 15), a = 12.0766(11) Å, b = 16.2778(14) Å, c = 14.7605(13) Å, β = 97.8580(10)∘, V = 2874.4(4) Å3, Z = 4, Rgt(F) = 0.0420, wRref (F2) = 0.0988, T = 298.15 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":" ","pages":""},"PeriodicalIF":0.3,"publicationDate":"2023-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46253099","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of (E)-2-(2-(4-(diethylamino)styryl)-1-ethyl-1,4-dihydroquinolin-4-yl) malononitrile, C26H26N4 (E)-2-(2-(4-(二乙基氨基)苯基)-1-乙基-1,4-二氢喹啉-4-基)丙二腈C26H26N4的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-05 DOI: 10.1515/ncrs-2023-0340
Cheng-Tao Sun, Qin Li
Abstract C26H26N4, monoclinic, P21/c (no. 14), a = 16.565(2) Å, b = 17.468(2) Å, c = 7.5778(10) Å, β = 94.551(4)°, V = 2185.8(5) Å3, Z = 4, Rgt(F) = 0.0591, wRref(F2) = 0.1830, T = 300(2) K.
抽象C26H26N4，单斜，P21/C（14号），A=16565（2）'39ò，B=17468（2）'39ò，C=75778（10）'39ò，β=94551（4）°，V=2185.8（5）'39ò3，Z=4，RGT（F）=0.0591，Wrref（F2）=0.1830，T=300（2）'。
{"title":"Crystal structure of (E)-2-(2-(4-(diethylamino)styryl)-1-ethyl-1,4-dihydroquinolin-4-yl) malononitrile, C26H26N4","authors":"Cheng-Tao Sun, Qin Li","doi":"10.1515/ncrs-2023-0340","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0340","url":null,"abstract":"Abstract C26H26N4, monoclinic, P21/c (no. 14), a = 16.565(2) Å, b = 17.468(2) Å, c = 7.5778(10) Å, β = 94.551(4)°, V = 2185.8(5) Å3, Z = 4, Rgt(F) = 0.0591, wRref(F2) = 0.1830, T = 300(2) K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":" ","pages":""},"PeriodicalIF":0.3,"publicationDate":"2023-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46683637","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The crystal structure of poly[bis(μ2-1,4-bi(1-imidazolyl)benzene-κ2N:N′)bis(μ2-4,4′-methylenebis(3-hydroxy-2-naphthoate)-κ2O:O′)cobalt(II)], C35H24CoN4O6 聚[双（μ2-1,4-双（1-咪唑基）苯-κ2N:N′）双（μ2-4,4′-亚甲基双（3-羟基-2-萘甲酸酯）-κ2O:O′）钴（II）]，C35H24CoN4O6的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-04 DOI: 10.1515/ncrs-2023-0318
Ji Qi, Shu-Ying Wang, J. Chu
Abstract C35H24CoN4O6, monoclinic, P21/n (no. 14), a = 11.444(2) Å, b = 11.648(2) Å, c = 21.478(4) Å, β = 97.05(3)°, V = 2841.5(10) Å3, Z = 4, R gt (F) = 0.0849, wRref(F2) = 0.1393, T = 153(2) K.
抽象C35H24CON4O6，单斜，P21/N（No.14），A=11444（2）“，B=11648（2）“，C=21478（4）“，β=97.05（3）°，V=2841.5（10）“，Z=4，RGT（F）=0.0849，Wrref（F2）=0.1393，T=153（2）“。
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引用次数: 0
The crystal structure of 2-anilino-1,4-naphthoquinone, C10H11NO2 2-苯胺基-1,4-萘醌C10H11NO2的晶体结构
IF 0.3 4区 化学 Q4 CRYSTALLOGRAPHY
Zeitschrift Fur Kristallographie-new Crystal Structures
Pub Date : 2023-09-04 DOI: 10.1515/ncrs-2023-0338
Mohammed A. E. Elmakki, Thato N. Taoana, F. J. F. Jacobs, J. Venter
Abstract C10H11NO2, monoclinic, P21/n (no. 14), a = 3.7617(3) Å, b = 12.9267(10) Å, c = 23.4609(17) Å, β = 92.337(3)°, V = 1139.87(15) Å3, Z = 4, R gt (F) = 0.0413, wR ref (F2) = 0.1071, T = 100 K.
摘要C10H11NO2，单斜晶系，P21/n（编号14），a=3.7617（3）Oh，b=12.9267（10）Oh，c为23.4609（17）To，β为92.337（3（3）°，V为1139.87（15）Å3，Z为4，Rgt（F）=0.0413，wRref（F2）=0.1071，T为100K。
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引用次数: 0
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