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Zeitschrift fur Lebensmittel-Untersuchung und -Forschung最新文献

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[Rapid and direct lead determination in honey]. [快速直接测定蜂蜜中的铅]。
M Voget, H Baudisch

Use of honey as a biological indicator for heavy metal contamination entails the analysis of a greater number of samples. To date the complex sugar matrix required sample preparation using digestion methods, which were time consuming and involved a high risk of contamination or loss. It is now possible, using the method described here, to measure lead in honey without degradation with the help of microprocessor-programmed conditions of temperature and time in the ggraphite tube of the Atomic-Absorption-Spectrophotometer. Two samples were analysed. One had a low lead content (I), the other had a high lead content (II). The statistical variation for a series of determinations was 8.3% (I, N=10) and 5.6% (II, N=22). These results can be considered satisfactory.

使用蜂蜜作为重金属污染的生物指标需要分析更多的样本。迄今为止,复杂的糖基质需要使用消化方法制备样品,这是耗时的,并且涉及污染或损失的高风险。现在,使用本文描述的方法,在原子吸收分光光度计的石墨管中,借助微处理器编程的温度和时间条件,可以在不降解的情况下测量蜂蜜中的铅。分析了两个样本。一种是低铅含量(I),另一种是高铅含量(II)。一系列测定的统计变异为8.3% (I, N=10)和5.6% (II, N=22)。这些结果是令人满意的。
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引用次数: 0
[Detection and determination of protein-bound formaldehyde. II. Improved recovery of formaldehyde by reduction with sodium cyanoborohydride (NaCNBH3)]. 蛋白结合甲醛的检测与测定。2用氰硼氢化钠(NaCNBH3)还原甲醛提高甲醛的回收率。
W Brunn, H Klostermeyer

When using NaCNBH3 as a reductant, it is possible to recover 70% of added formaldehyde in foods--in this skim milk powder. Formaldehyde is attached to the epsilon-Aminogroups of lysine and is detected after reduction in form of N epsilon-methyllysine in an automated amino acid analyzer system. After addition of N alpha-acetyllysine the reduction is carried out by incubating the skim milk powder at 70 degrees C for 1 h. The best combination of pH, concentration of reductant, time and temperature of incubation is described.

当使用NaCNBH3作为还原剂时,可以回收70%的食品中添加的甲醛-在这种脱脂奶粉中。甲醛附着在赖氨酸的ε -氨基基团上,在自动氨基酸分析系统中以N ε -甲基赖氨酸的形式还原后检测。在脱脂奶粉中加入N -乙酰赖氨酸后,在70℃下孵育1h,对pH、还原剂浓度、孵育时间和温度的最佳组合进行了描述。
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引用次数: 0
[Laws and regulations. Eggs, egg products, egg substitutes. Federal Republic of Germany]. 法律法规。鸡蛋,蛋制品,蛋替代品。德意志联邦共和国]。
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引用次数: 0
[Efficacy and duration of chemical food preservatives]. 【化学食品防腐剂的功效和持续时间】。
M von SCHELHORN
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引用次数: 0
[Heat loss of food in hot-carts]. [热车中食物的热量损失]。
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引用次数: 0
[Injury to the hair as a basis of evaluating permanent waving preparations]. [对头发的伤害作为评估永久性烫发剂的基础]。
K E SCHULTE
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引用次数: 0
[Nes methods of identification of anti- and pro-oxygenic properties of accessory substances of natural fats]. [新方法鉴定抗氧和促氧性质的辅助物质的天然脂肪]。
W WACHS
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引用次数: 0
[Toxicity of glycols]. [乙醇的毒性]。
A W FORST
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引用次数: 0
[Structure and consistency of butter]. [黄油的结构和稠度]。
W MOHR
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引用次数: 0
Are baking aids necessary? 需要烘焙助剂吗?
J SVENSON
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引用次数: 0
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