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Pd/USY触媒による鈴木・宮浦カップリング反応 Pd/USY催化的铃木-宫浦偶联反应
Pub Date : 2010-09-10 DOI: 10.20731/ZEORAITO.27.3.81
Kazuo Okumura, 奥村和, Mikio Niwa, 丹羽幹
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引用次数: 0
Verified Synthesis of Zeolitic Materials(Synthesis Commission of IZA)の紹介 沸石材料的合成验证(IZA合成委员会)
Pub Date : 2009-06-10 DOI: 10.20731/ZEORAITO.26.2.65
S. Inagaki, 稲垣怜史, Y. Oumi, 近江靖則
{"title":"Verified Synthesis of Zeolitic Materials(Synthesis Commission of IZA)の紹介","authors":"S. Inagaki, 稲垣怜史, Y. Oumi, 近江靖則","doi":"10.20731/ZEORAITO.26.2.65","DOIUrl":"https://doi.org/10.20731/ZEORAITO.26.2.65","url":null,"abstract":"","PeriodicalId":23983,"journal":{"name":"Zeolites","volume":"115 1","pages":"65-71"},"PeriodicalIF":0.0,"publicationDate":"2009-06-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78990533","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 12
触媒調製の標準化プロジェクト(ゼオライトのイオン交換)の紹介 催化剂制备标准化项目(沸石离子交换)介绍
Pub Date : 2009-03-10 DOI: 10.20731/ZEORAITO.26.1.28
Naonobu Katada, 片田直伸
{"title":"触媒調製の標準化プロジェクト(ゼオライトのイオン交換)の紹介","authors":"Naonobu Katada, 片田直伸","doi":"10.20731/ZEORAITO.26.1.28","DOIUrl":"https://doi.org/10.20731/ZEORAITO.26.1.28","url":null,"abstract":"","PeriodicalId":23983,"journal":{"name":"Zeolites","volume":"32 1","pages":"28-31"},"PeriodicalIF":0.0,"publicationDate":"2009-03-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74077218","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
天然鉱物シリーズ(1)clinoptiloliteとheulandite 天然矿物系列(1)clinoptilolite和heulandite
Pub Date : 2008-12-10 DOI: 10.20731/ZEORAITO.25.4.155
K. Sugiyama, 杉山和正, S. Ogihara, 荻原成騎
{"title":"天然鉱物シリーズ(1)clinoptiloliteとheulandite","authors":"K. Sugiyama, 杉山和正, S. Ogihara, 荻原成騎","doi":"10.20731/ZEORAITO.25.4.155","DOIUrl":"https://doi.org/10.20731/ZEORAITO.25.4.155","url":null,"abstract":"","PeriodicalId":23983,"journal":{"name":"Zeolites","volume":"53 1","pages":"155-161"},"PeriodicalIF":0.0,"publicationDate":"2008-12-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78169979","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
ゼオライト細孔内ナノクラスターの調製,構造,触媒特性 沸石细孔内纳米簇的制备、结构和催化特性
Pub Date : 2008-06-10 DOI: 10.20731/ZEORAITO.25.2.67
Yasuaki Okamoto, 岡本康昭, T. Kadono, 角野健史, Takeshi Kubota, 久保田岳志
{"title":"ゼオライト細孔内ナノクラスターの調製,構造,触媒特性","authors":"Yasuaki Okamoto, 岡本康昭, T. Kadono, 角野健史, Takeshi Kubota, 久保田岳志","doi":"10.20731/ZEORAITO.25.2.67","DOIUrl":"https://doi.org/10.20731/ZEORAITO.25.2.67","url":null,"abstract":"","PeriodicalId":23983,"journal":{"name":"Zeolites","volume":"63 1","pages":"67-74"},"PeriodicalIF":0.0,"publicationDate":"2008-06-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90763543","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
アンモニアIRMS-TPD法とDFT(密度汎関数)計算を併用するゼオライトブレーンステッド酸性質に関する研究 联合使用氨IRMS-TPD法和DFT(密度泛函)计算的关于输液管酸性质的研究
Pub Date : 2008-03-10 DOI: 10.20731/ZEORAITO.25.1.22
Mikio Niwa, 丹羽幹, Naonobu Katada, 片田直伸, Katsuki Suzuki, 鈴木克生
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引用次数: 0
Adsorption of copper valerate on zeolite H-ZSM-5 and γ-Al2O3 沸石H-ZSM-5和γ-Al2O3对戊酸铜的吸附
Pub Date : 1997-11-01 DOI: 10.1016/S0144-2449(97)00104-8
Zeshan Hu, Junxiu Dong, Wei Li, Songying Chen, Shaoyi Peng

The adsorption of copper valerate, compared with copper nitrate, on HZSM-5 and γ-Al2O3 was studied using IR and inductively coupled plasma (ICP). The surface area and pore structure of HZSM-5 and γ-Al2O3 was measured with nitrogen physical adsorption. Results indicated a chemical adsorption of copper valerate occurred on the surface of γ-Al2O3 and external surface of HZSM-5. The =(COO)2Cu was the adsorbing group. There even existed a chemical reaction, which resulted in the formation of valeric acid.

采用红外光谱和电感耦合等离子体(ICP)研究了与硝酸铜相比,戊酸铜在HZSM-5和γ-Al2O3上的吸附性能。用氮气物理吸附法测定了HZSM-5和γ-Al2O3的比表面积和孔隙结构。结果表明,γ-Al2O3表面和HZSM-5表面均发生了对戊酸铜的化学吸附。吸附基团为=(COO)2Cu。甚至有一个化学反应,导致了戊酸的形成。
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引用次数: 2
Properties of [Ti,Al]-beta with different titanium content 不同钛含量[Ti,Al]- β的性能
Pub Date : 1997-11-01 DOI: 10.1016/S0144-2449(97)00121-8
S.L. Jahn, P.A.P. Nascente, D. Cardoso

Crystallization curves of [Ti,Al]-Beta were obtained from reaction mixtures having Si/Ti ratios between 20 and 125 and Si/Al approx. 200. It was observed that practically all aluminum is incorporated into the solid during the first hours of reaction, whereas titanium and silicon are continuously incorporated. Increasing Ti content in the reaction mixture results in an increase in particle size, indicating that the presence of Ti reduces the nucleation rate. X-ray diffraction and diffuse reflectance spectra show that when the Ti content is less than 4% of the tetrahedral atoms, this element is incorporated in the sieve framework in isolated form.

在Si/Ti比值为20 ~ 125、Si/Al近似的反应混合物中,得到了[Ti,Al]- β的结晶曲线。200. 据观察,在反应的最初几个小时内,几乎所有的铝都被掺入固体中,而钛和硅则不断被掺入。反应混合物中Ti含量的增加导致颗粒尺寸的增大,表明Ti的存在降低了成核速率。x射线衍射和漫反射光谱表明,当Ti含量低于4%的四面体原子时,该元素以孤立形式结合在筛骨架中。
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引用次数: 11
Patent report 专利报告
Pub Date : 1997-11-01 DOI: 10.1016/S0144-2449(97)00135-8
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引用次数: 0
Solid-state defects in calcined CaA zeolite 煅烧CaA沸石的固态缺陷
Pub Date : 1997-11-01 DOI: 10.1016/S0144-2449(97)00120-6
Hideyuki Oka, Kunikazu Kamioka, Yuji Tokunaga, Tadashi Okada

Ca ion-exchanged zeolites have been characterized by electron spin resonance (e.s.r.), 27Al magic-angle spinning nuclear magnetic resonance (MAS n.m.r.), 29Si MAS n.m.r., and diffuse reflectance Fourier transform infrared spectroscopy (i.r.). The presence of the radical species that are assigned to solid-state defects was confirmed in CaA zeolites, and the amount of the radical was dependent on the thermal treatment temperature in air. The present experimental results suggest that the formation of extralattice aluminum in the CaA sodalite cage and the change of calcium species by thermal treatment relate to the formation and disappearance of radical species.

采用电子自旋共振(e.s.r)、27Al魔角自旋核磁共振(MAS n.m.r)、29Si MAS n.m.r和漫反射傅里叶变换红外光谱(i.r)对钙离子交换沸石进行了表征。在CaA沸石中,被分配到固态缺陷的自由基物种的存在得到了证实,并且自由基的数量取决于空气中的热处理温度。实验结果表明,CaA钠岩笼中晶格外铝的形成和热处理过程中钙种类的变化与自由基种类的形成和消失有关。
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引用次数: 2
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