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Improving the Erosion Behavior of Inconel 625 Substrate by PTA-Deposited Stellite6/B4C Composite Cladding PTA沉积钨铬钴合金6/B4C复合镀层改善铬镍铁合金625基体的腐蚀行为
Pub Date : 2022-11-01 DOI: 10.47176/jame.41.2.24331
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引用次数: 0
A Review of Resistive Gas Sensors Based on Semiconducting Metal Oxides 基于半导体金属氧化物的电阻式气体传感器研究进展
Pub Date : 2022-11-01 DOI: 10.47176/jame.41.2.20741
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引用次数: 0
Investigation of Photocatalytic Properties of TiO2 and TiO2-4wt.%CdO Nanoparticles for Degradation of Methylene Blue TiO2和TiO2-4wt%光催化性能的研究CdO纳米粒子降解亚甲蓝的研究
Pub Date : 2022-11-01 DOI: 10.47176/jame.41.2.24451
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引用次数: 0
The Influence of Peroxides and Washing Process on Metal-Organic Framework of MOF-5 Synthesized by Direct Mixing Method 过氧化物和洗涤工艺对直接混合法合成MOF-5金属有机骨架的影响
Pub Date : 2022-11-01 DOI: 10.47176/jame.41.2.22143
A. Mehdikhani, H. Fallah-Arani, F. Dabir, A. Ghanbari
In this research, the effect of hydrogen peroxide (H 2 O 2 ) and benzoyl peroxide (BPO) on the structural properties, porosity, active pores, and surface area of the MOF-5 (Zn 4 O(BDC) 3 ) metal-organic framework was studied. For this purpose, the metal-organic framework was synthesized by direct mixing and the molar ratios of the precursors to the ligand were modified to minimize the stoichiometric calculation error as well as the washing process to improve the properties of the synthesized MOF-5. In order to characterize the synthesized compounds and to investigate the effect of peroxides and washing process on the properties of the samples, X-ray diffraction (XRD), fourier Transform infrared spectroscopy (FTIR), and thermogravimetric/Differential scanning calorimetry (TG-DSC) analysis were performed. Structure, pore volume (1.212 cm 3 /g), and specific surface area (2307 m 2 /g) were compared to the sample synthesized with H 2 O 2 . DM-P-03 was selected as the optimal sample and prepared for thermal stability. According to TG-DSC analysis, the remaining zinc compounds in the sample were checked and the thermal stability of MOF-5 structure was confirmed up to 470°C.
研究了过氧化氢(H2 O2)和过氧化苯甲酰(BPO)对MOF-5(Zn4O(BDC)3)金属有机骨架的结构性能、孔隙率、活性孔和表面积的影响。为此,通过直接混合合成金属-有机骨架,并修改前体与配体的摩尔比以最小化化学计量计算误差,以及洗涤过程以改善合成的MOF-5的性能。为了表征合成的化合物,并研究过氧化物和洗涤工艺对样品性能的影响,进行了X射线衍射(XRD)、傅立叶变换红外光谱(FTIR)和热重/差示扫描量热法(TG-DSC)分析。将结构、孔体积(1.212cm 3/g)和比表面积(2307m2/g)与H2 O2合成的样品进行了比较。选择DM-P-03作为最佳样品并制备热稳定性。根据TG-DSC分析,检查了样品中剩余的锌化合物,并确认MOF-5结构的热稳定性高达470°C。
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引用次数: 0
Investigating the Effect of B, Sb, and Ge Elements on the Structural and Magnetic Properties of Rare Earth Elements -Free Permanent MnBi Magnets B、Sb和Ge元素对无稀土永久MnBi磁体结构和磁性能影响的研究
Pub Date : 2022-11-01 DOI: 10.47176/jame.41.2.21461
M. Tavoosi, Gh.R. Gordani, A. Ghasemi, H. Jamali, M. L. Estarki
The goal of this study was the investigation of the structural and magnetic characteristics of MnBi permanent magnets. In this regard, the mechanical milling and annealing processes were used for the synthesis of Mn 45 Bi 50 M 5 (M= Sb, Ge, B) samples. Based on the results, the best annealing temperature and time for the formation of the highest value of MnBi ferromagnetic phase with optimum magnetic properties (Hc=1750 Oe and Ms= 12 emu/g) were recognized at 325 o C and 24 h, respectively. B, Ge, and Sb elements had a distractive effect on the stabilization of the MnBi ferromagnetic phase. Consequently, the samples containing B, Ge, and Sb showed lower magnetic characteristics in comparison with the Mn 50 Bi 50 stoichiometric sample.
本研究的目的是研究MnBi永磁体的结构和磁性。为此,采用机械铣削和退火工艺合成了Mn 45 Bi 50 m5 (M= Sb, Ge, B)样品。结果表明,在325℃和24 h时,形成MnBi铁磁相的最佳退火温度和时间分别为Hc=1750 Oe和Ms= 12 emu/g。B、Ge和Sb元素对MnBi铁磁相的稳定有分散作用。结果表明,含B、Ge和Sb的样品比含mn50bi 50的样品具有更低的磁性。
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引用次数: 0
FABRICATION AND CHARACTERIZATION OF MICROSTRUCTURE AND MECHANICAL PROPERTIES OF NANOCOMPOSITES BASED ON NICRALY ALLOY REINFORCED WITH SI3N4 PARTICLES BY SPARK PLASMA SINTERING METHOD 火花等离子烧结法制备SI3N4增强镍基合金纳米复合材料及其微观结构和力学性能研究
Pub Date : 2022-08-01 DOI: 10.47176/jame.41.1.24191
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引用次数: 0
CHARACTERIZATION OF CHITOSAN AND POLYETHYLENE GLYCOL BIOPOLYMERS COATINGS ON MAGNETIC SPINEL FeFe2O4 NANOPARTICLES 磁性自旋FeFe2O4纳米粒子上壳聚糖和聚乙二醇生物聚合物涂层的表征
Pub Date : 2022-08-01 DOI: 10.47176/jame.41.1.02203
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引用次数: 0
EFFECT OF TOOL ROTATION RATE IN FRICTION STIR SPOT WELDING ON LIQUATION CRACKING OF AZ91 ALLOY 搅拌摩擦点焊工具转速对AZ91合金液化开裂的影响
Pub Date : 2022-08-01 DOI: 10.47176/jame.41.1.24261
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引用次数: 0
INVESTIGATION OF THE ADDITION OF METHIONINE ON THE CORROSION OF 316L STAINLESS STEEL FABRICATED BY SLM METHOD IN SULFURIC ACID MEDIA 蛋氨酸对SLM法制备316L不锈钢在硫酸介质中腐蚀的影响
Pub Date : 2022-08-01 DOI: 10.47176/jame.41.1.23391
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引用次数: 0
EVALUATION OF ANTIBACTERIAL PROPERTIES OF POLYLACTIC ACID-POLYCAPROLACTONE-CONTAINING HYDROXYAPATITE AND ZINC OXIDE NANOPARTICLES IN HARD TISSUE ABSORBABLE SCAFFOLDS 聚乳酸-聚己内酯羟基磷灰石和氧化锌纳米颗粒在硬组织可吸收支架中的抗菌性能评价
Pub Date : 2022-08-01 DOI: 10.47176/jame.41.1.23881
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引用次数: 0
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