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Cyclic voltammogram analysis of the environmental aspects of the use of ferrocenyl carbinols 使用二茂铁羰基甲醇的环境方面的循环伏安分析
Pub Date : 2021-12-01 DOI: 10.55923/jo.ijeal.2.4.202
ahmad alkawaldeh
Ferrocene and its derivatives have ecologically effective antidetane properties. In this regard, ferrocene reacts with cyclic ketones and ferrosenylcarbinols are synthesized. It should be noted that ferrocene enters into electrophilic reactions and the process takes place in an acidic environment. In addition, the yield of the new product was small compared to the reactions of ferrocene with non-cyclic ketones. This is due to the spatial structures of molecules. The elemental analysis of obtained compounds was carried out; the structures were researched by cyclic voltammograms and Chronoamperometric.
二茂铁及其衍生物具有生态上有效的对烷性质。在这方面,二茂铁与环酮反应和二茂铁羰基醇合成。值得注意的是,二茂铁进入亲电反应,该过程发生在酸性环境中。此外,与非环酮与二茂铁的反应相比,新产物的产率较小。这是由于分子的空间结构。对所得化合物进行了元素分析;采用循环伏安法和计时安培法对其结构进行了研究。
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引用次数: 0
Technology patterns in Nanochemistry Based on GII Indicator 基于GII指标的纳米化学技术模式
Pub Date : 2021-09-01 DOI: 10.55923/jo.ijeal.2.3.703
A. Alkhawaldeh
Trends focused on the Global Innovation Index (GII) as a measure for progress of nanochemistry. This paper provides projections of recent developments in the word in nanochemistry based on the Global Innovation Index as a predictor for certain Arab countries. The GII is an annual ranking of countries by its ability and performance in innovation and is calculated on a basic average from five and two pillars in two sub-indexes, the Innovation Input Index and the Innovation Output Index. Each pillar represents a trait of creativity and consists of up to five measures, with a weighted average formula for measuring their ranking. In 2008, the GII rose to 36.3 in 2016 from 0.5. The GII is smaller than the GII in Arabic countries worldwide. During the years 2013-2016, the worldwide GII was increasing while for the same period, for Arabic countries, this decline could be explained by economic and industrial wars in the Arab region.
趋势集中在全球创新指数(GII)作为纳米化学进展的衡量标准。本文以全球创新指数作为某些阿拉伯国家的预测指标,对世界纳米化学的最新发展进行了预测。全球创新指数是根据各国在创新方面的能力和表现对其进行的年度排名,它是根据创新投入指数和创新产出指数这两个子指数的五个和两个支柱的基本平均值计算得出的。每一项指标都代表了创造力的一种特征,由多达五项指标组成,用加权平均公式来衡量它们的排名。2008年,全球创新指数从0.5上升至2016年的36.3。GII比全球阿拉伯国家的GII要小。在2013-2016年期间,全球GII呈上升趋势,而在同一时期,对于阿拉伯国家来说,这种下降可以解释为阿拉伯地区的经济和工业战争。
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引用次数: 1
THE EFFECTIVENESS OF "Click Click" TEACHING STRATEGY IN THE ACADEMIC PERFORMANCE OF GRADE SIX LEARNERS IN MATHEMATICS “咔哒咔哒”教学策略对六年级数学学习成绩的影响
Pub Date : 2021-07-01 DOI: 10.55923/jo.ijeal.2.21.405
Shallimar A. Bayucca
This study aimed to determine the effect of “Click Click” strategy in the academic performance of Grade six pupils in Mathematics. The study used an experimental method using posttest only design with a 20-item test questionnaire as an instrument to gather data from ninety-six (96) respondents using convenience sampling technique. This study used Microsoft Excel data analysis to treat the data with the use of the following statistical tools: weighted mean, standard deviation, and t-test. Result shows that the control group’s mean score was interpreted as having “Average Mastery” of the lesson upon receiving traditional way of teaching. While the mean score of the experimental group showed “Closely Approximating Mastery” of the lessons after receiving the “Click Click” strategy. The mean score of the experimental group is higher than the mean score of the control group. In addition, since the computed T-value is greater than the tabular value/ critical value, it rejects the null hypothesis which further means that there is a significant difference in the mean score on the posttest between the control and experimental groups. With the foregoing results, the researcher recommended using PowerPoint presentations with interactive slides to involve them in the teaching-learning process since pupils learn, play, and is entertained all in one. The result encourages school Administrators to provide the teachers opportunities to update themselves on the use of technology for them to be adept with the demands of their work in the present generation.
本研究旨在探讨“咔哒咔哒”策略对六年级小学生数学学业成绩的影响。本研究采用仅后测设计的实验方法,以20项测试问卷为工具,采用方便抽样技术对96名调查对象进行数据收集。本研究采用Microsoft Excel数据分析,采用加权均值、标准差、t检验等统计工具对数据进行处理。结果表明,在接受传统教学方式时,对照组的平均分被解释为对课程的“平均掌握”。实验组学生在接受“咔哒咔哒”策略后的平均成绩为“接近掌握”。实验组的平均得分高于对照组的平均得分。此外,由于计算的t值大于表格值/临界值,因此拒绝原假设,这进一步意味着对照组和实验组之间的后测平均得分存在显著差异。根据上述结果,研究人员建议使用带有互动幻灯片的PowerPoint演示文稿,让他们参与到教学过程中来,因为学生们学习、玩耍和娱乐是一体的。这一结果鼓励学校管理者为教师提供机会,让他们更新自己对技术的使用,使他们能够熟练地适应这一代人的工作要求。
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引用次数: 0
Potential pharmacological Therapeutics options for COVID-19: Review COVID-19的潜在药物治疗方案:综述
Pub Date : 2021-07-01 DOI: 10.55923/jo.ijeal.2.21.406
A. Alkhawaldeh
Unusual pneumonia result from unknown pathogen was emerged in December 2019 in a seafood market of Wuhan city in China. The pathogen was soon identified as a novel coronavirus (2019-nCoV), which is closely related to sever acute respiratory syndrome CoV (SARS-CoV) which has taken the world to the edge of health emergency. On 11th March 2020, COVID-19 was declared a pandemic by the World Health Organization. SARS-CoV-2 belongs to the family of Coronaviridae. Corona virus has been reported to cause similar morbific impacts on the lower respiratory system. Transmits occurs when people breathe in air contaminated by droplets and small airborne particles. Transmission can also occur if sprayed with contaminated fluids, in the eyes, nose or mouth. People remain contagious for up to 20 days, and can spread the virus even if they do not develop any symptoms. Although this disease primarily targets lungs, damages in other organs, such as heart, kidney, liver, and testis, may occur.
2019年12月,中国武汉市某海鲜市场出现不明病原体感染的异常肺炎。该病原体很快被确定为新型冠状病毒(2019-nCoV),与将世界推向卫生紧急状态的严重急性呼吸综合征冠状病毒(SARS-CoV)密切相关。2020年3月11日,世界卫生组织宣布COVID-19为大流行。SARS-CoV-2属于冠状病毒科。据报道,冠状病毒会对下呼吸系统造成类似的致病影响。当人们吸入被飞沫和空气中的小颗粒污染的空气时,就会传播。如果被污染的液体喷洒在眼睛、鼻子或嘴巴中,也可能发生传播。人们保持传染性长达20天,即使他们没有出现任何症状,也可以传播病毒。虽然这种疾病主要针对肺部,但也可能损害其他器官,如心脏、肾脏、肝脏和睾丸。
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引用次数: 0
A Vision Future for Application Artificial Intelligent in Solar Energy 人工智能在太阳能中的应用前景展望
Pub Date : 2021-03-01 DOI: 10.55923/jo.ijeal.2.1.602
A. Alkhawaldeh, M. Albzeirat, Kadhim H. Suffer, N. Zulkepli
This research paper aims to review the applications of artificial intelligence in energy and to develop a future vision for new applications. The research methodology focuses on clarifying the basic concepts of approaches to artificial intelligence (AI) and renewable energy and developing a visualization of the link between them.
本研究论文旨在回顾人工智能在能源领域的应用,并对未来的新应用进行展望。研究方法的重点是澄清人工智能(AI)和可再生能源方法的基本概念,并开发它们之间联系的可视化。
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引用次数: 0
Electrochemical Sensors and Determination for Heavy Metal by Rotating Disk Platinum Electrode and Chronoamperometric Method 旋转圆盘铂电极电化学传感器及计时安培法测定重金属
Pub Date : 2020-11-25 DOI: 10.20944/preprints202011.0628.v1
A. Alkhawaldeh, Ayat Alzawahreh, Rawia Alkhawaldeh
Pollution by heavy metals is one of the most severe environmental issues that threaten global sustainability. This review presents a recent advance in electrochemical sensors for heavy metal detection Rotating Disk Platinum Electrode are discussed. This study on the production of a modern natural water electrochemical antimony (II) and cupper (II) test include the use of platinum electrode. Antimony and cupper were pre-concentrated on the modified electrode surface and adsorbed to the surface, oxidizing at E = 540 mV and E = 85 mV, respectively. After 20 min of accumulation, time the best-defined anodic peak was obtained of surface. The precision was tested by carrying out chronoamperometric measurements at a concentration of Sb+2 and Cu+2 8.5x10-8 M and 9.5x10-7 M, respectively.
重金属污染是威胁全球可持续发展的最严重的环境问题之一。综述了近年来用于重金属检测的电化学传感器的研究进展,并对旋转圆盘铂电极进行了讨论。本课题研究了现代天然水中锑(II)和铜(II)的电化学制备方法,包括使用铂电极进行测试。将锑和铜预浓缩在修饰后的电极表面并吸附在表面,分别在E = 540 mV和E = 85 mV下氧化。积累20min后,获得了最佳定义的表面阳极峰。在Sb+2和Cu+2的浓度分别为8.5x10-8 M和9.5x10-7 M的情况下,通过计时电流测量来测试其精度。
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引用次数: 1
Intelligent Medical Companion using Internet of Things 使用物联网的智能医疗伴侣
Pub Date : 2020-09-01 DOI: 10.55923/jo.ijeal.1.4.505
A. Alkhawaldeh, Rawia Alkhawaldeh, Adeeb Ibrahim
Improvement in quality of health and medicine has become of paramount importance. The solution to this problem requires a wearable device for continuous monitoring for the patient. As a result, Medical companion was the best choice for the patient who suffers Arrhythmia due to its low-cost and efficacy to save the life of the patient. Moreover, this system is able to deliver reliable heartbeat and body temperature data to a user in a real-time, with a smart mobile application. This system mainly consists of MAX30100 and LM35 that detect heart rate and temperature of the human respectively. The output of these sensors is given to the esp32 section, which runs an Arrhythmia algorithm, which is already programmed, into it. If an abnormal heartbeat is detected, then it activates the alert in the mobile application. This mobile application will automatically send an alert message for the emergency centre and the patient's caregiver; thereby the life of the person can be saved.
提高保健和医疗质量已变得极为重要。要解决这个问题,需要一种可穿戴设备对患者进行持续监测。因此,医疗伴侣以其低成本和有效挽救患者生命的优势成为心律失常患者的最佳选择。此外,该系统能够通过智能移动应用程序实时向用户提供可靠的心跳和体温数据。该系统主要由MAX30100和LM35组成,分别检测人体心率和体温。这些传感器的输出被提供给esp32部分,该部分运行心律失常算法,该算法已经被编程到其中。如果检测到异常心跳,它就会在移动应用程序中激活警报。这个移动应用程序将自动向急救中心和病人的护理人员发送警报信息;因此,这个人的生命可以被挽救。
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引用次数: 0
Platinum Nanoparticles for the Electrochemical Study of Heavy Metal ions Formed by the Sputtering Deposition of the ion beam Electrode 铂纳米粒子在离子束电极上溅射沉积形成重金属离子的电化学研究
Pub Date : 2020-06-02 DOI: 10.20944/preprints202006.0342.v1
A. Alkhawaldeh
An electrochemical sensing platinum nanoparticle in the tantalum electrode is provided by means of an Ion Beam Sputtering Deposition (IBSD). The electrode was made with a Pt solution, sputtered simultaneously with hydrochloric acid corrosion on tantalum substrate. In the study of heavy metal ions, for example, the platinum nanoparticle electrodes as prepared were used Square wavelength voltammetry (OSWV) Hg2+, Cu2+ and Ag2+. The porous electrodes were observed in a broader range by the Pt nanostructure electrode for heavy metal ions. Furthermore, the susceptibility to detection has been shown to be saturated as the thickness of the layer electrode exceeded 50 nm. For Hg2+ 0,003-1 M, for Cu2+ 0,005-3 M and for Ag2+ the linear detection scale is 0,009-4 M. There has also been good reusability and repeatability. In addition, a scan electron microscope (SEM) used to study platinum electrode forming process and nanostructure. This electrode will have interesting applications in sensing systems.
通过离子束溅射沉积(IBSD)的方法,在钽电极中制备了电化学传感铂纳米粒子。电极是用铂溶液在钽衬底上与盐酸腐蚀同时溅射制备的。以重金属离子研究为例,所制备的铂纳米粒子电极分别采用方波伏安法(OSWV) Hg2+、Cu2+和Ag2+。Pt纳米结构电极对重金属离子的多孔电极的观察范围更广。此外,当层电极的厚度超过50 nm时,检测敏感性达到饱和。对Hg2+ 0.003 -1 M、Cu2+ 0.005 -3 M和Ag2+的线性检测尺度为0.009 -4 M,具有良好的可重复使用性和重复性。此外,利用扫描电子显微镜(SEM)研究了铂电极的形成过程和纳米结构。这种电极将在传感系统中有有趣的应用。
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引用次数: 5
Electrochemical Analysis of Heavy metal by Cyclic Voltammetry Method 循环伏安法电化学分析重金属
Pub Date : 2020-06-01 DOI: 10.55923/jo.ijeal.2.2.402
A. Alkhawaldeh
Bismuth and Bismuth oxides are well-known electro-catalysts in fuel cells systems; they are usually used as anodic materials for the oxidation of low molecular weight alcohols. The utilization of BiO2 and MnO2 as catalysts in the pharmaceutical analysis is analytical method for the determination of heavy metal antibacterial agents in Pharmaceutical Dosage form is developed. The method is based on the voltammetric determination of heavy metal using Bidified platinum electrode by Bismuth oxide. The two components are oxidized at the Bidified electrode surface with the development of current that is linearly proportional to their concentrations in the range of 7.04*10-7- 1*10-3 M heavy metal. The oxidation reaction of the two components is pH-dependent, in which the buffer used is Britton-Robinson at pH = 7.00 where maximum peak current and maximum peak separation is obtained. The regression factors obtained from the calibration curves are 0.9812. The method of analysis was validated, where the limit of detection (LOD) and the limit of quantitation (LOQ) were calculated to be 1.44*10-4 M, 4.36*10-4 M and 1.27*10-4 M, 3.84*10-4 M respectively, The percentage recovery of both components was also calculated to 77 % for heavy metal.
铋和铋氧化物是燃料电池系统中众所周知的电催化剂;它们通常用作氧化低分子量醇的阳极材料。建立了利用二氧化硅和二氧化锰作为催化剂进行药物分析的方法,用于药物剂型中重金属抗菌剂的测定。建立了用氧化铋氧化双铂电极伏安法测定重金属的方法。在7.04*10-7- 1*10-3 M的重金属浓度范围内,这两种组分在双相化电极表面被氧化,电流的发展与它们的浓度成线性正比。两组分的氧化反应是pH依赖性的,其中使用的缓冲液为briton - robinson, pH = 7.00时获得最大的峰电流和最大的峰分离。标定曲线的回归因子为0.9812。对分析方法进行验证,其检出限(LOD)和定量限(LOQ)分别为1.44*10-4 M、4.36*10-4 M和1.27*10-4 M、3.84*10-4 M,重金属的回收率均为77%。
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引用次数: 1
Highly Sensitive Copper Heavy Metal Analysis on Nanoparticle Platinum and Palladium Electrode 纳米颗粒铂和钯电极上铜重金属的高灵敏度分析
Pub Date : 2020-05-05 DOI: 10.20944/preprints202005.0069.v1
A. Alkhawaldeh, Rawia Alkhawaldeh
The copper deposition on the platinum and palladium nanoelectrode has been studied using cyclic voltammetry. The use of nanoelectrode platinum and palladium are defined in the study of heavy metals. The noble nanoelectrode of metal has a typical silicone processing structure. In comparison to the nanoelectrodes, the geometry of the electrode series is complex and balanced. Nanoelectrodes of platinum are found effective in detecting heavy metal. There was regular analysis of the use of the sensors. The identification constraints down to the ng /L level was accomplished by refined electrode geometry and the stripping procedures. The process was used for the study of water sample determination. Another heavy metal ion attack voltammetric reaction was studied. The SEM picture clearly observed and characterized the nanoparticle electrode by X-ray diffraction and cyclic voltammetry.
用循环伏安法研究了铜在铂和钯纳米电极上的沉积。定义了纳米电极铂和钯在重金属研究中的应用。贵金属纳米电极具有典型的有机硅加工结构。与纳米电极相比,电极系列的几何结构复杂而平衡。铂纳米电极是检测重金属的有效材料。对传感器的使用情况进行了定期分析。通过改进电极几何形状和剥离程序,鉴定约束降低到ng /L水平。将该方法用于水样测定的研究。研究了另一种重金属离子攻击伏安反应。通过x射线衍射和循环伏安法对纳米颗粒电极的SEM图进行了清晰的观察和表征。
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引用次数: 6
期刊
International Journal of Engineering and Artificial Intelligence
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