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On the microstructure and tensile properties of Inconel 718 alloy fabricated by selective laser melting and conventional casting 选择激光熔化法和常规铸造法制备Inconel 718合金的显微组织和拉伸性能
Q3 Engineering Pub Date : 2021-10-06 DOI: 10.1142/s2424913021410034
Minglin He, Y. Ni, Shuai Wang
In this work, we investigated the microstructure and tensile properties of Inconel 718 alloy processed by selective laser melting (SLM) and conventional casting technique using multiscale characterization methods. Results indicated that a columnar grain structure containing cellular structure units with submicron size was the major feature in the as-printed Inconel 718 alloy. At the cellular structure boundaries, the high-density dislocation tangles, segregation of Nb/Mo atoms and nano-sized Laves phases were found. Meanwhile, we also observed dislocation pile-ups and stacking faults in the interior of the cellular structure. In contrast, in the as-cast Inconel 718 alloy, both the grains and Laves phases were much coarser. Discrete dislocations, dislocation tangles and [Formula: see text]” precipitates were locally observed in the grains. Tensile results showed the as-printed Inconel 718 alloy had a higher strength and a lower elongation in comparison with those in the as-cast alloy. Based on the experimental results, the formation mechanism of the cellular structure was discussed.
本文采用多尺度表征方法研究了选择性激光熔化(SLM)和常规铸造工艺制备的Inconel 718合金的显微组织和拉伸性能。结果表明:印态Inconel 718合金的主要特征是含有亚微米大小的细胞结构单元的柱状晶粒结构;在细胞结构边界处,发现了高密度的位错缠结、Nb/Mo原子的偏析和纳米Laves相。同时,我们还观察到在细胞结构内部存在位错堆积和层错。相比之下,铸态Inconel 718合金的晶粒和Laves相都要粗得多。在晶粒中局部观察到离散位错、位错缠结和[公式:见文本]。拉伸结果表明,与铸态合金相比,打印态的Inconel 718合金具有更高的强度和更低的延伸率。在实验结果的基础上,讨论了细胞结构的形成机理。
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引用次数: 4
Preface: Special Issue on Mechanical Behaviours of Functional Materials and Structures 前言:《功能材料与结构的力学行为》特刊
Q3 Engineering Pub Date : 2021-09-01 DOI: 10.1142/s2424913021020021
Jinglei Yang, David May, Erfan Kazemi, L. Chang
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引用次数: 0
Influence of the base material on the mechanical behaviors of polycrystal-like meta-crystals 基体材料对类多晶偏晶力学行为的影响
Q3 Engineering Pub Date : 2021-08-27 DOI: 10.1142/s2424913021500041
J. Lertthanasarn, C. Liu, M. Pham
Architected lattice metamaterials offer extraordinary specific strength and stiffness that can be tailored through the architecture. Meta-crystals mimic crystalline strengthening features in crystalline alloys to obtain high strength and improved post-yield stability of lattice materials. This study investigates synergistic effects of the base material’s intrinsic crystalline microstructure and architected polycrystal-like architecture on the mechanical behavior of architected metamaterials. Four different polygrain-like meta-crystals were fabricated from 316L, Inconel 718 (IN718) and Ti6Al4V via laser powder bed fusion (L-PBF). While the elastic modulus of the meta-crystals did not vary significantly with the base material or the number of meta-grains, the strength of the meta-crystals showed strong increasing correlation with reducing the size of meta-grains. The differences between meta-crystals made by the three alloys were the most substantial in the post-yield behavior, where the 316L meta-crystals were the most stable while Ti6Al4V meta-crystals were the most erratic. The differences in the post-yield behavior were attributed to the base material’s ductility and intrinsic work-hardening. For all base materials, increasing the number of meta-grains improved the post-yield stability of meta-crystals. The tolerance to the processing defects also differed with the base material. Detrimental defects such as the high surface roughness on the downskin of the struts or the large, irregularly shaped pores near the surface of the struts led to early strut fracture in Ti6Al4V meta-crystals. In contrast, ductile IN718 was able to tolerate such defects, enabling the most significant synergistic strengthening across lengthscales to achieve architected materials of low relative density, but with a very high strength and an excellent energy absorption.
建筑晶格超材料提供了非凡的比强度和刚度,可以通过建筑进行定制。偏晶模拟结晶合金中的结晶强化特征,以获得高强度和改进的晶格材料的屈服后稳定性。本研究研究了基底材料的固有晶体微观结构和建筑类多晶体结构对建筑超材料力学行为的协同效应。以316L、铬镍铁合金718(IN718)和Ti6Al4V为原料,通过激光粉末床熔融(L-PBF)制备了四种不同的类聚晶亚晶。虽然元晶体的弹性模量没有随着基体材料或元晶粒的数量而显著变化,但元晶体的强度随着元晶粒尺寸的减小而表现出强烈的增加相关性。三种合金制备的偏晶之间的后屈服行为差异最大,其中316L偏晶最稳定,而Ti6Al4V偏晶最不稳定。屈服后行为的差异归因于基材的延展性和内在加工硬化。对于所有基体材料,增加偏晶粒的数量提高了偏晶体的屈服后稳定性。对加工缺陷的容忍度也因基材而异。有害缺陷,如支柱的下表皮上的高表面粗糙度或支柱表面附近的大的、不规则形状的孔隙,导致Ti6Al4V偏晶中的早期支柱断裂。相比之下,韧性IN718能够容忍这样的缺陷,使得能够在纵向范围内进行最显著的协同强化,以实现低相对密度但具有非常高的强度和优异的能量吸收的建筑材料。
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引用次数: 1
High strength Al alloy development for laser powder bed fusion 激光粉末床熔合用高强度铝合金的研制
Q3 Engineering Pub Date : 2021-07-16 DOI: 10.1142/S2424913021410010
Jin'e Sun, Baicheng Zhang, X. Qu
High strength Al alloy development is the key technique to additive manufacturing (AM) applied on lightweight of aerospace, automotive and military industry. Unlike the conventional wrought Al–Si eutectic alloys available for AM process, the strength of new developed Al alloy can be improved by in situ or additional nano-precipitated phase. This paper presents an overview of high strength Al alloys development including metallic additives, such as Zr, Sc, Mn, Cu, etc., and nanoparticle additives, such as ceramics (TiB2, TiC, LaB6 and TiN) as well as carbon nanotubes (CNTs). The addition of Zr and Sc elements significantly prevents hot tearing and enhances the strength of laser processed Al alloys because the nanoscale Al3Zr, Al3Sc and Al3 (Sc, Zr) precipitated phases generate, facilitate the heterogeneous nucleation of Al matrix and refine the microstructure. Moreover, the addition of Mn and Cu elements provides an increment in the toughness and strength of laser processed Al alloys through the superimposed effect of multi-element solid solution reinforcement and precipitation strengthening role of some Al2CuMg and Al6Mn. The growth process of Al alloy can be interrupted by the addition of nanoceramics particles as additional nucleation site which leads the columnar grain transforms to the equiaxed grain. Furthermore, the mechanism of mutual solubility of LaB6, TiB2, TiC and TiN in Al alloys is systematically studied. Finally, an assessment of the state in laser processed high strength Al alloys and the research demands for the expansion of laser powder bed fusion of Al metallic components are provided.
高强度铝合金的开发是增材制造在航空航天、汽车、军工等轻量化领域应用的关键技术。与可用于AM工艺的传统锻造Al–Si共晶合金不同,新开发的Al合金的强度可以通过原位或添加纳米沉淀相来提高。本文概述了高强度铝合金的发展,包括金属添加剂,如Zr、Sc、Mn、Cu等,以及纳米颗粒添加剂,如陶瓷(TiB2、TiC、LaB6和TiN)和碳纳米管(CNTs)。Zr和Sc元素的加入显著防止了热撕裂,并提高了激光加工Al合金的强度,因为纳米级Al3Zr、Al3Sc和Al3(Sc,Zr)沉淀相的产生,促进了Al基体的非均匀成核并细化了微观结构。此外,Mn和Cu元素的加入通过多元素固溶体增强和一些Al2CuMg和Al6Mn的沉淀增强作用的叠加作用,提高了激光加工铝合金的韧性和强度。通过添加纳米陶瓷颗粒作为额外的成核位点,可以中断铝合金的生长过程,使柱状晶粒转变为等轴晶粒。此外,系统地研究了LaB6、TiB2、TiC和TiN在铝合金中的互溶机理。最后,对激光加工高强度铝合金的状态进行了评估,并对铝金属构件的激光粉末床熔接扩展提出了研究要求。
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引用次数: 8
On Eshelby’s inclusion problem in nonlinear anisotropic elasticity 非线性各向异性弹性中的Eshelby包含问题
Q3 Engineering Pub Date : 2021-06-28 DOI: 10.1142/s2424913021500028
A. Yavari
In this paper, the recent literature of finite eignestrains in nonlinear elastic solids is reviewed, and Eshelby’s inclusion problem at finite strains is revisited. The subtleties of the analysis of combinations of finite eigenstrains for the example of combined finite radial, azimuthal, axial and twist eigenstrains in a finite circular cylindrical bar are discussed. The stress field of a spherical inclusion with uniform pure dilatational eigenstrain in a radially-inhomogeneous spherical ball made of arbitrary incompressible isotropic solids is analyzed. The same problem for a finite circular cylindrical bar is revisited. The stress and deformation fields of an orthotropic incompressible solid circular cylinder with distributed eigentwists are analyzed.
本文综述了非线性弹性固体中有限应变的最新文献,并重新讨论了有限应变下的Eshelby包含问题。以有限圆柱杆中有限径向、方位、轴向和扭转本征应变的组合为例,讨论了有限本征应变组合分析的微妙之处。分析了由任意不可压缩各向同性固体组成的径向非均匀球形球体中具有均匀纯膨胀本征应变的球形夹杂的应力场。对有限圆柱杆的相同问题进行了重新讨论。分析了具有分布本征扭曲的正交各向异性不可压缩固体圆柱的应力场和变形场。
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引用次数: 5
Machine learning-based prediction of the translaminar R-curve of composites from simple tensile test of pre-cracked samples 预裂样品简单拉伸试验中基于机器学习的复合材料跨层r曲线预测
Q3 Engineering Pub Date : 2021-06-28 DOI: 10.1142/s2424913020500174
Cheng Qiu, Yu-Lin Han, L. Shanmugam, Zhidong Guan, Zhong Zhang, Shanyi Du, Jinglei Yang
A novel approach to determine the translaminar crack resistance curve of composite laminates by means of a machine learning model is presented in this paper. The main objective of the proposed method is to extract hidden information of crack resistance from strength values of center-cracked laminates. Compared to traditional measurements, the notable advantage is that only tensile strength values are required which can be obtained by a rather simpler experimental procedure. This is achieved by the incorporation of the finite fracture mechanics, which links crack resistance with strength values. In order to get training dataset, a semi-analytical method using both finite element method and finite fracture mechanics is employed to generate strength values of center-cracked specimens with different random R-curves, which serve as inputs for our artificial neural network. Regarding the outputs, principal component analysis is performed to reduce dimensionality and find suitable descriptors for crack resistance curves. After successfully training machine learning model, experimental studies on basalt fiber reinforced laminates are conducted as validation. Results have proven the effectiveness of the proposed strategy for predicting crack resistance curves, as well as the feasibility of using machine learning-based framework to find out more information about composites from simple experimental data.
本文提出了一种利用机器学习模型确定复合材料层压板跨层抗裂曲线的新方法。该方法的主要目的是从中心裂纹层压板的强度值中提取抗裂性的隐藏信息。与传统测量相比,显著的优点是只需要拉伸强度值,这可以通过相当简单的实验程序获得。这是通过结合有限断裂力学来实现的,该力学将抗裂性与强度值联系起来。为了获得训练数据集,采用有限元法和有限断裂力学的半解析方法生成具有不同随机R曲线的中心裂纹试件的强度值,作为我们的人工神经网络的输入。关于输出,进行主成分分析以降维并为抗裂曲线找到合适的描述符。在成功训练了机器学习模型后,对玄武岩纤维增强层压板进行了实验研究。结果证明了所提出的预测抗裂曲线的策略的有效性,以及使用基于机器学习的框架从简单的实验数据中找出更多关于复合材料的信息的可行性。
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引用次数: 5
Martensite decomposition during post-heat treatments and the aging response of near-α Ti–6Al–2Sn–4Zr–2Mo (Ti-6242) titanium alloy processed by selective laser melting (SLM) 选择性激光熔化(SLM)近α Ti-6Al-2Sn-4Zr-2Mo (Ti-6242)钛合金热处理后马氏体分解及时效响应
Q3 Engineering Pub Date : 2021-06-24 DOI: 10.1142/s2424913020500186
Haiyang Fan, Yahui Liu, Shoufeng Yang
Ti–6Al–2Sn–4Zr–2Mo (Ti-6242), a near-[Formula: see text] titanium alloy explicitly designed for high-temperature applications, consists of a martensitic structure after selective laser melting (SLM). However, martensite is thermally unstable and thus adverse to the long-term service at high temperatures. Hence, understanding martensite decomposition is a high priority for seeking post-heat treatment for SLMed Ti-6242. Besides, compared to the room-temperature titanium alloys like Ti–6Al–4V, aging treatment is indispensable to high-temperature near-[Formula: see text] titanium alloys so that their microstructures and mechanical properties are pre-stabilized before working at elevated temperatures. Therefore, the aging response of the material is another concern of this study. To elaborate the two concerns, SLMed Ti-6242 was first isothermally annealed at 650[Formula: see text]C and then water-quenched to room temperature, followed by standard aging at 595[Formula: see text]C. The microstructure analysis revealed a temperature-dependent martensite decomposition, which proceeded sluggishly at [Formula: see text]C despite a long duration but rapidly transformed into lamellar [Formula: see text] above the martensite transition zone (770[Formula: see text]C). As heating to [Formula: see text]C), it produced a coarse microstructure containing new martensites formed in water quenching. The subsequent mechanical testing indicated that SLM-built Ti-6242 is excellent in terms of both room- and high-temperature tensile properties, with around 1400 MPa (UTS)[Formula: see text]5% elongation and 1150 MPa (UTS)[Formula: see text]10% elongation, respectively. However, the combination of water quenching and aging embrittled the as-built material severely.
Ti–6Al–2Sn–4Zr–2Mo(Ti-6242)是一种明确设计用于高温应用的近[公式:见正文]钛合金,在选择性激光熔化(SLM)后由马氏体结构组成。然而,马氏体是热不稳定的,因此不利于在高温下长期使用。因此,了解马氏体分解是寻求SLMed Ti-6242后热处理的高度优先事项。此外,与Ti–6Al–4V等室温钛合金相比,时效处理对于高温近[公式:见正文]钛合金来说是必不可少的,这样它们的微观结构和机械性能在高温下工作之前就得到了预稳定。因此,材料的老化反应是本研究的另一个关注点。为了详细说明这两个问题,SLMed Ti-6242首先在650[公式:见正文]C下等温退火,然后水淬至室温,然后在595[公式:参见正文]C进行标准老化。微观结构分析显示了依赖于温度的马氏体分解,尽管持续时间很长,但在[公式:见正文]C下缓慢进行,但在马氏体过渡区(770[公式:参见正文]C)上方迅速转变为层状[公式:看正文]。当加热到[公式:见正文]C)时,它产生了一种粗糙的微观结构,其中包含在水淬火中形成的新马氏体。随后的机械测试表明,SLM构建的Ti-6242在室温和高温拉伸性能方面都非常出色,分别具有约1400MPa(UTS)[公式:见正文]5%的伸长率和1150MPa(UTS,公式:见文本]10%的伸长率。然而,水淬和时效的结合使竣工材料严重脆化。
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引用次数: 16
Modeling of heterogeneous materials at high strain rates with machine learning algorithms trained by finite element simulations 利用有限元模拟训练的机器学习算法对高应变率下的非均质材料进行建模
Q3 Engineering Pub Date : 2021-06-17 DOI: 10.1142/s2424913021500016
X. Long, Minghui Mao, Chang Lu, R. Li, Fengrui Jia
Great progress has been made in the dynamic mechanical properties of concrete which is usually assumed to be homogenous. In fact, concrete is a typical heterogeneous material, and the meso-scale structure with aggregates has a significant effect on its macroscopic mechanical properties of concrete. In this paper, concrete is regarded as a two-phase composite material, that is, a combination of aggregate inclusion and mortar matrix. To create the finite element (FE) models, the Monte Carlo method is used to place the aggregates as random inclusions into the mortar matrix of the cylindrical specimens. To validate the numerical simulations of such an inclusion-matrix model at high strain rates, the comparisons with experimental results using the split Hopkinson pressure bar are made and good agreement is achieved in terms of dynamic increasing factor. By performing more extensive FE predictions, the influences of aggregate size and content on the macroscopic dynamic properties (i.e., peak dynamic strength) of concrete materials subjected to high strain rates are further investigated based on the back-propagation (BP) artificial neural network method. It is found that the particle size of aggregate has little effect on the dynamic mechanical properties of concrete but the peak dynamic strength of concrete increases obviously with the content increase of aggregate. After detailed comparisons with FE simulations, machine learning predictions based on the BP algorithm show good applicability for predicting dynamic mechanical strength of concrete with different aggregate sizes and contents. Instead of FE analysis with complicated meso-scale aggregate pre-processing, time-consuming simulation and laborious post-processing, machine learning predictions reproduce the stress–strain curves of concrete materials under high strain rates and thus the constitutive behavior can be efficiently predicted.
在通常被认为是均质的混凝土的动态力学性能方面已经取得了很大的进展。事实上,混凝土是一种典型的非均质材料,骨料的细观结构对其宏观力学性能有着重要影响。本文将混凝土视为一种两相复合材料,即骨料夹杂和砂浆基体的组合。为了创建有限元(FE)模型,使用蒙特卡罗方法将骨料作为随机夹杂物放入圆柱形试样的砂浆基体中。为了验证这种包含矩阵模型在高应变速率下的数值模拟,将其与使用分裂霍普金森压杆的实验结果进行了比较,并在动态增长因子方面取得了良好的一致性。通过进行更广泛的有限元预测,基于反向传播(BP)人工神经网络方法,进一步研究了骨料尺寸和含量对高应变速率下混凝土材料宏观动态特性(即峰值动态强度)的影响。研究发现,骨料粒径对混凝土的动态力学性能影响不大,但随着骨料含量的增加,混凝土的峰值动态强度明显增加。经过与有限元模拟的详细比较,基于BP算法的机器学习预测在预测不同骨料尺寸和含量的混凝土动态力学强度方面显示出良好的适用性。机器学习预测再现了混凝土材料在高应变速率下的应力-应变曲线,从而可以有效地预测本构行为,而不是复杂的中尺度骨料预处理、耗时的模拟和费力的后处理的有限元分析。
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引用次数: 7
Preface: Special Issue: Recent Advances in 3D/4D Printing 前言:特刊:3D/4D打印的最新进展
Q3 Engineering Pub Date : 2021-06-01 DOI: 10.1142/s242491302102001x
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引用次数: 0
Progress in fabrication and characterization of mullite whiskers 莫来石晶须的制备与表征研究进展
Q3 Engineering Pub Date : 2021-03-01 DOI: 10.1142/s242491302150003x
Zhuohao Xiao, Wenqiang Wang, Xiuying Li, Ling Zhang, Tianshu Zhang, Ming Gao, L. Kong, Kun Zhou, Yin Liu
Mullite has an orthorhombic crystal structure, with various advantages, such as high mechanical strength, and stable chemical and physical properties. Especially, mullite whiskers have been widely acknowledged to be potential candidates as reinforcing elements in the fabrication of ceramic-matrix composites. Various strategies have been developed to synthesize mullite whiskers, such as catalytic methods, liquid-phase reaction, molten salt reaction, solid-state reaction and high-energy ball milling process. In different synthesis methods, the underlying mechanisms governing the anisotropic grain growth of mullite grains vary. This paper aims to offer an overview on the progress in fabrication of mullite whiskers with different methods, and the perspectives on these special materials are briefly discussed.
莫来石具有正交晶体结构,具有机械强度高、化学物理性能稳定等优点。特别是莫来石晶须已被广泛认为是陶瓷基复合材料中增强元素的潜在候选人。合成莫来石晶须的方法有催化法、液相法、熔盐法、固相法和高能球磨法等。在不同的合成方法中,控制莫来石晶粒各向异性生长的潜在机制各不相同。本文综述了不同方法制备莫来石晶须的研究进展,并对这些特殊材料的发展前景作了简要的讨论。
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引用次数: 0
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Journal of Micromechanics and Molecular Physics
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