首页 > 最新文献

Volume 3B: Design and Analysis最新文献

英文 中文
Development of New Design Fatigue Curves in Japan: Discussion of Best Fit Curves Based on Fatigue Test Data With Large Scale Piping 日本新设计疲劳曲线的发展:基于大型管道疲劳试验数据的最佳拟合曲线探讨
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-84436
M. Bodai, Y. Fukuta, S. Asada, K. Hayashi
In order to develop new design fatigue curves for austenitic carbon steels & low alloy steels and stainless steels and a new design fatigue evaluation method that are rational and have clear design basis, Design Fatigue Curve (DFC) Phase 1 subcommittee and Phase 2 subcommittee were established in the Atomic Energy Research Committee in the Japan Welding Engineering Society. The study on design fatigue curves was actively performed in the subcommittees. In the subcommittees, domestic and foreign fatigue data of small test specimens in air were collected and a comprehensive fatigue database was constructed. Using this fatigue database, the accurate best-fit curves of austenitic carbon steels & low alloy steels and stainless steels were developed by applying tensile strength to a parameter of the curve. Regarding design factors on design fatigue curves, data scatter, mean stress correction, surface finishing effect, size effect and variable loading effect were investigated and each design factor was decided to be individually considered on the design fatigue curves. A Japanese utility project performed large scale fatigue tests using austenitic stainless steel piping and carbon and low-alloy steel flat plates as well as fatigue tests using small specimens to obtain not only basic data but also fatigue data of mean stress effect and surface finishing effect. Those test results were provided to the subcommittee and utilized the above studies. In this paper, the large scale fatigue tests using austenitic stainless steel piping and the best-fit curve of austenitic stainless steel are discussed.
为了开发新的奥氏体碳钢、低合金钢和不锈钢的设计疲劳曲线和一种合理的、有明确设计依据的设计疲劳评价新方法,日本焊接工程学会原子能研究委员会成立了设计疲劳曲线(DFC)第一阶段和第二阶段小组委员会。小组委员会积极开展设计疲劳曲线研究。在小组中,收集了国内外空气中小试件的疲劳数据,建立了一个全面的疲劳数据库。利用该疲劳数据库,将抗拉强度作为曲线参数,得到了奥氏体碳钢、低合金钢和不锈钢的精确最佳拟合曲线。针对设计疲劳曲线上的设计因素,研究了数据散点、平均应力修正、表面整理效应、尺寸效应和变载荷效应,并确定了每个设计因素在设计疲劳曲线上单独考虑。日本某公用事业项目采用奥氏体不锈钢管、碳钢和低合金钢平板进行了大型疲劳试验,并采用小试件进行了疲劳试验,不仅获得了基本数据,而且获得了平均应力效应和表面整理效果的疲劳数据。这些测试结果已提供给小组委员会,并利用了上述研究。本文讨论了奥氏体不锈钢管道的大型疲劳试验及奥氏体不锈钢的最佳拟合曲线。
{"title":"Development of New Design Fatigue Curves in Japan: Discussion of Best Fit Curves Based on Fatigue Test Data With Large Scale Piping","authors":"M. Bodai, Y. Fukuta, S. Asada, K. Hayashi","doi":"10.1115/PVP2018-84436","DOIUrl":"https://doi.org/10.1115/PVP2018-84436","url":null,"abstract":"In order to develop new design fatigue curves for austenitic carbon steels & low alloy steels and stainless steels and a new design fatigue evaluation method that are rational and have clear design basis, Design Fatigue Curve (DFC) Phase 1 subcommittee and Phase 2 subcommittee were established in the Atomic Energy Research Committee in the Japan Welding Engineering Society. The study on design fatigue curves was actively performed in the subcommittees.\u0000 In the subcommittees, domestic and foreign fatigue data of small test specimens in air were collected and a comprehensive fatigue database was constructed. Using this fatigue database, the accurate best-fit curves of austenitic carbon steels & low alloy steels and stainless steels were developed by applying tensile strength to a parameter of the curve.\u0000 Regarding design factors on design fatigue curves, data scatter, mean stress correction, surface finishing effect, size effect and variable loading effect were investigated and each design factor was decided to be individually considered on the design fatigue curves.\u0000 A Japanese utility project performed large scale fatigue tests using austenitic stainless steel piping and carbon and low-alloy steel flat plates as well as fatigue tests using small specimens to obtain not only basic data but also fatigue data of mean stress effect and surface finishing effect. Those test results were provided to the subcommittee and utilized the above studies.\u0000 In this paper, the large scale fatigue tests using austenitic stainless steel piping and the best-fit curve of austenitic stainless steel are discussed.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"10 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126327613","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Simplified Analysis of Strains Accumulated in the State of Elastic Shakedown Considering Multi-Parameter Loadings 考虑多参数载荷的弹性安定状态累积应变的简化分析
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-84070
H. Hübel, B. Vollrath
In case of cyclic loading, strain may accumulate due to a ratcheting mechanism until the state of shakedown is possibly achieved. Design Codes frequently require strain limits to be satisfied at the end of the specified lifetime of the structure. However, this requirement is sometimes tied to misleading prerequisites, and little guidance is provided on how the strains accumulated in the state of shakedown can be calculated. Incremental elastic-plastic analyses which require to go step-by-step through many cycles of a given load histogram are rather costly in terms of engineering time and numerical effort. As an alternative, the Simplified Theory of Plastic Zones (STPZ) is used in the present paper. Being a direct method, effects from load history are disregarded. The theory is described shortly and exemplarily applied to a simplification of a pipe bend and a straight pipe, both subjected to combinations of several loads which vary independently from each other so that a multidimensional load domain is represented. It is shown that the Simplified Theory of Plastic Zones is well suited to provide reasonable estimates of strains accumulated in the state of elastic shakedown at the cost of few linear elastic analyses.
在循环加载的情况下,由于棘轮机制,应变可能会累积,直到可能达到安定状态。设计规范经常要求在结构的规定寿命结束时满足应变极限。然而,这一要求有时与误导性的先决条件联系在一起,并且很少提供关于如何计算安定状态下累积的应变的指导。增量弹塑性分析需要在给定载荷直方图的多个循环中逐步进行,这在工程时间和数值计算方面是相当昂贵的。本文采用简化塑性区理论(STPZ)作为替代方法。作为一种直接方法,忽略了负荷历史的影响。该理论被简短地描述,并举例应用于管道弯管和直管的简化,两者都受到相互独立变化的几种载荷的组合,以便表示多维载荷域。结果表明,简化塑性区理论可以较好地提供在弹性安定状态下的应变累积的合理估计,而只需进行很少的线性弹性分析。
{"title":"Simplified Analysis of Strains Accumulated in the State of Elastic Shakedown Considering Multi-Parameter Loadings","authors":"H. Hübel, B. Vollrath","doi":"10.1115/PVP2018-84070","DOIUrl":"https://doi.org/10.1115/PVP2018-84070","url":null,"abstract":"In case of cyclic loading, strain may accumulate due to a ratcheting mechanism until the state of shakedown is possibly achieved. Design Codes frequently require strain limits to be satisfied at the end of the specified lifetime of the structure. However, this requirement is sometimes tied to misleading prerequisites, and little guidance is provided on how the strains accumulated in the state of shakedown can be calculated. Incremental elastic-plastic analyses which require to go step-by-step through many cycles of a given load histogram are rather costly in terms of engineering time and numerical effort. As an alternative, the Simplified Theory of Plastic Zones (STPZ) is used in the present paper. Being a direct method, effects from load history are disregarded. The theory is described shortly and exemplarily applied to a simplification of a pipe bend and a straight pipe, both subjected to combinations of several loads which vary independently from each other so that a multidimensional load domain is represented. It is shown that the Simplified Theory of Plastic Zones is well suited to provide reasonable estimates of strains accumulated in the state of elastic shakedown at the cost of few linear elastic analyses.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"42 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130908119","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Numerical Study on the Startup Performance for the High Pressure Inner Casing of the Solar Steam Turbine 太阳能汽轮机高压内壳启动性能的数值研究
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-84418
Peng Wang, Gang Chen, Wenfu Li
Operation flexibility and the high efficiency of thermal cycle are the two hot research topics for the steam turbine unit. For the operation flexibility, it requires the turbine unit be able to start up quickly and frequently, and good thermal fatigue properties of the components are a must. On the other hand, the trend to higher temperature with ultra supercritical (USC) steam is the key drive of ongoing development for the validation of a method to improve the thermal cycle efficiency, but the application of the higher steam temperature will intensify the component’s thermal fatigue. In this paper, a high pressure inner casing for the new designed solar steam turbine was studied, and the Finite Element Method (FEM) combined with linear elastic material was applied to simulate the transient stress and temperature fields during the daily warm/hot startup process. On the basis of the stress spectrum in the critical zone, the standard DIN EN-12952-3 and the fatigue curve were used to evaluate the low cycle fatigue life consumption in the transient process.
运行灵活性和热循环的高效性是汽轮机组研究的两个热点。对于运行灵活性,要求汽轮机组能够快速频繁地启动,并且部件必须具有良好的热疲劳性能。另一方面,超超临界(USC)蒸汽向更高温度的发展趋势是提高热循环效率方法验证的关键驱动力,但更高蒸汽温度的应用将加剧部件的热疲劳。以新设计的太阳能汽轮机高压内壳为研究对象,采用有限单元法结合线弹性材料对其日常热/热启动过程中的瞬态应力场和温度场进行了数值模拟。在临界区应力谱的基础上,采用DIN EN-12952-3标准和疲劳曲线对瞬态过程的低周疲劳寿命消耗进行了评价。
{"title":"Numerical Study on the Startup Performance for the High Pressure Inner Casing of the Solar Steam Turbine","authors":"Peng Wang, Gang Chen, Wenfu Li","doi":"10.1115/PVP2018-84418","DOIUrl":"https://doi.org/10.1115/PVP2018-84418","url":null,"abstract":"Operation flexibility and the high efficiency of thermal cycle are the two hot research topics for the steam turbine unit. For the operation flexibility, it requires the turbine unit be able to start up quickly and frequently, and good thermal fatigue properties of the components are a must. On the other hand, the trend to higher temperature with ultra supercritical (USC) steam is the key drive of ongoing development for the validation of a method to improve the thermal cycle efficiency, but the application of the higher steam temperature will intensify the component’s thermal fatigue.\u0000 In this paper, a high pressure inner casing for the new designed solar steam turbine was studied, and the Finite Element Method (FEM) combined with linear elastic material was applied to simulate the transient stress and temperature fields during the daily warm/hot startup process. On the basis of the stress spectrum in the critical zone, the standard DIN EN-12952-3 and the fatigue curve were used to evaluate the low cycle fatigue life consumption in the transient process.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"249 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"124744604","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Evaluation of Strength of Pipe With Metal-Loss due to CUI by FFS and FEA Which Considered the Fracture Ductility 考虑断裂延性的金属损管的FFS和有限元强度评价
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-84741
A. Yamaguchi, N. Yoshida
Corrosion under insulation (CUI) is an aging degradation issue in long-term service vessels and pipes made of carbon steel and low-alloy steel. One of the problems in managing CUI is an equivocal evaluation technique of thinning detected by inspection. A replacement period with more accuracy can be evaluated more appropriately by performing fitness-for-service (FFS) assessment in this equipment. It is important to verify the validity of the FFS assessment using actually corroded pipes in order to promote the spread of FFS assessment in the domestic industry. In the present paper, pipes with complicated metal-loss due to CUI that were used in a chemical plant are burst in burst tests. An estimated burst pressure, which is calculated based on the assessment of metal-loss and through finite element analysis (FEA) based on FFS assessment, is compared with experimentally obtained burst pressures in order to validate the integrity evaluation. The burst pressure is then estimated by FEA, in which the ductile fracture under the multiaxial stress condition is considered. The burst pressure estimated by FFS approximately matched the burst pressure obtained based on experimental results. Fitness-for-service is sufficiently valid for investigating the remaining strength or burst pressure of corroded pipe. In addition, the burst pressure estimated by FEA that considered the ductile fracture under the multiaxial stress condition agreed with the experimental results and is valid so long as the remaining strength factor (RSF) is less than 0.6.
绝缘下腐蚀(CUI)是碳钢和低合金钢制成的长期服役容器和管道的老化退化问题。在CUI管理中存在的问题之一是检测检测到的稀化评价技术的模糊性。通过对该设备进行使用适应度(FFS)评估,可以更准确地评估更换周期。为了促进FFS评估在国内行业的推广,利用实际腐蚀管道验证FFS评估的有效性是非常重要的。本文对某化工装置中具有复杂金属损耗的管道进行了爆破试验。基于金属损失评估和基于FFS评估的有限元分析(FEA)计算了估计的破裂压力,并将其与实验得到的破裂压力进行了比较,以验证完整性评估。在考虑多轴应力条件下的韧性断裂的情况下,采用有限元法估算破裂压力。FFS估算的爆破压力与实验结果的爆破压力基本吻合。适用于调查腐蚀管道的剩余强度或破裂压力是充分有效的。此外,考虑多轴应力条件下韧性断裂的FEA爆破压力估算值与实验结果吻合,在残余强度因子(RSF)小于0.6时有效。
{"title":"Evaluation of Strength of Pipe With Metal-Loss due to CUI by FFS and FEA Which Considered the Fracture Ductility","authors":"A. Yamaguchi, N. Yoshida","doi":"10.1115/PVP2018-84741","DOIUrl":"https://doi.org/10.1115/PVP2018-84741","url":null,"abstract":"Corrosion under insulation (CUI) is an aging degradation issue in long-term service vessels and pipes made of carbon steel and low-alloy steel. One of the problems in managing CUI is an equivocal evaluation technique of thinning detected by inspection. A replacement period with more accuracy can be evaluated more appropriately by performing fitness-for-service (FFS) assessment in this equipment. It is important to verify the validity of the FFS assessment using actually corroded pipes in order to promote the spread of FFS assessment in the domestic industry. In the present paper, pipes with complicated metal-loss due to CUI that were used in a chemical plant are burst in burst tests. An estimated burst pressure, which is calculated based on the assessment of metal-loss and through finite element analysis (FEA) based on FFS assessment, is compared with experimentally obtained burst pressures in order to validate the integrity evaluation. The burst pressure is then estimated by FEA, in which the ductile fracture under the multiaxial stress condition is considered. The burst pressure estimated by FFS approximately matched the burst pressure obtained based on experimental results. Fitness-for-service is sufficiently valid for investigating the remaining strength or burst pressure of corroded pipe. In addition, the burst pressure estimated by FEA that considered the ductile fracture under the multiaxial stress condition agreed with the experimental results and is valid so long as the remaining strength factor (RSF) is less than 0.6.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"33 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125330183","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Shakedown-Ratcheting Analysis of a Spherical Pressure Vessel by Anisotropic Continuum Damage Mechanics 基于各向异性连续损伤力学的球形压力容器安定-棘轮分析
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-84065
A. Nayebi, Azam Surmiri, H. Rokhgireh
In cyclic loading and when plastic flow occurs, discontinuities grow. In this research, interaction diagram of Bree has been developed when the spherical pressure vessel contains discontinuities such as voids and microcracks. Bree’s diagram is used for ratcheting assessment of pressurized equipment in ASME III NH. Nature of these defects leads to an anisotropic damage. Anisotropic Continuum Damage Mechanics (CDM) is considered to account effects of these discontinuities on the behavior of the structure. Shakedown – ratcheting response of a hollow sphere under constant internal pressure and cyclic thermal loadings are studied by using anisotropic CDM theory coupled with nonlinear kinematic hardening of Armstrong-Frederick m’s model (A-F). Return mapping method is used to solve numerically the developed relations. Elastic, elastic shakedown, plastic shakedown and ratcheting regions are illustrated in the modified Bree’s diagram. Influence of anisotropic damage due to the plastic deformation is studied and it was shown that the plastic shakedown region is diminished because of the developed damage.
在循环加载和塑性流动发生时,不连续面增大。本研究绘制了球形压力容器中存在空隙、微裂纹等不连续时的Bree相互作用图。布里图用于ASME III NH中加压设备的棘轮评估。这些缺陷的性质导致了各向异性损伤。各向异性连续损伤力学(CDM)被认为是考虑这些不连续性对结构行为的影响。采用各向异性CDM理论,结合Armstrong-Frederick m模型(a - f)的非线性运动硬化,研究了空心球体在恒内压和循环热载荷作用下的安定棘轮响应。采用返回映射法对已开发的关系进行数值求解。弹性,弹性安定,塑料安定和棘轮区域在修改后的布里图中说明。研究了各向异性损伤对塑性变形的影响,结果表明,损伤的发展使塑性安定区减小。
{"title":"Shakedown-Ratcheting Analysis of a Spherical Pressure Vessel by Anisotropic Continuum Damage Mechanics","authors":"A. Nayebi, Azam Surmiri, H. Rokhgireh","doi":"10.1115/PVP2018-84065","DOIUrl":"https://doi.org/10.1115/PVP2018-84065","url":null,"abstract":"In cyclic loading and when plastic flow occurs, discontinuities grow. In this research, interaction diagram of Bree has been developed when the spherical pressure vessel contains discontinuities such as voids and microcracks. Bree’s diagram is used for ratcheting assessment of pressurized equipment in ASME III NH. Nature of these defects leads to an anisotropic damage. Anisotropic Continuum Damage Mechanics (CDM) is considered to account effects of these discontinuities on the behavior of the structure. Shakedown – ratcheting response of a hollow sphere under constant internal pressure and cyclic thermal loadings are studied by using anisotropic CDM theory coupled with nonlinear kinematic hardening of Armstrong-Frederick m’s model (A-F). Return mapping method is used to solve numerically the developed relations. Elastic, elastic shakedown, plastic shakedown and ratcheting regions are illustrated in the modified Bree’s diagram. Influence of anisotropic damage due to the plastic deformation is studied and it was shown that the plastic shakedown region is diminished because of the developed damage.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"92 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126201388","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Application of the T-Scaling Method to Predict Fracture Toughness Under Compressive Residual Stress in the Transition Temperature Region t标度法在过渡温度区残余压应力下断裂韧性预测中的应用
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-84151
T. Meshii, K. Ishihara
The fracture toughness Jc of a material in the ductile-to-brittle transition temperature region shows a test specimen thickness (TST) effect and temperature dependence, and apparently increases when a compressive residual stress is applied. Many models to explain these phenomena have been proposed that can also consider the large scatter of Jc. On the contrary, the authors have focused on the mean Jc and have demonstrated that the TST effect on Jc and temperature dependence of Jc are due to “the loss of the one-to-one correspondence between J and the crack-tip stress distribution” and that the “scaled” crack-tip stress distribution at fracture is independent of the TST effect on Jc or temperature. The T-scaling method was proposed and validated for this purpose. In this study, the fracture prediction of a specimen with compressive residual stress was performed using the T-scaling method, and its validity was confirmed for high-strength steel of 780-MPa class and 0.45 % carbon steel JIS S45C.
在韧脆转变温度区,材料的断裂韧性Jc表现出试样厚度效应和温度依赖性,施加压残余应力时断裂韧性Jc明显增加。已经提出了许多模型来解释这些现象,这些模型也可以考虑Jc的大分散。相反,作者关注的是平均Jc,并证明了高温对Jc的影响和Jc的温度依赖性是由于“J与裂纹尖端应力分布之间的一对一对应关系的丧失”,并且断裂处的“尺度”裂纹尖端应力分布与高温对Jc或温度的影响无关。为此提出并验证了t标度法。本文采用t标度法对含有残余压应力的试样进行了断裂预测,并对780-MPa级高强钢和0.45%碳素钢JIS S45C进行了验证。
{"title":"Application of the T-Scaling Method to Predict Fracture Toughness Under Compressive Residual Stress in the Transition Temperature Region","authors":"T. Meshii, K. Ishihara","doi":"10.1115/PVP2018-84151","DOIUrl":"https://doi.org/10.1115/PVP2018-84151","url":null,"abstract":"The fracture toughness Jc of a material in the ductile-to-brittle transition temperature region shows a test specimen thickness (TST) effect and temperature dependence, and apparently increases when a compressive residual stress is applied. Many models to explain these phenomena have been proposed that can also consider the large scatter of Jc. On the contrary, the authors have focused on the mean Jc and have demonstrated that the TST effect on Jc and temperature dependence of Jc are due to “the loss of the one-to-one correspondence between J and the crack-tip stress distribution” and that the “scaled” crack-tip stress distribution at fracture is independent of the TST effect on Jc or temperature. The T-scaling method was proposed and validated for this purpose. In this study, the fracture prediction of a specimen with compressive residual stress was performed using the T-scaling method, and its validity was confirmed for high-strength steel of 780-MPa class and 0.45 % carbon steel JIS S45C.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"75 1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"126986074","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Analysis of the Influence of the Cooling Patterns and the Shape of the Bulges on the Levels of Stress in the Cylindrical Section of Delayed Coke Drums 冷却方式和鼓体形状对延迟焦炭鼓筒段应力水平的影响分析
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-85009
G. Vivas, Armando J. Moret, R. Bello, Luis M. Melian, J. Bedoya
Coke drums are thin-walled pressure vessels that experience low cycle fatigue due to thermal loadings. The delayed coking process is comprised by three major stages: heating, coking and cooling, which repeat at intervals between 20 and 48 hours. The cyclic changes of temperature increase the growth of bulges and cracks which with the passing of time, propagate and eventually cause failures due to the loss of containment. A better understanding of the phenomena of the thermal gradients and their influence on the generated stresses would reduce the effects of the damage mechanisms afflicting coke drums, for example; a continuous monitoring system could be implemented in order to control the cooling ramp to obtain a more homogeneous quenching around the cylinder of the coke drum and consequently increase its lifetime. It is been widely accepted that there is a relationship between high cooling rates in isolated zones and high axial stresses. However, this relationship has not been fully validated, since there are also been reported events of low cooling rates and high stresses. This study shows a predictable behavior (trend) that relates the spatial thermal gradients and the axial and circumferential stresses generated. A coke drum in an upgrader facility was instrumented with two arrays or grids, each of them having 24 thermocouples and 2 strain gauges in zones with distinct bulges. One arrangement was located at an inward bulge while the other was located at an outward bulge. Computational models were carried out to reproduce the behavior of the instrumented zones with their actual deformations obtained from laser scanning. Finite element models were developed using a sequentially coupled thermo-mechanical analysis to determine the transient temperature and stress distributions. The effect of the circumferential thermal gradients on the stress levels in the instrumented cylindrical sections were analyzed, considering two cases; the first of them a perfect cylinder (without deformation) and the second one considering the presence of bulges in the area of interest. The results indicate that there is a relationship between the circumferential thermal gradients [°C/m] or [°F/ft] and the axial stress levels, i.e., cold zones generate axial tensile stresses, and hot zones produce compressive axial stresses. This relationship is affected — exacerbated or counteracted — by the presence of the bulges. Additionally, the results obtained in this paper confirm those of previous investigations showing that outward bulges subject to pressure and thermal loading generate high stresses on its internal surface and low stresses on its external face whereas inward bulges produce the opposite effect.
焦炭桶是薄壁压力容器,由于热负荷而经历低周疲劳。延迟焦化过程由三个主要阶段组成:加热、焦化和冷却,每隔20至48小时重复一次。温度的循环变化增加了凸起和裂缝的生长,随着时间的推移,凸起和裂缝扩展并最终由于失去遏制而导致破坏。例如,更好地了解热梯度现象及其对产生的应力的影响将减少焦炭桶的损坏机制的影响;可以实施连续监测系统,以控制冷却斜坡,以获得更均匀的焦炭滚筒周围的淬火,从而增加其寿命。人们普遍认为,孤立区的高冷却速率与高轴向应力之间存在关系。然而,这种关系尚未得到充分验证,因为也有报道了低冷却速率和高应力的事件。该研究显示了空间热梯度与轴向和周向应力之间的可预测行为(趋势)。在升级装置中的焦炭桶上安装了两个阵列或网格,每个阵列或网格在不同凸起的区域有24个热电偶和2个应变片。一种布置位于向内凸起处,而另一种布置位于向外凸起处。利用激光扫描得到的实际变形,建立了计算模型来再现被测区域的行为。采用顺序耦合热-力分析方法建立了有限元模型,确定了瞬态温度和应力分布。考虑两种情况,分析了周向热梯度对仪器圆柱形截面应力水平的影响;第一个是一个完美的圆柱体(没有变形),第二个是考虑到在感兴趣的区域存在凸起。结果表明,周向热梯度[°C/m]或[°F/ft]与轴向应力水平之间存在一定的关系,即冷区产生轴向拉应力,热区产生轴向压应力。这种关系受到肿块存在的影响——加剧或抵消。此外,本文得到的结果证实了以往的研究结果,即在压力和热载荷作用下,向外凸起在其内表面产生高应力,在其外表面产生低应力,而向内凸起则产生相反的效果。
{"title":"Analysis of the Influence of the Cooling Patterns and the Shape of the Bulges on the Levels of Stress in the Cylindrical Section of Delayed Coke Drums","authors":"G. Vivas, Armando J. Moret, R. Bello, Luis M. Melian, J. Bedoya","doi":"10.1115/PVP2018-85009","DOIUrl":"https://doi.org/10.1115/PVP2018-85009","url":null,"abstract":"Coke drums are thin-walled pressure vessels that experience low cycle fatigue due to thermal loadings. The delayed coking process is comprised by three major stages: heating, coking and cooling, which repeat at intervals between 20 and 48 hours. The cyclic changes of temperature increase the growth of bulges and cracks which with the passing of time, propagate and eventually cause failures due to the loss of containment. A better understanding of the phenomena of the thermal gradients and their influence on the generated stresses would reduce the effects of the damage mechanisms afflicting coke drums, for example; a continuous monitoring system could be implemented in order to control the cooling ramp to obtain a more homogeneous quenching around the cylinder of the coke drum and consequently increase its lifetime. It is been widely accepted that there is a relationship between high cooling rates in isolated zones and high axial stresses. However, this relationship has not been fully validated, since there are also been reported events of low cooling rates and high stresses. This study shows a predictable behavior (trend) that relates the spatial thermal gradients and the axial and circumferential stresses generated.\u0000 A coke drum in an upgrader facility was instrumented with two arrays or grids, each of them having 24 thermocouples and 2 strain gauges in zones with distinct bulges. One arrangement was located at an inward bulge while the other was located at an outward bulge. Computational models were carried out to reproduce the behavior of the instrumented zones with their actual deformations obtained from laser scanning. Finite element models were developed using a sequentially coupled thermo-mechanical analysis to determine the transient temperature and stress distributions. The effect of the circumferential thermal gradients on the stress levels in the instrumented cylindrical sections were analyzed, considering two cases; the first of them a perfect cylinder (without deformation) and the second one considering the presence of bulges in the area of interest.\u0000 The results indicate that there is a relationship between the circumferential thermal gradients [°C/m] or [°F/ft] and the axial stress levels, i.e., cold zones generate axial tensile stresses, and hot zones produce compressive axial stresses. This relationship is affected — exacerbated or counteracted — by the presence of the bulges. Additionally, the results obtained in this paper confirm those of previous investigations showing that outward bulges subject to pressure and thermal loading generate high stresses on its internal surface and low stresses on its external face whereas inward bulges produce the opposite effect.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"4 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134087886","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Improvement of J Estimation Schemes Based on Reference Stress for Linear Hardening Behavior 基于参考应力的线性硬化J估计方法的改进
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-84410
P. Gilles
In Elastic-Plastic Fracture Mechanics, several J-estimation schemes are based on the reference stress approach. This approach has been developed initially for creep analyses and later on for elasto-plastic fracture assessments in 1984, then included in the R6 rule. Much later, other methods, based on the reference stress concept, were derived for 3D applications like the Js method introduced in the French RSE-M code in 1997 and the Enhanced Reference Stress (ERS) method in Korea around 2001. However, these developments are based on the J2 deformation plasticity theory and well established for a pure power hardening law. Js and ERS schemes propose some corrections for recorded behavior laws which cannot be fitted by a power law. Nevertheless, their application to materials governed by a bilinear hardening law has been called into question by several studies. One of these, carried out by M. T. Kirk and R. H. Dodds [1, 2] is of great interest since addressing the practical case of a surface cracked plate.
在弹塑性断裂力学中,有几种基于参考应力法的j估计方法。该方法最初用于蠕变分析,后来在1984年用于弹塑性断裂评估,然后纳入R6规则。很久以后,基于参考应力概念的其他方法被衍生出来用于3D应用,如1997年法国RSE-M代码中引入的Js方法和2001年左右韩国的增强参考应力(ERS)方法。然而,这些发展都是基于J2变形塑性理论,并建立了纯粹的功率硬化规律。Js和ERS方案对幂律不能拟合的记录行为规律提出了一些修正。然而,它们在双线性硬化规律支配下的材料上的应用受到了一些研究的质疑。其中一项是由M. T. Kirk和R. H. Dodds[1,2]进行的,由于解决了表面裂纹板的实际情况,因此引起了极大的兴趣。
{"title":"Improvement of J Estimation Schemes Based on Reference Stress for Linear Hardening Behavior","authors":"P. Gilles","doi":"10.1115/PVP2018-84410","DOIUrl":"https://doi.org/10.1115/PVP2018-84410","url":null,"abstract":"In Elastic-Plastic Fracture Mechanics, several J-estimation schemes are based on the reference stress approach. This approach has been developed initially for creep analyses and later on for elasto-plastic fracture assessments in 1984, then included in the R6 rule. Much later, other methods, based on the reference stress concept, were derived for 3D applications like the Js method introduced in the French RSE-M code in 1997 and the Enhanced Reference Stress (ERS) method in Korea around 2001. However, these developments are based on the J2 deformation plasticity theory and well established for a pure power hardening law. Js and ERS schemes propose some corrections for recorded behavior laws which cannot be fitted by a power law. Nevertheless, their application to materials governed by a bilinear hardening law has been called into question by several studies. One of these, carried out by M. T. Kirk and R. H. Dodds [1, 2] is of great interest since addressing the practical case of a surface cracked plate.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"21 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"134300003","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Sulfidation Rate Prediction on Tube-to-Tubesheet Joints in a Waste Heat Boiler in a Sulphur Plant 某硫磺厂余热锅炉管板接头硫化速率预测
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-85070
F. Ju, Allen Miller, Simon Yuen, Brian Tkachyk
Sulfidation corrosion of the carbon steel tubes at the tube-to-tubesheet joint often governs the life of waste heat boilers in sulphur recovery plants. Conventional tube joints typically have a welded joint located at the hot-side face of the tubesheet. An alternative design involves welding the tubesheet joint at the cold-side face of the tubesheet, close to the boiler feed water. The alternative design also employs stainless steel cladding on the tubesheet face and a tube-hole sleeve selectively at high-temperature locations. Finite element heat transfer analysis is used to establish the thermal profiles of the conventional and the alternative designs. From the worked example, the alternative design provided a lower metal temperature by approximately 80 °F at the joint, as compared to the conventional tube joint. Sulfidation rate prediction based on a sample gas composition using ASSET (Alloy Selection System for Elevated Temperatures) Software predicts that the alternative design can reduce the sulfidation rate by 35% because of the lower metal temperature.
在硫磺回收装置中,管板接头处碳钢管的硫化腐蚀是影响余热锅炉寿命的重要因素。传统的管接头通常在管板的热侧面有一个焊接接头。另一种设计是在靠近锅炉给水的管板冷面焊接管板接头。替代设计还在管板表面采用不锈钢包层,并在高温位置选择性地使用管孔套。采用有限元传热分析建立了常规设计和备选设计的热分布。从工作实例来看,与传统的管接头相比,替代设计在接头处提供了约80°F的低金属温度。使用ASSET(高温合金选择系统)软件基于样品气体成分的硫化率预测预测,由于金属温度较低,替代设计可以将硫化率降低35%。
{"title":"Sulfidation Rate Prediction on Tube-to-Tubesheet Joints in a Waste Heat Boiler in a Sulphur Plant","authors":"F. Ju, Allen Miller, Simon Yuen, Brian Tkachyk","doi":"10.1115/PVP2018-85070","DOIUrl":"https://doi.org/10.1115/PVP2018-85070","url":null,"abstract":"Sulfidation corrosion of the carbon steel tubes at the tube-to-tubesheet joint often governs the life of waste heat boilers in sulphur recovery plants. Conventional tube joints typically have a welded joint located at the hot-side face of the tubesheet. An alternative design involves welding the tubesheet joint at the cold-side face of the tubesheet, close to the boiler feed water. The alternative design also employs stainless steel cladding on the tubesheet face and a tube-hole sleeve selectively at high-temperature locations. Finite element heat transfer analysis is used to establish the thermal profiles of the conventional and the alternative designs. From the worked example, the alternative design provided a lower metal temperature by approximately 80 °F at the joint, as compared to the conventional tube joint. Sulfidation rate prediction based on a sample gas composition using ASSET (Alloy Selection System for Elevated Temperatures) Software predicts that the alternative design can reduce the sulfidation rate by 35% because of the lower metal temperature.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"131741621","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
FEM Calculations of SIF and COA for Through Axial Cracks in Pipes in Geometrically Nonlinear Formulation 几何非线性形式下管道贯通裂纹SIF和COA的有限元计算
Pub Date : 2018-07-15 DOI: 10.1115/PVP2018-85033
A. Oryniak, I. Orynyak
The determination of stress intensity factors (SIF) and crack opening area or displacements (COA or COD) is important constituent when performing the “leak before break” analysis of piping systems in NPPs. The tabulated parametrical results of their calculation are widely presented in modern scientific and normative literature. Nevertheless, there is one aspect of crack behavior, at least in thin walled pipes, which still had not obtained its due attention. We mean here the geometrically nonlinear effect, which can be the big enough to be accounted for in practical applications. It is considered in geometrically linear analysis that only the inner pressure opens the crack, and COA and SIF are directly proportional to it. SIF is presented usually as solution for infinite plate multiplied by so-called bulging factor, BF, which depends on dimensionless crack length, i.e. ratio of crack length divided on square root of product of radius, R, and wall thickness, t. Two loading factors in thin walled pipes can contribute to geometrically nonlinear behavior. The first one is axial stresses induced by value of axial force or bending moment. The second one – is the inner pressure itself. The most attention in present paper is given to influence of the axial force. With this goal the numerical models were created for pipes with different ratios of R/t (20, 30, 40, 50) and different dimensionless crack length (2, 4, 6, 8). To exclude the nonlinearity due to circumferential stress the inner pressure is kept as a very small value and dimensionless SIF and COD values are calculated with respect to axial force. To prove the correctness of choosing the finite element types, meshing, number of elements along the thickness, loading steps the auxiliary problem of nonlinear modeling of transverse beam loaded additionally by very big axial force is considered. The very good correspondence was attained. For the pipe with axial crack the careful verification of numerical model was performed by comparison with linear results existing in literature. The results obtained are presented as a percentage of difference between the linear and nonlinear results. They show that influence of geometrical nonlinearity is fairly essential to be accounted in practice and can reach for practically real cases almost 3–10%. The change of SIF in percentages due to geometrical nonlinearity for different axial stress levels and for different crack lengths can be fairly well presented as unique dependence from product of stresses, radius to thickness ratio, and square root of dimensionless crack length. The change COD in central point of crack is slightly bigger than for SIF and the same unique dependence can be formulated for COD with only exception for small cracks λ < 3.
在对核电站管道系统进行“先漏后破”分析时,应力强度因子(SIF)和裂纹张开面积或位移(COA或COD)的确定是重要的组成部分。其计算的表化参数结果在现代科学和规范文献中广泛出现。然而,有一个方面的裂纹行为,至少在薄壁管道,仍然没有得到应有的重视。我们这里指的是几何非线性效应,它可以大到足以在实际应用中得到解释。在几何线性分析中,认为只有内压才能使裂纹开裂,COA和SIF与之成正比。SIF通常表示为无限大板的解乘以所谓的胀形因子BF,它取决于无因次裂纹长度,即裂纹长度除以半径R与壁厚t乘积的平方根的比率。薄壁管道中的两个载荷因素会导致几何非线性行为。第一类是由轴向力或弯矩值引起的轴向应力。第二,是内心的压力。本文重点讨论了轴向力的影响。为此,建立了具有不同R/t比(20、30、40、50)和不同无因次裂纹长度(2、4、6、8)的管道的数值模型。为了排除由于周向应力引起的非线性,管内压力保持为非常小的值,并且计算了轴向力的无因次SIF和COD值。为了证明所选择的有限元类型、网格划分、单元数沿厚度、加载步骤的正确性,考虑了横向梁在很大轴向力附加作用下的非线性建模辅助问题。达到了很好的通信。对于含轴向裂纹的管道,通过与已有的线性计算结果的比较,对数值模型进行了细致的验证。所得结果以线性和非线性结果之间的差异百分比表示。结果表明,几何非线性的影响在实际应用中是相当重要的,可以达到近3-10%的实际情况。不同轴向应力水平和不同裂纹长度下,几何非线性导致的SIF百分比变化可以很好地表现为应力积、半径厚度比和无因次裂纹长度平方根的独特依赖关系。裂纹中心点的COD变化略大于SIF,除了小裂纹λ < 3外,COD与SIF具有相同的惟一依赖关系。
{"title":"FEM Calculations of SIF and COA for Through Axial Cracks in Pipes in Geometrically Nonlinear Formulation","authors":"A. Oryniak, I. Orynyak","doi":"10.1115/PVP2018-85033","DOIUrl":"https://doi.org/10.1115/PVP2018-85033","url":null,"abstract":"The determination of stress intensity factors (SIF) and crack opening area or displacements (COA or COD) is important constituent when performing the “leak before break” analysis of piping systems in NPPs. The tabulated parametrical results of their calculation are widely presented in modern scientific and normative literature. Nevertheless, there is one aspect of crack behavior, at least in thin walled pipes, which still had not obtained its due attention. We mean here the geometrically nonlinear effect, which can be the big enough to be accounted for in practical applications.\u0000 It is considered in geometrically linear analysis that only the inner pressure opens the crack, and COA and SIF are directly proportional to it. SIF is presented usually as solution for infinite plate multiplied by so-called bulging factor, BF, which depends on dimensionless crack length, i.e. ratio of crack length divided on square root of product of radius, R, and wall thickness, t.\u0000 Two loading factors in thin walled pipes can contribute to geometrically nonlinear behavior. The first one is axial stresses induced by value of axial force or bending moment. The second one – is the inner pressure itself.\u0000 The most attention in present paper is given to influence of the axial force. With this goal the numerical models were created for pipes with different ratios of R/t (20, 30, 40, 50) and different dimensionless crack length (2, 4, 6, 8). To exclude the nonlinearity due to circumferential stress the inner pressure is kept as a very small value and dimensionless SIF and COD values are calculated with respect to axial force.\u0000 To prove the correctness of choosing the finite element types, meshing, number of elements along the thickness, loading steps the auxiliary problem of nonlinear modeling of transverse beam loaded additionally by very big axial force is considered. The very good correspondence was attained.\u0000 For the pipe with axial crack the careful verification of numerical model was performed by comparison with linear results existing in literature.\u0000 The results obtained are presented as a percentage of difference between the linear and nonlinear results. They show that influence of geometrical nonlinearity is fairly essential to be accounted in practice and can reach for practically real cases almost 3–10%. The change of SIF in percentages due to geometrical nonlinearity for different axial stress levels and for different crack lengths can be fairly well presented as unique dependence from product of stresses, radius to thickness ratio, and square root of dimensionless crack length. The change COD in central point of crack is slightly bigger than for SIF and the same unique dependence can be formulated for COD with only exception for small cracks λ < 3.","PeriodicalId":384066,"journal":{"name":"Volume 3B: Design and Analysis","volume":"36 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2018-07-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125229998","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
期刊
Volume 3B: Design and Analysis
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1