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Effect of Initial Microstructure on Soft Annealing of a Low-Carbon Bainitic Steel 初始组织对低碳贝氏体钢软退火的影响
Lei Zhu, Y. Yang, Yuyang Li, Huanhuan Xuan, Hongtao Chen, Yanxiang Zhang, M. Yan
A low-carbon bainitic drilled steel exhibits high hardness after hot rolling, which is not conducive to machining. In order to soften this type of drilled steel less than 260 HB and accelerate the subsequent soft annealing, a pre-austenitizing was designed based on thermodynamic calculations of phase stability.Different initial microstructures were prepared with three austenitizing temperatures (680 oC, 850 oC, 1000 oC) and three cooling methods (water quenching, oil quenching, and air cooling). The effects of initial microstructure during annealing with different temperatures and times on microstructures and mechanical properties were studied. The softening equations as a function of λ-value was established for different initial microstructures, and the relationships between annealing temperature, annealing time, activation energy and hardness were explored. The predicted hardness were consistent with the measured values. The initial microstructures affect activation energy, i.e., the activation energy for diffusion with respect to the martensitic structure was less than that of the bainitic structure, and the corresponding softening rate with the martensitic initial structure was greater. In addition, the higher the carbide content in the bainitic structure, the greater the proportion of martensite in the martensite-retained austenite (M/A) structure, the more lath-shaped M/A and the less massive M/A, the smaller the activation energy tended to be.
低碳贝氏体钻孔钢热轧后硬度高,不利于加工。基于相稳定性的热力学计算,设计了一种预奥氏体化工艺,以使此类钻孔钢的软化程度小于260 HB,并加快后续的软退火过程。采用三种奥氏体化温度(680℃、850℃、1000℃)和三种冷却方式(水淬、油淬、空冷)制备了不同的初始组织。研究了不同退火温度和退火时间初始组织对合金组织和力学性能的影响。建立了不同初始组织的软化方程λ值函数,探讨了退火温度、退火时间、活化能与硬度的关系。预测硬度与实测值一致。初始组织影响活化能,即马氏体组织的扩散活化能小于贝氏体组织的扩散活化能,相应的软化速率与马氏体初始组织有关。贝氏体组织中碳化物含量越高,马氏体-保留奥氏体(M/A)组织中马氏体所占比例越大,板条状的M/A越多,块状的M/A越少,活化能越小。
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引用次数: 0
Impact of strain aging kinetics on the failure of thin steel wire ropes 应变老化动力学对细钢丝绳失效的影响
T. Mező, P. Barkóczy
Under quasi-static loading an irregular failure mode of high-strength thin-carbon steel cords were observed after low temperature thermal aging. Character and kinetics of damage in such wire ropes highly depend on the plastic elongation of the steel wires, which is significantly modified by the strain aging effect. In this paper, the static strain aging effect on heavily drawn high-carbon steel wires and their cords is experimentally studied in the 100–200 °C temperature range. Quantitative analysis of the affected strength and strain parameters is given. Kinetics of the aging process is discussed, and based on this, the macroscopic failure mechanism is fundamentally explained.
在准静态载荷作用下,高强度薄碳钢帘线经低温热老化后呈现不规则破坏模式。这种钢丝绳的损伤特性和损伤动力学高度依赖于钢丝的塑性伸长,而钢丝的塑性伸长受到应变老化效应的显著影响。本文在100 ~ 200℃的温度范围内,实验研究了高碳钢钢丝及其绳的静态应变老化效应。定量分析了受影响的强度和应变参数。讨论了时效过程动力学,在此基础上,从根本上解释了宏观破坏机理。
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引用次数: 0
Niobium oxide and tantalum oxide micro- and nanostructures grown using material recovered from mining tailings 利用尾矿回收材料制备氧化铌和氧化钽微纳米结构
B. Sotillo, L. Alcaraz, F. López, F. J. Alguacil, O. Rodríguez, P. Fernández
: Niobium and tantalum-based oxides were recovered from mining tailings. These oxides were used as starting material for growing micro- and nanostructures by the evaporation method. The morphology and crystal structure of the final oxides were evaluated using X-ray diffraction (XRD), micro-Raman spectroscopy, and scanning electron microscopy (SEM). After the thermal treatment, microrods of both oxides were obtained, which presented exotic stoichiometries Nb 22 O 54 and K 6 Ta 10.8 O 30 , respectively.
:从尾矿中回收铌、钽基氧化物。这些氧化物被用作蒸发法制备微纳米结构的起始材料。利用x射线衍射(XRD)、微拉曼光谱(micro-Raman spectroscopy)和扫描电子显微镜(SEM)对最终氧化物的形貌和晶体结构进行了表征。热处理后得到了两种氧化物的微晶,其化学计量量分别为Nb 22 O 54和k6 Ta 10.8 O 30。
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引用次数: 0
Research on the friction properties of DP600 stainless steel as a function of bending angle and pin diameter DP600不锈钢摩擦性能随弯曲角和销径的变化规律研究
S. Sanchez-Caballero, M. A. Selles, R. Pla-Ferrando, J. Seguí, M. Peydro
: The rapid evolution of materials and manufacturing processes, driven by global competi-tion and new safety and environmental regulations has had an impact on automotive structures (Body In White; BIW) manufacturing. The need for lighter vehicles, with more equipment, that are safer and eco-friendly at the same time, relates to the entire life cycle of the car. Car and steelmakers agree that weight reduction is possible, and the solution involves the use of new advanced high-strength steels. Thinner and stronger materials lead to higher demands on stamping, the most used manufacturing in BIW parts. The use of advanced high-strength steels raises new challenges, especially concerning the lubrication between the die and the sheet. To study the lubrication conditions of the stamping process, a sheet metal forming a simulator was developed. The simulator consists of two cylinders that pull the strip of steel and a pin in between. The angle between the cylinders can be adjusted from 0 to 90 degrees, which allows analysis of the effect of the stamping angle. The pull force and velocity can be set and measured, and the peripheric pin velocity, the strain, and the strain velocity can be measured as well. In this work, the tribological properties of Dual-Phase 600 stainless steel using different processing conditions have been analyzed. To this end, a factorial experiments design with twelve parameters that compare the behavior of different angles and diameters was run. The results showed that the friction coefficient increases by increasing the bending angle and decreases with pin diameter.
在全球竞争和新的安全和环境法规的推动下,材料和制造工艺的快速发展对汽车结构产生了影响(白车身;BIW)制造。对更轻、装备更多、同时更安全、更环保的车辆的需求关系到汽车的整个生命周期。汽车和钢铁制造商一致认为,减轻重量是可能的,解决办法包括使用新型先进的高强度钢材。更薄和更强的材料导致对冲压的更高要求,这是白车身零件中最常用的制造方法。先进的高强度钢的使用提出了新的挑战,特别是关于模具和板之间的润滑。为研究冲压成形过程中的润滑条件,研制了板料成形模拟器。模拟器由两个拉动钢带的圆柱体和中间的一个销钉组成。气缸之间的角度可以从0到90度调整,从而可以分析冲压角度的影响。可以设置和测量拉力和速度,还可以测量外周销速度、应变和应变速度。本文对双相600不锈钢在不同加工条件下的摩擦学性能进行了分析。为此,进行了12个参数的析因试验设计,比较了不同角度和直径的行为。结果表明:摩擦系数随弯曲角的增大而增大,随销径的增大而减小;
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引用次数: 2
Recent advances in Digital Image analysis applied to metal forming 数字图像分析在金属成形中的应用进展
M. A. Selles, S. Sanchez-Caballero, Jaume Gomez-Caturla, O. Gonzalez, Miguel Angel Peydró-Rasero
Digital Image analysis is used, among other things, to see how an object's surface changes over time. This technology can be applied to metal forming. A complete literature review of the recent advances in the application of such image analysis to metal forming processes is presented. We analyze how researchers apply the technique to different tests (tensile, bending, or fatigue tests), observing the advantages it presents compared to conventional methods, as well as the advances that have been made regarding the methodology used throughout the last years, including an analysis of the different existing patterns and their application procedures. We found that the image analysis has great applicability and that, in addition, the data obtained through it have high reliability when compared with numerical results. In the paper, the advantages of using Digital Image analysis applied to metals characterization are reviewed, and some examples of using this technique are also presented.
除其他外,数字图像分析用于观察物体表面如何随时间变化。该技术可应用于金属成形。完整的文献综述,最近的进展,在应用这种图像分析金属成形过程提出。我们分析了研究人员如何将该技术应用于不同的测试(拉伸、弯曲或疲劳测试),观察了与传统方法相比它所呈现的优势,以及在过去几年中所使用的方法方面取得的进展,包括对不同现有模式及其应用程序的分析。我们发现图像分析具有很强的适用性,并且通过它获得的数据与数值结果相比具有很高的可靠性。本文综述了数字图像分析应用于金属表征的优点,并给出了应用该技术的一些实例。
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引用次数: 0
Hot stamping research scenarios from the last decade 烫印研究场景从过去的十年
Luis Miguel Arias, G. Artola, Igone Porto
Hot stamping technology has shown a significant scientific yield in the last decade. The research activity in that field has spread across several disciplines such as materials science, mechanics, process engineering, instrumentation, physics, or part-tool design engineering. Some recent publications have gathered this richness in the format of scientific reviews. This work is aimed to draw a picture of this scientific production in bibliometric terms, which are complementary to the existing reviews. The literature is, in this case, approached from different angles: geographical, collaborative, disseminative and keyword based. The first one leads to mapping the share of each region worldwide in the advance of the hot stamping technology in terms of scientific production volume. The second angle allows identifying the most productive networks that have been stablished between institutions and the most influent agents in the field. The third one ranks the most influent journals and events based on citation rates, which indicates where to publish in order to get the highest impact. Finally, the fourth approach targets to infer research trends from assessing the keywords employed in the published scientific literature. Altogether, the results show a scenario with Asia as the major player both in volume and networking success, CHS2 as the most relevant event and exploring alternatives to the conventional AlSi coated 22MnB5 hot stamping as a subject rising of interest.
在过去的十年里,热冲压技术已经显示出显著的科学成果。该领域的研究活动已经扩展到几个学科,如材料科学、力学、工艺工程、仪器仪表、物理学或零件工具设计工程。最近的一些出版物以科学评论的形式收集了这种丰富的内容。这项工作的目的是用文献计量学的术语来描绘这一科学生产的图景,这是对现有评论的补充。文献,在这种情况下,从不同的角度:地理,协作,传播和关键字为基础。第一个导致映射的份额,每个地区在全球范围内的热冲压技术的进步,在科学的产量。第二个角度可以确定机构与该领域最有影响力的行动者之间建立的最具生产力的网络。第三个是根据引用率对最具影响力的期刊和事件进行排名,这表明在哪里发表文章才能获得最大的影响力。最后,第四种方法旨在通过评估已发表的科学文献中使用的关键词来推断研究趋势。总之,结果表明亚洲在数量和网络成功方面都是主要参与者,CHS2是最相关的事件,探索传统AlSi涂层22MnB5热冲压的替代方案是一个越来越感兴趣的主题。
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引用次数: 1
Microstructural and thermomechanical simulation of the additive manufacturing process in 316L austenitic stainless steel 316L奥氏体不锈钢增材制造过程的显微组织和热力学模拟
G. Haidemenopoulos, M. Sotiriou, John S. Aristeidakis, Maria-Ioanna T. Tzini, I. Papadioti, N. Aravas
Additive manufacturing of an AISI 316L austenitic stainless steel was studied via an integrated thermomechanical and microstructural modelling approach. A finite element technique was employed to evaluate the temperature evolution due to successive material deposition. Heat transfer simulations provided the temperature field history, required to determine the microstructural evolution. Thermodynamic and kinetic simulations were employed to calculate temporal and spatial distribution of phases and alloying elements upon solidification and subsequent thermal cycling. The ensuing microstructural properties could be provided as an input for a mechanical finite element analysis to calculate, based on local mechanical properties, the residual stresses and distortions.
采用综合热力学和显微组织建模方法,研究了aisi316l奥氏体不锈钢的增材制造工艺。采用有限元方法分析了连续沉积过程中温度的变化规律。传热模拟提供了确定微观组织演变所需的温度场历史。采用热力学和动力学模拟计算了凝固过程和热循环过程中相和合金元素的时空分布。随后的微观组织性能可以作为力学有限元分析的输入,根据局部力学性能,计算残余应力和变形。
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引用次数: 1
Derivation of appropriate conditions for Additive Manufacturing technology using hot-wire laser method 热丝激光增材制造技术适宜条件的推导
Song Zhu, Youichi Nakahara, H. Aono, R. Ejima, Motomichi Yamamoto
The aim of this research was to develop a high-efficiency and high-material-utilization additive manufacturing technology using the hot-wire laser method. In this study, the optimization of process conditions using a combination of a high-power diode laser with a relatively large laser spot hot-wire system was investigated. The effects of welding parameters such as the laser power, process speed, and wire feeding rate (wire feeding speed/process speed) on the bead appearance evaluation and the cross-sectional characteristics ( e.g. effective width, effective height, maximum height, and near net shape rate) were studied in detail. The process phenomena of the three-layer and multi-layer deposition were investigated by in-situ observation via a high-speed camera. Energy density input and wire feeding rate were found to be dominant parameters influencing both the stability of phenomena and bead appearance. With the increase of process speed, the effective width decreases, the effective height, maximum height, and the near net shape rate increases. Additionally, all measured values of the wire feeding rate of 30 improve compared with the values of the wire feeding rate of 20. The near net shape rate increased and the effective width over 10mm of three-layer deposition for the laser spot width of 11 mm was obtained with suitable process parameters. The defect-free 15-layer wall modeling of more than 50 mm in height, 8 mm in width, and 250 mm in length was obtained with high efficiency using the optimum conditions by the hot-wire laser method.
本研究的目的是利用热线激光方法开发一种高效率、高材料利用率的增材制造技术。本文研究了大功率二极管激光器与较大激光光斑热线系统相结合的工艺条件优化。详细研究了激光功率、工艺速度、送丝速度(送丝速度/工艺速度)等焊接参数对焊缝外观评价和截面特性(有效宽度、有效高度、最大高度和近净形率)的影响。利用高速摄像机对三层和多层沉积的过程现象进行了原位观察。发现能量密度输入和送丝速度是影响现象稳定性和珠形的主要参数。随着加工速度的增加,有效宽度减小,有效高度、最大高度增大,近净形率增大。此外,与送丝率为20时相比,送丝率为30时的所有测量值都有所提高。在合适的工艺参数下,近净成形率提高,激光光斑宽度为11 mm时,三层沉积的有效宽度大于10mm。在最佳条件下,利用热线激光方法高效地获得了高大于50 mm、宽大于8 mm、长大于250 mm的无缺陷15层墙体造型。
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引用次数: 3
Extraction of iron from Russian red mud by a carbothermic reduction and magnetic separation process 碳热还原-磁选法从俄罗斯赤泥中提取铁
D. Zinoveev, A. Petelin, P. Grudinsky, A. Zakunov, V. Dyubanov
Red mud is a hazardous waste of alumina production. Currently, the total accumulated amount of red mud is over 4 billion tons. The promising method of red mud processing is carbothermic reduction of iron at 1000–1400 °C into metallic form followed by magnetic separation. In this study, the mechanism of carbothermic solid-phase reduction of red mud was investigated. Based on the experimental data, the two-step mechanism of the first rapid stage of the process was proposed, which leads to almost full iron reduction. The estimated value of activation energy has indicated that solid-phase diffusion is a rate-controlling step for this stage. However, almost full reduction is necessary, but insufficient factor for successful magnetic separation. The second crucial factor of the process is enlargement of iron grain size, which leads to gangue-grain release during grinding and increases efficiency of the magnetic separation. The prediction model of iron grain growth process during the carbothermic reduction process was suggested. The calculation of average size of iron grains formed during reduction process that performed according to the assumption of diffusion-controlled process showed their correlation with experimental data. Various methods were proposed to promote the process of iron grain growth during carbothermic reduction of red mud.
赤泥是氧化铝生产过程中产生的有害废物。目前,我国赤泥累计总量已超过40亿吨。铁在1000 ~ 1400℃碳热还原成金属形态,再进行磁分离,是一种很有前途的赤泥处理方法。研究了赤泥碳热固相还原的机理。根据实验数据,提出了该过程第一快速阶段的两步机制,该阶段导致铁几乎完全还原。活化能的估计值表明,固相扩散是这一阶段的速率控制步骤。然而,几乎完全还原是必要的,但不足以使磁选成功。该工艺的第二个关键因素是铁粒度的增大,这导致了磨矿过程中脉石颗粒的释放,提高了磁选效率。提出了碳热还原过程中铁晶粒生长过程的预测模型。根据扩散控制过程的假设对还原过程中形成的铁晶粒的平均尺寸进行了计算,结果与实验数据具有一定的相关性。提出了促进赤泥碳热还原过程中铁粒生长的多种方法。
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引用次数: 1
PREDICTIVE TOOLS FOR IN-LINE ISOTHERMAL EXTRUSION OF 6XXX ALUMINUM ALLOYS 6xxx铝合金在线等温挤压预测工具
S. Barella, A. Gruttadauria, Riccardo Gerosa, Giacomo Mainetti, Teodoro Mainetti
: During the last fifty years, the metal forming of aluminum alloys advanced significantly, leading to a more competitive market on which production rate and overall quality are kept as high as possible. Within the aluminum industries, extrusion plays an important role, since many industrial products with structural or even aesthetic functions are realized with this technology. Especially in the automotive industry, the use of aluminum alloys is growing very fast, since it permits a considerable weight loss and thus a reduction of the emission. Nevertheless, the stringent quality standards required don’t allow the use of extruded aluminum alloys produced for common build-ing applications. An important parameter that can be used as an index of the quality of the extruded product is the emergent temperature: if the temperature at the exit of the press is kept constant within a certain limit, products with homogeneous properties and high-quality surface are obtained and the so called “isothermal extrusion” is achieved. As extrusion industries are spread all over the world with different levels of automation and control, a universal but simple on-line tool for deter-mining the best process condition to achieve isothermal extrusion is of particular interest. The aim of this work is to implement this model, which allows evaluation of the thermal gradient which has to be imposed on the billet. Several experiments have been carried out on an industrial extrusion press, and the outer temperature was recorded and compared with the simulated one to demon-strate the model consistency.
在过去的五十年里,铝合金的金属成形取得了显著的进步,导致了一个更有竞争力的市场,在这个市场上,生产率和整体质量尽可能地保持在高水平。在铝工业中,挤压扮演着重要的角色,因为许多具有结构甚至美学功能的工业产品都是用这种技术实现的。特别是在汽车工业中,铝合金的使用增长非常快,因为它允许相当大的重量减轻,从而减少排放。然而,严格的质量标准要求不允许使用为普通建筑应用而生产的挤压铝合金。可以作为挤压产品质量指标的一个重要参数是出料温度:如果在挤出机出口温度保持恒定在一定范围内,就可以得到性能均匀、表面高质量的产品,即所谓的“等温挤压”。由于挤压工业遍布世界各地,自动化和控制水平各不相同,一种通用但简单的在线工具用于确定实现等温挤压的最佳工艺条件是特别有趣的。这项工作的目的是实现该模型,该模型允许对必须施加在坯料上的热梯度进行评估。在一台工业挤压机上进行了多次实验,记录了外部温度,并与模拟温度进行了比较,验证了模型的一致性。
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引用次数: 1
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