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Synthesis, Characterization and Thermal Study of Some new Copolyesters from mono-carbonyl analogues of Curcumin and Thymol blue dye 姜黄素与百里酚蓝染料单羰基共聚物的合成、表征及热性能研究
Pub Date : 2023-08-28 DOI: 10.36329/jkcm/2022/v2.i9.13322
None Muhanad T. Almayyahi, None Basil A. Saleh, None Baqer A. Almayyahi
A series of copolyesters were prepared from a dicarboxylic acid, curcumin analogues (monocarbonyl) and thymol blue dye in the mole ratio of 2:1:1 by direct polycondensation using triethylamine (Et3N) as the condensation agent. The dicarboxylic used is 2,6-Pyridine dicarbonyl dichloride acid. The curcumin analogues were prepared by acid catalyzed Aldol condensation reaction. These copolyesters were characterized by FT-IR. The fluorescence of the synthesized copolyesters was also investigated. Furthermore, Thermo gravimetric analysis (TGA) was used to investigate the thermal stability of these copolymers
以三乙胺(Et3N)为缩合剂,以二羧酸、姜黄素类似物(单羰基)和百里香酚蓝染料为原料,按摩尔比2:1:1直接缩聚制得一系列共聚酯。所使用的二羧酸是2,6-吡啶二羰基二氯酸。采用酸催化醛醇缩合反应制备姜黄素类似物。用FT-IR对这些共聚酯进行了表征。并对合成的共聚酯的荧光特性进行了研究。此外,用热重分析(TGA)研究了这些共聚物的热稳定性
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Journal of Kufa for Chemical Sciences
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