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FEATURES OF MICROARC OXIDATION OF MAGNESIUM ALLOYS AND CORROSION DESTRUCTION OF THE RESULTING COATINGS 镁合金微弧氧化的特点及其镀层的腐蚀破坏
Pub Date : 2023-10-16 DOI: 10.15588/1607-6885-2023-3-1
V. Greshta, M. Brykov, V. Shalomeev, D. Pavlenko, D. Tkach, V. Efremenko, I. Petryshynets
Purpose of this work was to determine the characteristics of coatings formed on magnesium alloys during the process of micro-arc oxidation (MAO) in an electrolyte with minimal content of basic solution components. Additionally, the study aims to identify research directions that can ensure controlled solubility of magnesium alloys with MAO coatings in a corrosive and active environment. Research methods. The study was performed on samples of MЛ5 alloy. The MAO was conducted using an alternating current of 380 V and 50 Hz, along with a battery of capacitors with adjustable capacity. The electrolyte used was a combination of potassium hydroxide and sodium liquid glass. Corrosion tests of the treated samples were conducted in a 3 % aqueous NaCl solution. The surface of the samples after MAO was examined using optical and scanning electron microscopy. Results. The results of research in the field of MAO of magnesium alloys are considered. It is shown that the use of MAO coatings is one of the promising directions for developing methods to control the dissolution rate of magnesium alloy products. The concentration of reagents in the electrolyte and the processing time were minimized. It was found that it is advisable to complete the treatment before the phase of intense sparking. The initiation of the sparking process leads to the damage of the barrier layer by microarc discharges, which reduces the corrosion resistance of the coating. Scientific novelty. It was found that the degree of corrosion damage was minimal for the sample treated for 30 s. The obtained result can be explained by the termination of the MАO process at the moment when a dense coating has already formed at the first stage of the process, but the second stage with the formation of micro-arc discharges, which damage the already formed oxide layer, has not yet begun. Practical value. The results of the study will serve as a basis for further work aimed at creating magnesium alloy products with a controlled dissolution time in a corrosive environment. This is especially relevant for medical products, namely metal fixators for osteosynthesis with a controlled rate of biological resorption.
研究方法。研究对象为MЛ5合金样品。所使用的电解质是氢氧化钾和液态玻璃钠的混合物。处理后的样品在3% NaCl水溶液中进行腐蚀试验。结果。电解液中试剂的浓度和处理时间被最小化。结果表明,在产生强烈火花的阶段之前完成处理是可取的。火花过程的引发导致微弧放电对阻挡层的破坏,降低了涂层的耐腐蚀性。 科学的新奇。结果表明,处理30 s后,试样的腐蚀损伤程度最小。所得到的结果可以用MАO过程的终止来解释,在该过程的第一阶段,致密涂层已经形成,而第二阶段,微弧放电的形成,破坏已经形成的氧化层,还没有开始。 实用价值。研究结果将作为进一步工作的基础,旨在创造在腐蚀性环境中具有控制溶解时间的镁合金产品。这尤其适用于医疗产品,即用于骨合成的金属固定物,具有可控的生物吸收率。
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 Research methods. The study was performed on samples of MЛ5 alloy. The MAO was conducted using an alternating current of 380 V and 50 Hz, along with a battery of capacitors with adjustable capacity. The electrolyte used was a combination of potassium hydroxide and sodium liquid glass. Corrosion tests of the treated samples were conducted in a 3 % aqueous NaCl solution. The surface of the samples after MAO was examined using optical and scanning electron microscopy.
 Results. The results of research in the field of MAO of magnesium alloys are considered. It is shown that the use of MAO coatings is one of the promising directions for developing methods to control the dissolution rate of magnesium alloy products. The concentration of reagents in the electrolyte and the processing time were minimized. It was found that it is advisable to complete the treatment before the phase of intense sparking. The initiation of the sparking process leads to the damage of the barrier layer by microarc discharges, which reduces the corrosion resistance of the coating.
 Scientific novelty. It was found that the degree of corrosion damage was minimal for the sample treated for 30 s. The obtained result can be explained by the termination of the MАO process at the moment when a dense coating has already formed at the first stage of the process, but the second stage with the formation of micro-arc discharges, which damage the already formed oxide layer, has not yet begun.
 Practical value. The results of the study will serve as a basis for further work aimed at creating magnesium alloy products with a controlled dissolution time in a corrosive environment. This is especially relevant for medical products, namely metal fixators for osteosynthesis with a controlled rate of biological resorption.","PeriodicalId":489209,"journal":{"name":"Novì materìali ì tehnologìï v metalurgìï ta mašinobuduvannì","volume":"18 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136112228","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
MATHEMATICAL MODELING OF PITTING RESISTANCE IN 06XH28МДТ ALLO-HEAT EXCHANGERS EXPOSED TO CIRCULATING WATERS 暴露于循环水中的06xh28МДТ allow -热交换器点蚀电阻的数学建模
Pub Date : 2023-10-16 DOI: 10.15588/1607-6885-2023-3-7
A. Dzhus, O. Narivskyi, S. Byelikov, S. Subbotin, T. Pulina, S. Leoshchenko
Purpose. The aim of the study is to develop mathematical models that describe the dependences of critical pitting temperatures of 06ХН28МДТ alloy (analogous to AISI904L steel) in model circulating waters with pH 4...8 and chloride concentration from 350 to 600 mg/L. Research methods. The developed mathematical models are based on multivariate linear regressions of the first order and multivariate quadratic regressions with a combination of features. Results. It has been established that the critical pitting temperatures of the 06ХН28МДТ alloy increase with increasing pH of model circulating waters, Ni, Mo content, volume of titanium nitrides, and decreasing chloride concentration in the medium, Cr content within the standard, and average austenite grain diameter. Scientific novelty. Based on the established dependencies between the critical pitting temperatures of the 06ХН28МДТ alloy and its chemical composition within the standard and structural heterogeneity, the mechanisms of their influence on the pitting resistance of this structural material in recycled industrial waters were developed. It was found that the size of inclusions of titanium nitrides and oxysulfides in the alloy does not affect the probability of the formation and growth of stable pitting in their vicinity in chloride-containing media. Practical value. To apply the developed mathematical models to the selection of the most resistant to pitting in recycled industrial waters of 06ХН28МДТ alloy melts and to predict their pitting during the use of heat exchangers have been offered.
目的。该研究的目的是建立数学模型,描述06ХН28МДТ合金(类似于AISI904L钢)在pH为4的模型循环水中的临界点蚀温度的依赖性。8、氯化物浓度350 ~ 600mg /L。 研究方法。所建立的数学模型是基于一阶多元线性回归和多元二次回归的特征组合。 结果。结果表明:06ХН28МДТ合金的临界点蚀温度随着模型循环水pH值、Ni、Mo含量、氮化钛体积、介质中氯离子浓度、Cr含量在标准范围内、平均奥氏体晶粒直径的降低而升高;科学的新奇。基于已建立的06ХН28МДТ合金的临界点蚀温度与其在标准范围内的化学成分和结构非均质性之间的依赖关系,研究了它们对该结构材料在再生工业水中抗点蚀性能的影响机制。结果表明,在含氯介质中,合金中氮化钛和氧化硫化物夹杂物的大小不影响其附近稳定点蚀形成和生长的概率。 实用价值。将所建立的数学模型应用于06ХН28МДТ合金熔体在循环工业水中抗点蚀的选择,并对其在换热器使用过程中的点蚀进行预测。
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引用次数: 0
CALCULATION OF THE STRESS-STRAIN STATE OF THE NOSE STAND OF AN AIRCRAFT LANDING GEAR WITH A RADIUS TRANSITION BY THICKNESS WHEN BUILDING A LOCAL MODEL 建立局部模型时,计算了某型飞机起落架机头架半径随厚度变化的应力-应变状态
Pub Date : 2023-10-16 DOI: 10.15588/1607-6885-2023-3-10
T. Levytska, I. Pozhuieva, O. Mytryashkin, O. Manzhos
Purpose. Study of the stress-strain state and fatigue life of the local zone of the compartment structure, namely, the radial transition between the wall thicknesses from the regular zone to the place of thickening in the connection zone with the reinforcement element. The main task of this work is to estimate the level of stress in the zone of the radial transition using the numerical solution of the problem, for the further assessment of the resource of the structure. Research methods. Construction of a local model and numerical calculations of the stress-strain state of the considered structure using PATRAN/NASTRAN software complexes. Using the Mesh Seed tool to mark the position of nodes on the edges of surfaces. In addition to flat elements, bar elements were used in the model to simulate rivets. For the numerical solution of the presented problem, the nonlinear solver 106 - Nonlinear Static was used. Results. A numerical calculation of the stress-strain state of the nose strut of the aircraft landing gear with a radial transition in thickness during local modeling was carried out. Visualization of linear displacement and fields of normal stresses, as well as graphs of normal stresses on the lower and upper surface of the wall, and the dependence of the values of normal stresses in the radial transition zone were obtained. The deflection of the plate between the reinforcement element is plotted and the maximum deflection in the middle of the span is obtained. Scientific novelty. Application of the method of calculating the stress-strain state of complex structures of aviation equipment elements using computer software complexes in the conditions of modern development of aviation science and technology. Practical value. The obtained calculations made it possible to estimate the resource of the local area of the structure - the radius transition between different wall thicknesses. The results of the analysis and the method of numerical calculation of the stress-strain state of the considered model can be used for further assessment of the resource and static strength of the structure of the aircraft landing gear compartment.
目的。研究隔室结构局部区域的应力-应变状态和疲劳寿命,即与配筋单元连接区域的壁厚从规则区到加厚处的径向过渡。本工作的主要任务是利用问题的数值解估计径向过渡区域的应力水平,以便进一步评估结构的资源。 研究方法。利用PATRAN/NASTRAN复合软件建立局部模型并对考虑结构的应力-应变状态进行数值计算。使用网格种子工具在曲面边缘标记节点的位置。模型除采用平面单元外,还采用杆单元模拟铆钉。对于所提出的问题的数值解,使用非线性求解器106 -非线性静态。 结果。对某型飞机起落架机头支柱进行了局部建模时厚度径向过渡的应力-应变状态的数值计算。得到了直线位移场和正应力场的可视化,以及壁面上下表面的正应力图,以及径向过渡区正应力值的依赖关系。绘制了加固单元之间的板的挠度,并得到了跨中部的最大挠度。 科学的新奇。利用计算机复合体软件计算航空装备元件复杂结构应力应变状态方法在现代航空科学技术发展条件下的应用[j] x0D;实用价值。得到的计算可以估计结构局部区域的资源-不同壁厚之间的半径过渡。所考虑模型的应力-应变状态的分析结果和数值计算方法可用于进一步评估飞机起落架室结构的资源和静强度。
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 Research methods. Construction of a local model and numerical calculations of the stress-strain state of the considered structure using PATRAN/NASTRAN software complexes. Using the Mesh Seed tool to mark the position of nodes on the edges of surfaces. In addition to flat elements, bar elements were used in the model to simulate rivets. For the numerical solution of the presented problem, the nonlinear solver 106 - Nonlinear Static was used.
 Results. A numerical calculation of the stress-strain state of the nose strut of the aircraft landing gear with a radial transition in thickness during local modeling was carried out. Visualization of linear displacement and fields of normal stresses, as well as graphs of normal stresses on the lower and upper surface of the wall, and the dependence of the values of normal stresses in the radial transition zone were obtained. The deflection of the plate between the reinforcement element is plotted and the maximum deflection in the middle of the span is obtained.
 Scientific novelty. Application of the method of calculating the stress-strain state of complex structures of aviation equipment elements using computer software complexes in the conditions of modern development of aviation science and technology.
 Practical value. The obtained calculations made it possible to estimate the resource of the local area of the structure - the radius transition between different wall thicknesses. The results of the analysis and the method of numerical calculation of the stress-strain state of the considered model can be used for further assessment of the resource and static strength of the structure of the aircraft landing gear compartment.","PeriodicalId":489209,"journal":{"name":"Novì materìali ì tehnologìï v metalurgìï ta mašinobuduvannì","volume":"75 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136112400","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
MULTICRITERION OPTIMIZATION OF PRESS COLUMN CROSSSECTION 压柱截面的多准则优化
Pub Date : 2023-10-11 DOI: 10.15588/1607-6885-2023-3-9
V. Shevchenko, S. Ryagin, D. Artsybasheva
Purpose. Increase of the competitiveness is the important scientific and practical task in machine building. The press is the stationary equipment, but reduction of weight of its elements, in particular – columns, reduces manufacturing cost, facilitates transportation and installation, therefore assists in increase of product attraction at market relations. The purpose is to reduce press column weight without complication of technological process of its manufacturing and without additional expenses for a concrete one-columned press by means of structure optimization. Research methods. The mathematical model has been developed on the basis of formula of combined strength of materials. The pure bending with tension results from operation of one-columned press. Multicriterion optimization has been carried out by means of computer facilities. Calculation was carried out by means of the program written in language Basic. Results. The press П6330 with box-shaped cross-section has been chosen as a base variant. The optimal geometrical dimensions have been determined for the offered T-shaped welded cross-section of a column. Technological process of manufacturing of such column is simplified. Scientific novelty. The T-shaped welded column cross-section has been offered for the purpose of modernization. Such cross-section scheme is more perspective and technological. The following 3 criteria have been chosen at multicriterion optimization carrying out: equal strength with the base variant, the greatest uniformity of distribution of stress by cross-section, the least area of cross-section. The main geometrical dimensions of cross-section have been chosen as 4 variable parameters. It was considered, that thickness of metal sheet is discrete and standard. Practical value. Multicriterion optimization that had been carried out provides reduction of column weight approximately by 45 % for the modernized variant without increase in dimensions of cross-section. It gives the opportunity to reduce considerably the column manufacturing cost in comparison with a base variant, and also to facilitate transportation and installation of the press.
目的。提高竞争力是机械制造业的重要科学和现实任务。压力机是一种固定设备,但由于其各部件,特别是立柱重量的减轻,降低了制造成本,方便了运输和安装,因此有助于增加产品在市场关系中的吸引力。目的是通过结构优化,在不增加混凝土单柱压力机制造工艺的复杂性和额外费用的情况下,减轻压力机柱的重量。 研究方法。在材料组合强度公式的基础上建立了数学模型。纯张力弯曲是由单柱压力机运行造成的。利用计算机设备进行了多准则优化。用Basic. 编写程序进行计算;结果。选择具有箱形截面的压力机П6330作为基本型号。确定了所提供的t形焊接截面的最佳几何尺寸。简化了这种塔的制造工艺流程。 科学的新奇。为现代化建设提供了t形焊接柱截面。这样的截面方案更具前瞻性和技术性。在进行多准则优化时,选取了与基型强度相等、截面应力分布均匀性最大、截面面积最小的3个准则。横截面的主要几何尺寸选择为4个可变参数。考虑到金属板的厚度是离散的和标准的。 实用价值。在不增加截面尺寸的情况下,进行了多准则优化,使现代化改型的柱重减少了约45%。与基础变体相比,它提供了大大降低柱制造成本的机会,也便于印刷机的运输和安装。
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 Research methods. The mathematical model has been developed on the basis of formula of combined strength of materials. The pure bending with tension results from operation of one-columned press. Multicriterion optimization has been carried out by means of computer facilities. Calculation was carried out by means of the program written in language Basic.
 Results. The press П6330 with box-shaped cross-section has been chosen as a base variant. The optimal geometrical dimensions have been determined for the offered T-shaped welded cross-section of a column. Technological process of manufacturing of such column is simplified.
 Scientific novelty. The T-shaped welded column cross-section has been offered for the purpose of modernization. Such cross-section scheme is more perspective and technological. The following 3 criteria have been chosen at multicriterion optimization carrying out: equal strength with the base variant, the greatest uniformity of distribution of stress by cross-section, the least area of cross-section. The main geometrical dimensions of cross-section have been chosen as 4 variable parameters. It was considered, that thickness of metal sheet is discrete and standard.
 Practical value. Multicriterion optimization that had been carried out provides reduction of column weight approximately by 45 % for the modernized variant without increase in dimensions of cross-section. It gives the opportunity to reduce considerably the column manufacturing cost in comparison with a base variant, and also to facilitate transportation and installation of the press.","PeriodicalId":489209,"journal":{"name":"Novì materìali ì tehnologìï v metalurgìï ta mašinobuduvannì","volume":"20 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136253776","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
DESTRUCTION AND INCREASE OF STRENGTH OF POWDER PRODUCTS 破坏和提高粉末制品的强度
Pub Date : 2023-10-11 DOI: 10.15588/1607-6885-2023-3-13
V. Pleskach, I. Akimov
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引用次数: 0
THE INFLUENCE ELECTROSLAG HARD-FACING ON THE CHEMICAL COMPOUND OF NONMETALLIC INCLUSIONS AND FUSION ZONE 电渣堆焊对非金属夹杂物化学成分及熔合区的影响
Pub Date : 2023-10-11 DOI: 10.15588/1607-6885-2023-3-6
Е. Parahnevich
Purpose. As a result of the study, it is necessary to determine the factors that influence the chemical composition of the fusion zone and non-metallic inclusions during electroslag surfacing, which is used in the restoration of railway transport parts, namely electric locomotives of the ЧС-4, ЧС-6, ЧС-8, etc. brands. Research methods. The chemical composition of non-metallic inclusions was studied using the CAMECA X-ray spectroscopic microanalysis unit and the "SUPRA 40 WDS" scanning electron microscope manufactured by Carl Zeiss (Germany). The measurement error is no more than 1 %. The nature of non-metallic inclusions (microstructure, morphology and topography) was studied by the petrographic method using a complex methodology. Samples for research were cut from the metal of the experimental deposits in such a way that the fusion zone was located in the middle of the sample. Chemical etching of the metal with a 4% solution of sulfuric acid was carried out to identify the fusion zone. Results. As a result of the study of the chemical and mineralogical nature of non-metallic inclusions, it is shown that in the base metal (Ст.3 steel) when approaching the fusion zone, the number and size of non-metallic inclusions decrease, as well as their shape, microstructure and composition change. There are practically no non-metallic inclusions in the heating zone (immediately near the fusion zone). Scientific novelty. It is shown that the content of elements from the base metal to the deposited metal practically does not change, with the exception of chromium, the content of which gradually increases from Ст.3 steel to 12X13 steel in the fusion zone. Practical value. The results of the work make it possible to explain the effect of electroslag restoration of electric locomotive parts on the quality of the fusion zone and to explain the mechanism of structure defects and possible types of non-metallic inclusions as a result of surfacing.
目的。研究结果表明,有必要确定电渣堆焊过程中熔合区化学成分和非金属夹杂物的影响因素,并将其应用于铁路运输部件,即ЧС-4、ЧС-6、ЧС-8等品牌的电力机车的修复。 研究方法。采用德国卡尔蔡司公司的“SUPRA 40 WDS”扫描电镜和CAMECA x射线显微分析装置对非金属夹杂物的化学成分进行了研究。测量误差不大于1%。采用复杂的岩石学方法研究了非金属夹杂物的微观结构、形貌和形貌。用于研究的样品是从实验沉积物的金属中切割出来的,这种方式使得熔合区位于样品的中间。用4%的硫酸溶液对金属进行化学腐蚀以确定熔合区。 结果。对非金属包裹体的化学和矿物学性质进行了研究,结果表明,在母材中(Ст。当接近熔合区时,非金属夹杂物的数量和尺寸减少,形状、显微组织和成分发生变化。在加热区(紧挨着熔合区)几乎没有非金属夹杂物。科学的新奇。结果表明,除铬含量从Ст开始逐渐升高外,母材到镀层的各元素含量几乎没有变化。3钢到12X13钢的熔合区 实用价值。研究结果可以解释电渣修复对电机车零件熔合区质量的影响,并解释堆焊产生结构缺陷的机理和可能产生的非金属夹杂物类型。
{"title":"THE INFLUENCE ELECTROSLAG HARD-FACING ON THE CHEMICAL COMPOUND OF NONMETALLIC INCLUSIONS AND FUSION ZONE","authors":"Е. Parahnevich","doi":"10.15588/1607-6885-2023-3-6","DOIUrl":"https://doi.org/10.15588/1607-6885-2023-3-6","url":null,"abstract":"Purpose. As a result of the study, it is necessary to determine the factors that influence the chemical composition of the fusion zone and non-metallic inclusions during electroslag surfacing, which is used in the restoration of railway transport parts, namely electric locomotives of the ЧС-4, ЧС-6, ЧС-8, etc. brands. \u0000Research methods. The chemical composition of non-metallic inclusions was studied using the CAMECA X-ray spectroscopic microanalysis unit and the \"SUPRA 40 WDS\" scanning electron microscope manufactured by Carl Zeiss (Germany). The measurement error is no more than 1 %. The nature of non-metallic inclusions (microstructure, morphology and topography) was studied by the petrographic method using a complex methodology. Samples for research were cut from the metal of the experimental deposits in such a way that the fusion zone was located in the middle of the sample. Chemical etching of the metal with a 4% solution of sulfuric acid was carried out to identify the fusion zone. \u0000Results. As a result of the study of the chemical and mineralogical nature of non-metallic inclusions, it is shown that in the base metal (Ст.3 steel) when approaching the fusion zone, the number and size of non-metallic inclusions decrease, as well as their shape, microstructure and composition change. There are practically no non-metallic inclusions in the heating zone (immediately near the fusion zone). \u0000Scientific novelty. It is shown that the content of elements from the base metal to the deposited metal practically does not change, with the exception of chromium, the content of which gradually increases from Ст.3 steel to 12X13 steel in the fusion zone. \u0000Practical value. The results of the work make it possible to explain the effect of electroslag restoration of electric locomotive parts on the quality of the fusion zone and to explain the mechanism of structure defects and possible types of non-metallic inclusions as a result of surfacing.","PeriodicalId":489209,"journal":{"name":"Novì materìali ì tehnologìï v metalurgìï ta mašinobuduvannì","volume":"15 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136252946","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
IMPLEMENTATION OF MODERN NITRIDING TECHNOLOGIESTO IMPROVE WORKING CONDITIONS AND ENHANCE THE ENVIRONMENTAL FACILITIES FOR PROCESSES 实施现代氮化技术,改善工作条件,提高工艺设施的环境
Pub Date : 2023-10-11 DOI: 10.15588/1607-6885-2023-3-12
О. Nesterov, V. Ruban, V. Kuzmenko
IMPLEMENTATION OF MODERN NITRIDING TECHNOLOGIESTOIMPROVE WORKING CONDITIONS AND ENHANCE THE ENVIRONMENTAL FACILITIES FOR PROCESSES
实施现代氮化技术,改善工作条件,提高工艺环境设施
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引用次数: 0
THREE-DIMENSIONAL THERMAL CONDUCTIVITY PROBLEM FOR A MULTILAYER PLATE WITH IMPERFECT THERMAL CONTACT BETWEEN ITS LAYERS 多层板层间热接触不完全时的三维导热问题
Pub Date : 2023-10-11 DOI: 10.15588/1607-6885-2023-3-8
N. Antonenko, I. Tkachenko
Purpose. It consists in obtaining an analytical expression for calculating the temperature at the points of a multilayer plate under the condition of imperfect thermal contact between its layers, presenting obtained formulas in a for convenient for numerical implementation and investigating the influence of the thermal resistance coefficient on the temperature distribution in the plate layers. Research methods. To solve the given problem, the method of integral transformations (double integral Fourier transform) and the method of compliance functions were used. Results. In the form of improper Fourier integrals the formulas for calculating the temperature at any point of the multilayer plate were obtained. Numerical results for three-layer plates were conducted, on the outer surfaces of which a thermal load that uniformly distributed over the square (the intensity of the thermal loads on the lower boundary is ten times more than on the upper one) was given. The graphs that illustrate the influence of the thermal resistance coefficients on the temperature distribution at the points of the lower boundaries of the first and second layers were obtained. It was shown that the raise of the coefficients of thermal resistance leads to decreasing of the temperature at the points of these boundaries. The proposed method can be used to determine the temperature at the points of the plates with any finite number of layers. Scientific novelty. For the first time, the three-dimensional problem of thermal conductivity for the layered plate with imperfect thermal contact between its layers was solved by the method of compliance functions. Previously, only two-dimensional and axisymmetric problems of this type were solved by this method. Practical value. The obtained results can be used as the test ones when performing analogous calculations by other methods. Based on the results of numerical calculations in designing layered structures, it is possible to select their elements with the necessary thermal characteristics.
目的。其内容包括:在多层板层间不完全热接触的情况下,得到多层板各点温度的解析表达式,并以方便数值实现的形式给出所得公式,同时研究热阻系数对多层板层内温度分布的影响。 研究方法。为了解决给定的问题,使用了积分变换法(二重积分傅里叶变换)和柔度函数法。 结果。以反常傅里叶积分的形式,得到了多层板任意点温度的计算公式。对三层板的外表面进行了数值计算,得到了均匀分布在正方形上的热载荷(下边界的热载荷强度是上边界的十倍)。得到了热阻系数对第一层和第二层下边界点温度分布的影响曲线图。结果表明,热阻系数的增大会导致边界处温度的降低。所提出的方法可用于确定任意有限层数的板上各点的温度。科学的新奇。首次用柔度函数法求解了层间热接触不完全的层状板的三维导热系数问题。以前,这种方法只能解决这类二维和轴对称问题。 实用价值。所得结果可作为用其他方法进行类似计算时的试验结果。在层状结构设计中,根据数值计算结果,可以选择具有必要热特性的单元。
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 Research methods. To solve the given problem, the method of integral transformations (double integral Fourier transform) and the method of compliance functions were used.
 Results. In the form of improper Fourier integrals the formulas for calculating the temperature at any point of the multilayer plate were obtained. Numerical results for three-layer plates were conducted, on the outer surfaces of which a thermal load that uniformly distributed over the square (the intensity of the thermal loads on the lower boundary is ten times more than on the upper one) was given. The graphs that illustrate the influence of the thermal resistance coefficients on the temperature distribution at the points of the lower boundaries of the first and second layers were obtained. It was shown that the raise of the coefficients of thermal resistance leads to decreasing of the temperature at the points of these boundaries. The proposed method can be used to determine the temperature at the points of the plates with any finite number of layers.
 Scientific novelty. For the first time, the three-dimensional problem of thermal conductivity for the layered plate with imperfect thermal contact between its layers was solved by the method of compliance functions. Previously, only two-dimensional and axisymmetric problems of this type were solved by this method.
 Practical value. The obtained results can be used as the test ones when performing analogous calculations by other methods. Based on the results of numerical calculations in designing layered structures, it is possible to select their elements with the necessary thermal characteristics.","PeriodicalId":489209,"journal":{"name":"Novì materìali ì tehnologìï v metalurgìï ta mašinobuduvannì","volume":"40 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136253947","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
PHYSICAL-MECHANICAL CHARACTERISTICS AND THERMAL STRESS OF PLASMA COVERING 等离子体覆盖层的物理力学特性和热应力
Pub Date : 2023-10-11 DOI: 10.15588/1607-6885-2023-3-4
V. Greshta, A. Yershov, V. Hrabovskyi, V. Vinichenko, S. Seidametov
Purpose. It is based on the method of determining the physical and mechanical characteristics and cohesive strength of the plasma coating. Research methods. Experimental research methods of plasma coating specimens and mathematical methods of the theory of strength of materials. Received results. The study of the mechanical properties of the ПРНХ15СР2 plasma coating during the bending test was carried out. Values of forces and moments of elastic forces during bending depending on the deformation of the plasma coating sample was determined. The dependence of the destructive stress on the relative deformation of the coating was calculated. The modulus of elasticity and strength for the outer and inner surfaces of the coating are determined. Scientific novelty. It is shown that when determining the mechanical characteristics of the coating bonded to the base, a systematic error occurs due to the uncertainty of the internal stress in the coating. Therefore, for measurement, it is proposed to use samples peeled from the base, which are practically devoid of internal stress. For the inner surface of the coating, the modulus of elasticity and the destructive stress are rather higher than for the outer surface. The detected difference is associated with the presence of a temperature gradient during coating application and the distribution of residual stresses over the thickness of the coating. The gradient of residual thermal stresses and the maximum permissible temperature in the process of the coating deposition are determined. Practical value. The obtained results are of practical value for determining the conditions of guaranteed preservation of the integrity of the coating in the presence of residual stresses and calculating its maximum thickness on the base surface. It is shown that when the power of the plasmatron is reduced, the thermal stress gradient and the maximum stress on the coating surface decrease. Therefore, it is recommended to use a wire instead of a powder plasmatron, which twice reduces thermal stresses by half.
目的。它是基于测定等离子体涂层的物理机械特性和内聚强度的方法。 研究方法。等离子涂层试样的实验研究方法及材料强度理论的数学方法。收到结果。对ПРНХ15СР2等离子涂层在弯曲试验中的力学性能进行了研究。根据等离子体涂层试样的变形,确定了弯曲过程中弹性力和弹性矩的取值。计算了破坏应力与涂层相对变形的关系。确定涂层外表面和内表面的弹性模量和强度。 科学的新奇。结果表明,由于涂层内应力的不确定性,在测定与基体结合的涂层的力学特性时,会产生系统误差。因此,对于测量,建议使用从基底剥离的样品,这实际上是没有内应力的。涂层内表面的弹性模量和破坏应力均高于外表面。检测到的差异与涂层应用期间温度梯度的存在和涂层厚度上残余应力的分布有关。确定了涂层沉积过程中残余热应力梯度和最高允许温度。 实用价值。所得结果对于确定在残余应力存在的情况下保证涂层完整性的条件和计算其在基面上的最大厚度具有实用价值。结果表明,当等离子体功率降低时,涂层表面的热应力梯度和最大应力减小。因此,建议使用线材代替粉末等离子体,这样可以将热应力减少一半。
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 Research methods. Experimental research methods of plasma coating specimens and mathematical methods of the theory of strength of materials. Received results. The study of the mechanical properties of the ПРНХ15СР2 plasma coating during the bending test was carried out. Values of forces and moments of elastic forces during bending depending on the deformation of the plasma coating sample was determined. The dependence of the destructive stress on the relative deformation of the coating was calculated. The modulus of elasticity and strength for the outer and inner surfaces of the coating are determined.
 Scientific novelty. It is shown that when determining the mechanical characteristics of the coating bonded to the base, a systematic error occurs due to the uncertainty of the internal stress in the coating. Therefore, for measurement, it is proposed to use samples peeled from the base, which are practically devoid of internal stress. For the inner surface of the coating, the modulus of elasticity and the destructive stress are rather higher than for the outer surface. The detected difference is associated with the presence of a temperature gradient during coating application and the distribution of residual stresses over the thickness of the coating. The gradient of residual thermal stresses and the maximum permissible temperature in the process of the coating deposition are determined.
 Practical value. The obtained results are of practical value for determining the conditions of guaranteed preservation of the integrity of the coating in the presence of residual stresses and calculating its maximum thickness on the base surface. It is shown that when the power of the plasmatron is reduced, the thermal stress gradient and the maximum stress on the coating surface decrease. Therefore, it is recommended to use a wire instead of a powder plasmatron, which twice reduces thermal stresses by half.","PeriodicalId":489209,"journal":{"name":"Novì materìali ì tehnologìï v metalurgìï ta mašinobuduvannì","volume":"91 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136253777","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
DETERMINATION OF THE INFLUENCE OF THE MIXTURE OF GASES ON IMPROVING THE QUALITY OF CATHODES FOR ION-PLASMA SPUTTERING 混合气体对提高离子等离子溅射阴极质量影响的测定
Pub Date : 2023-10-11 DOI: 10.15588/1607-6885-2023-3-5
O. Omelchenko, N. Shaleva, V. Yefanov
Purpose. Improvement of the technological modes of smelting sputtering cathodes based on nickel of the Ni-Cr-Al-Y system in order to improve their quality, namely, to reduce the total number of defects in the form of discontinuities, pores, non-melts and increase the homogeneity of the structure and chemical composition and application of the protective atmosphere of inert gases, the most widespread of which are helium and argon. Research methods. The equipment was improved, in particular, the vacuum-arc installation was equipped with a ramp and a helium cylinder. Test samples in the form of “washers” (diameter 127 mm and thickness 40 mm) were obtained, which were used to study the microstructure and chemical composition. Remelting modes have been worked out. The study of the chemical composition was carried out using a multipurpose scanning electron microscope REM 106I, equipped with a microanalysis system. Results. Based on the results of studies of the influence of the gas mixture concentration on the structure and composition of the cathodes, technological modes of melting were established, which made it possible to improve the quality indicators and economic indicators of the investigated cathodes. This will have a positive effect on the number of cathode failures, the performance of coated parts and the life of aircraft engines in general. Scientific novelty. The dependence of the influence of the concentration of the mixture of gases (argon-helium) was determined, which made it possible to obtain the optimal ratio of protective gases. With a gas ratio of 70/30 %, the highest quality cathodes were obtained, which were used for further research. Practical value. Quality of coating sputtering is determined by regimes of sputtering and quality of cathode itself. One of applied methods is by-layered melting of cathodes in copper water-cooled crystallizer using electrodes that are melted or non-melted. Optimal ratio of protective gases for receiving qualitative cathodes is determined.
目的。改进Ni-Cr-Al-Y系镍基溅射阴极的冶炼工艺模式,以提高其质量,即减少不连续、气孔、不熔点等缺陷的总数,增加结构和化学成分的均匀性,并使用惰性气体保护气氛,其中最普遍的是氦气和氩气。 研究方法。对设备进行了改进,特别是在真空电弧装置上增加了斜坡和氦气瓶。制备了直径127 mm、厚度40 mm的“垫圈”试样,对其微观组织和化学成分进行了研究。计算出了重熔模式。化学成分的研究采用多用途扫描电子显微镜REM 106I,配备微量分析系统。 结果。根据混合气体浓度对阴极结构和成分影响的研究结果,建立了熔化阴极的工艺模式,使所研究阴极的质量指标和经济指标得以提高。这将对阴极失效次数、涂层部件的性能和航空发动机的寿命产生积极影响。 科学的新奇。确定了氩气-氦气混合气体浓度对其影响的依赖关系,从而可以获得最佳的保护气体比例。当气体比为70/ 30%时,得到的阴极质量最高,可用于进一步的研究。 实用价值。镀层溅射的质量是由溅射方式和阴极本身的质量决定的。一种应用的方法是在铜水冷结晶器中使用熔化或未熔化的电极分层熔化阴极。确定了接收定性阴极时保护气体的最佳配比。
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 Research methods. The equipment was improved, in particular, the vacuum-arc installation was equipped with a ramp and a helium cylinder. Test samples in the form of “washers” (diameter 127 mm and thickness 40 mm) were obtained, which were used to study the microstructure and chemical composition. Remelting modes have been worked out. The study of the chemical composition was carried out using a multipurpose scanning electron microscope REM 106I, equipped with a microanalysis system.
 Results. Based on the results of studies of the influence of the gas mixture concentration on the structure and composition of the cathodes, technological modes of melting were established, which made it possible to improve the quality indicators and economic indicators of the investigated cathodes. This will have a positive effect on the number of cathode failures, the performance of coated parts and the life of aircraft engines in general.
 Scientific novelty. The dependence of the influence of the concentration of the mixture of gases (argon-helium) was determined, which made it possible to obtain the optimal ratio of protective gases. With a gas ratio of 70/30 %, the highest quality cathodes were obtained, which were used for further research.
 Practical value. Quality of coating sputtering is determined by regimes of sputtering and quality of cathode itself. One of applied methods is by-layered melting of cathodes in copper water-cooled crystallizer using electrodes that are melted or non-melted. Optimal ratio of protective gases for receiving qualitative cathodes is determined.","PeriodicalId":489209,"journal":{"name":"Novì materìali ì tehnologìï v metalurgìï ta mašinobuduvannì","volume":"131 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136253129","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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Novì materìali ì tehnologìï v metalurgìï ta mašinobuduvannì
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