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An analysis of the bonding mechanisms active in a high power diode laser generated two-stage ceramic tile grout 高功率二极管激光产生的两段瓷砖灌浆的键合机制分析
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-10-18 DOI: 10.1080/0898150021000054566
J. Lawrence
It is quite possible to bring about changes in the wettability characteristics of a two-stage ceramic tile grout by means of high power diode laser (HPDL) surface treatment. Such changes manifest themselves as a reduction in the contact angle, Š , and are due to the HPDL inducing changes which reduce the surface roughness, increase the surface O 2 content and increasing the polar component of the surface energy. What is more, HPDL treatment of the two-stage ceramic tile grout surface was found to effect an improvement in the bonding characteristics by increasing the work of adhesion, W ad . Along with wettability experiments carried out with selected liquid-metals, an electronic approach was used to identify the bonding characteristics of the two-stage ceramic tile grout before and after HPDL. It is thought that HPDL induced changes to the two-stage ceramic tile grout produced a surface with a reduced bandgap energy which consequently increased W ad by increasing the electron transfer at the metal-oxide i...
高功率二极管激光(HPDL)表面处理有可能改变两段瓷砖灌浆的润湿性。这种变化表现为接触角的减小,这是由于HPDL诱导的变化降低了表面粗糙度,增加了表面o2含量,增加了表面能的极性成分。此外,发现HPDL处理两段瓷砖浆液表面通过增加粘接功来改善粘接特性。结合选定液体金属的润湿性实验,采用电子方法对两段瓷砖灌浆在HPDL前后的粘结特性进行了分析。认为HPDL引起的两段瓷砖浆液的变化产生了带隙能量降低的表面,从而通过增加金属氧化物处的电子转移而增加了wad。
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引用次数: 5
Zero point field (ZPF) effects in the interaction of the ultra-short laser pulses with matter 超短激光脉冲与物质相互作用中的零点场效应
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/0898150021000054557
M. Kozłowski, J. Marciak-kozlowska
In this article, the effects of zero-point energy (ZPE) on the heat transport induced by ultra-short laser pulses are investigated. It is shown that the existence of the zero-point energy in a physical vacuum influences the heat transport on an atomic level. The interaction of the building blocks of matter-atoms with the zero-point fields (ZPFs), which generate the ZPE guarantees the stability of matter. The interaction of the ultra-short laser pulses ( j t ¨ 1 as) with matter can be used as a source of information on the ZPF.
本文研究了零点能量(ZPE)对超短激光脉冲热输运的影响。证明了物理真空中零点能量的存在会影响原子水平上的热输运。物质的组成部分——原子与零点场(zero-point field, ZPE)的相互作用保证了物质的稳定性。超短激光脉冲与物质的相互作用可以作为ZPF的信息来源。
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引用次数: 1
Formation of embedded nanoparticles in an excimer laser treated Mg alloy surface 准分子激光处理镁合金表面中嵌入纳米颗粒的形成
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/08981500220151783
B. Majumdar, R. Galun, B. Mordike, A. Weisheit
The surface melting characteristics of AZ91 alloy is investigated using excimer laser (pulses of length 45 ns) under ambient conditions and also a N 2 environment. Experiments are carried out on overlapping spots with close interval. The melt layer hardness for treatment in air is increased to 162 VHN as compared to 73 VHN for the untreated alloy (AZ91 T4 condition), whereas the hardness of the sample treated in an N 2 atmosphere is 116 VHN. A transmission electron microscopy study reveals that the laser treated surface contains nanoparticles of oxide and nitride embedded in the submicron grains of the Mg solid solution. This is responsible for the observed high hardness which gives rise to the improved abrasive resistance. We propose a model to describe the formation of nanoparticles during the laser treatment.
利用准分子激光(脉冲长度为45 ns)研究了AZ91合金在常温和n2环境下的表面熔化特性。在间隔较近的重叠点上进行了实验。与未处理合金(AZ91 T4条件)的73 VHN相比,在空气中处理的熔体层硬度增加到162 VHN,而在n2气氛中处理的样品的硬度为116 VHN。透射电镜研究表明,激光处理后的表面含有氧化物和氮化物纳米颗粒,嵌入在Mg固溶体的亚微米颗粒中。这是观察到的高硬度的原因,从而提高了耐磨性。我们提出了一个模型来描述激光治疗过程中纳米颗粒的形成。
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引用次数: 2
CO 2 laser cutting of Incoloy 800 HT alloy and its quality assessment 铬合金800ht的co2激光切割及其质量评价
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/0898150021000014092
B. Yilbas, M. Rashid
In this article CO 2 laser cutting of Incoloy 800 HT alloy is studied. The dross ejected from the kerf is monitored and the frequency of dross ejection correlated with the striation frequency. SEM microphotography and measurement of the surface roughness of the cut edges are carried out. International standards for thermal cutting are used to assess the quality of the cut edges. A statistical analysis employing a factorial analysis is carried out to determine the significance levels of the cutting speed, laser output intensity, thickness, and the pulse frequency of the laser beam for the waviness, out of flatness, and overall quality of the cut edges. It is found that the dross ejection frequency is directly related to the striation frequency. The results of SEM microphotography, surface roughness measurement, and the optical method for the striation frequency monitoring are found to be in good agreement. The overall quality of the cut edge improves within a certain range of pulsing frequency, which is ca...
本文研究了铬合金800ht的co2激光切割。对割缝中出屑的情况进行了监测,并将出屑频率与条纹频率进行了相关分析。进行了扫描电镜显微摄影和切割边缘表面粗糙度的测量。热切割的国际标准被用来评估切割边缘的质量。采用因子分析进行统计分析,以确定切割速度、激光输出强度、厚度和激光束脉冲频率对切割边缘的波幅、不平整度和整体质量的显著性水平。结果表明,出渣频率与磨粒频率直接相关。扫描电镜显微摄影、表面粗糙度测量和条纹频率监测的光学方法的结果是一致的。在一定的脉冲频率范围内,切割边缘的整体质量得到改善。
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引用次数: 15
A mathematical model to predict the thermal history and microstructure developed in laser surface alloying 建立了一种预测激光表面合金化热过程和微观组织的数学模型
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/0898150021000039284
J. Majumdar, I. Manna
Laser surface alloying involves tailoring the surface microstructure and composition by rapid melting, intermixing and solidification of a pre/co-deposited surface layer with a part of the underlying substrate. It is a potential method of enhancing hardness and wear resistance of engineering components. In the present study, a one-dimensional heat transfer model based on the explicit finite difference method has been developed to predict the thermal history (i.e., temperature profile, thermal gradient, cooling rate and solid-liquid interface velocity) and hence, the microstructure of the alloyed zone developed by laser surface alloying. The incident laser power and laser-matter interaction time are chosen as the main variables to study the effect of laser parameters on thermal history, and consequently, microstructure of the alloyed zone. The numerical calculations have been carried out for the model system of AISI 304 stainless steel laser surface alloyed with pre-deposited molybdenum. The predicted resu...
激光表面合金化包括通过快速熔化、混合和凝固预先/共沉积的表面层与底层基底的一部分来调整表面微观结构和组成。它是提高工程部件硬度和耐磨性的一种有潜力的方法。在本研究中,基于显式有限差分法建立了一维传热模型,用于预测激光表面合金化合金区的热历史(即温度分布、热梯度、冷却速率和固液界面速度),从而预测激光表面合金化合金区的微观组织。以入射激光功率和激光-物质相互作用时间为主要变量,研究了激光参数对合金区热历史的影响,进而对合金区的显微组织进行了研究。对aisi304不锈钢激光表面预镀钼合金模型系统进行了数值计算。预测的结果……
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引用次数: 9
On the differences between the beam interaction characteristics of CO 2, Nd:YAG, excimer and high power diode lasers with a SiO 2/Al 2O 3 ceramic 基于sio2 / al2o3陶瓷的CO 2、Nd:YAG、准分子和高功率二极管激光器光束相互作用特性的差异
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/08981500220151756
J. Lawrence, Lin Li
By using a number of techniques and approaches certain differences between the beam interaction characteristics of CO 2 laser, a Nd:YAG laser, a high power diode laser (HPDL) and an excimer laser with a SiO 2 /Al 2 O 3 ceramic have been investigated. By employing a derivative of Beer-Lambert's law, the laser beam absorption lengths of the four lasers were calculated as 470 - 22 µm for the CO 2 laser, 195 - 12 µm for the Nd:YAG laser, 177 - 15 µm for the HPDL and 7.5 - 19 µm for the excimer laser. The fluence threshold values at which significant material removal occurs the CO 2 laser, Nd:YAG laser, HPDL and excimer laser were found to be 68, 128, 181 and 0.12 J cm m 2 , respectively. Absorptivity measurements revealed that there is no correlation between the actual absorptivity of the SiO 2 /Al 2 O 3 ceramic and the absorption length for each of the four lasers. The thermal loading values for the CO 2 laser, the, Nd:YAG laser, the HPDL and the excimer laser were determined as 2.57, 6.73, 9.83 and 22.24 kJ...
采用多种技术和方法研究了CO 2激光器、Nd:YAG激光器、高功率二极管激光器(HPDL)和带有sio2 / al2o3陶瓷的准分子激光器的光束相互作用特性的差异。利用Beer-Lambert定律的导数,计算出4种激光器的光束吸收长度分别为:co2激光器470 ~ 22µm, Nd:YAG激光器195 ~ 12µm, HPDL激光器177 ~ 15µm,准分子激光器7.5 ~ 19µm。CO 2激光、Nd:YAG激光、HPDL激光和准分子激光的能量阈值分别为68、128、181和0.12 J cm m2。吸收率测量结果表明,sio2 / al2o3陶瓷的实际吸收率与四种激光器的吸收长度之间没有相关性。co2激光器、Nd:YAG激光器、HPDL激光器和准分子激光器的热载荷值分别为2.57、6.73、9.83和22.24 kJ。
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引用次数: 8
Method to evaluate residual stresses in the laser cutting process 激光切割过程中残余应力的评估方法
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/08981500290022752
Y. Zamachtchikov, F. Breabăn, P. Vantomme, A. Deffontaine
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引用次数: 7
A novel technique for micro profiling of slots 一种新的狭槽微轮廓技术
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/08981500290022761
N. Sivakumar, K. Venkatakrishnan, B. Ngoi
With the growing importance of micro machining, it has become important to characterise the profile of slot surfaces in order to understand the machining process in detail. In this paper, a novel optical layout adapting the concept of Mirau interferometry to polarization optics, in combination with instantaneous phase shifting interferometry, for measurement of slot surfaces is described. Experiments were carried out with this setup on a wafer surface with slot and the results were compared with that of a commercial surface profiler to demonstrate the applicability of the principle. The results obtained, were discussed with reference to the beam spot size, positioning of the object and the vertical resolution of the measurement setup, and compared with that of the commercial surface profiler.
随着微加工的日益重要,为了详细地了解加工过程,表征槽面轮廓变得非常重要。本文介绍了一种将Mirau干涉法的概念应用于偏振光学,结合瞬时移相干涉法测量狭缝表面的新型光学布局。利用该装置在带槽的晶圆表面上进行了实验,并与商用表面轮廓仪的结果进行了比较,以验证该原理的适用性。本文从光斑尺寸、目标定位和测量装置的垂直分辨率等方面对所得到的结果进行了讨论,并与商用表面轮廓仪的测量结果进行了比较。
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引用次数: 3
Microstructural characterisation of a dissimilar weld of alloy D9 and AISI 316M stainless steel produced using a 2.5 kW CW CO 2 laser 用2.5 kW连续co2激光对D9合金与AISI 316M不锈钢异种焊缝进行显微组织表征
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/0898150021000014083
R. Kaul, P. Ganesh, M. O. Ittoop, A. Nath, Aniruddha Kumar, R. Bhatt, Arun Kumar
The dissimilar weld, a fuel clad tube (D9 alloy) and an end plug made of AISI 316M forms a part of the fuel pin in the 500 MW Indian Prototype Fast Breeder Reactor (PFBR). The present study aimed at the development of a crack resistant microstructure of the dissimilar weld by optimisation of 2.5 kW CO 2 laser welding parameters. The D9 alloy, because of its low Cr eq /Ni eq ratio (close to 1), solidified first as primary austenite which makes its welds particularly susceptible to solidification cracking. In this study, the primary mode of solidification in the fusion zone was modulated by controlling the relative degree of fusion of the fuel clad tube and the end plug. A defect free weld with predominantly a primary ferrite mode of solidification was obtained by optimising laser parameters and displacing the focused laser beam towards the end plug side to achieve a greater contribution of end plug material to the fusion zone. The formation of a crater and associated defects at the termination site of lase...
在500兆瓦的印度原型快速增殖反应堆(PFBR)中,不同的焊缝、燃料包层管(D9合金)和由AISI 316M制成的端塞构成了燃料销的一部分。本研究旨在通过优化2.5 kW co2激光焊接参数,建立异种焊缝的抗裂纹组织。D9合金由于其较低的Cr当量/Ni当量比(接近1),首先凝固为初生奥氏体,这使得其焊缝特别容易凝固开裂。在本研究中,通过控制燃料包壳管和端塞的相对熔合度来调节熔合区的初级凝固模式。通过优化激光参数,将聚焦激光束向端塞侧偏移,使端塞材料对熔合区的贡献更大,获得了以初级铁氧体凝固模式为主的无缺陷焊缝。在激光终止处形成一个陨石坑和伴随的缺陷。
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引用次数: 6
Laser surface alloying of an Mg alloy with Al + Mn to improve corrosion resistance 用Al + Mn激光表面合金化镁合金以提高其耐蚀性
IF 0.5 4区 工程技术 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2002-01-01 DOI: 10.1080/0898150021000039275
J. Majumdar, T. Maiwald, R. Galun, B. Mordike, I. Manna
In the present study, an attempt has been made to enhance the corrosion resistance of a Mg alloy (MEZ) by laser surface alloying with Al + Mn. Laser surface alloying has been carried out with a 10 kW continuous wave CO 2 laser by melting and simultaneous feeding of a powder mixture of Al and Mn in the ratio of 3 : 1 and 1 : 3, respectively. Following laser irradiation, the alloyed zone has been characterized by a detailed microstructural observation and phase analysis. Moreover, the properties of the surface alloyed layer like microhardness and corrosion have been evaluated in detail. The surface modified layer predominantly consists of dendrites of Al + Mn and Al + Mg. The microhardness of the alloyed zone has been significantly enhanced to as high as 250-350 VHN as compared to 35 VHN of the substrate region. The corrosion rate in a 3.56 wt.% NaCl solution has significantly reduced to 250 mpy for laser surface alloyed specimen as compared to 1520 mpy of the MEZ substrate. The enhanced corrosion resistanc...
本研究尝试用Al + Mn激光表面合金化的方法提高镁合金(MEZ)的耐蚀性。采用10 kW连续波co2激光器,分别以3:1和1:3的比例熔化和同时进料Al和Mn的混合粉末,进行了激光表面合金化。激光辐照后,对合金区进行了详细的显微组织观察和物相分析。此外,还详细评价了表面合金层的显微硬度和腐蚀性能。表面改性层主要由Al + Mn和Al + Mg枝晶组成。合金区的显微硬度从基体区的35 VHN显著提高到250-350 VHN。在3.56 wt.% NaCl溶液中,激光表面合金试样的腐蚀速率从MEZ基体的1520 mpy显著降低至250 mpy。增强的耐蚀性…
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引用次数: 26
期刊
Lasers in Engineering
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