Pub Date : 2019-01-02DOI: 10.1080/0889311X.2018.1538214
H. Maynard-Casely
{"title":"Review of ‘the effective scientist, a handy guide to a successful academic career’","authors":"H. Maynard-Casely","doi":"10.1080/0889311X.2018.1538214","DOIUrl":"https://doi.org/10.1080/0889311X.2018.1538214","url":null,"abstract":"","PeriodicalId":54385,"journal":{"name":"Crystallography Reviews","volume":"25 1","pages":"78 - 79"},"PeriodicalIF":3.0,"publicationDate":"2019-01-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/0889311X.2018.1538214","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46259855","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-01-02DOI: 10.1080/0889311X.2019.1574289
P. Bombicz
{"title":"How to achieve the best possible diffraction data? Editorial for Crystallography Reviews, Issue 1 of 2019","authors":"P. Bombicz","doi":"10.1080/0889311X.2019.1574289","DOIUrl":"https://doi.org/10.1080/0889311X.2019.1574289","url":null,"abstract":"","PeriodicalId":54385,"journal":{"name":"Crystallography Reviews","volume":"25 1","pages":"1 - 2"},"PeriodicalIF":3.0,"publicationDate":"2019-01-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/0889311X.2019.1574289","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46339655","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2019-01-02DOI: 10.1080/0889311X.2019.1569643
A. Thompson
Abstract There is an increasing trend to reduce diffraction data collection to a set of numbers and the crystallography to a set of criteria. Many of these criteria have been passed on through generations of crystallographers. In Chemical Crystallography, the majority of small-molecule singe crystal diffraction data are still collected using laboratory equipment. Herein we review the methods for analysing data, discuss some of the influences on data quality and try to determine whether some of the validation tropes widely used are sound advice, or ‘Chinese Whispers’.
{"title":"Chemical Crystallography: when are ‘ bad data’ ‘good data’?","authors":"A. Thompson","doi":"10.1080/0889311X.2019.1569643","DOIUrl":"https://doi.org/10.1080/0889311X.2019.1569643","url":null,"abstract":"Abstract There is an increasing trend to reduce diffraction data collection to a set of numbers and the crystallography to a set of criteria. Many of these criteria have been passed on through generations of crystallographers. In Chemical Crystallography, the majority of small-molecule singe crystal diffraction data are still collected using laboratory equipment. Herein we review the methods for analysing data, discuss some of the influences on data quality and try to determine whether some of the validation tropes widely used are sound advice, or ‘Chinese Whispers’.","PeriodicalId":54385,"journal":{"name":"Crystallography Reviews","volume":"25 1","pages":"3 - 53"},"PeriodicalIF":3.0,"publicationDate":"2019-01-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/0889311X.2019.1569643","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41849243","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-12-11DOI: 10.1080/0889311X.2018.1553165
O. Mikhailov
Abstract The data have been systematized and generalized on the specific synthesis of elemental silver nano-sized crystals (Ag-NC) having the forms of various geometric bodies (pseudo spherical, prismatic, cubic, trigonal-pyramidal, etc.), obtained by various chemical, physicochemical and biological methods. It has been noted, that the form of the synthesized Ag-NC can be controlled by changing the thermodynamic and kinetic parameters at each key stage of the synthesis (nucleation, seeding, and growth). Moreover, the size range of spherical and cubic silver nanocrystals can be influenced by either physical, chemical or biological methods during the synthesis, but such forms as nanorods, nanowires and nanobars can only be synthesized by chemical or physical methods at the present time. The review covers articles comprehensively mainly published in the last 20 years.
{"title":"Elemental silver nano-sized crystals: various geometric forms and their specific growth parameters","authors":"O. Mikhailov","doi":"10.1080/0889311X.2018.1553165","DOIUrl":"https://doi.org/10.1080/0889311X.2018.1553165","url":null,"abstract":"Abstract The data have been systematized and generalized on the specific synthesis of elemental silver nano-sized crystals (Ag-NC) having the forms of various geometric bodies (pseudo spherical, prismatic, cubic, trigonal-pyramidal, etc.), obtained by various chemical, physicochemical and biological methods. It has been noted, that the form of the synthesized Ag-NC can be controlled by changing the thermodynamic and kinetic parameters at each key stage of the synthesis (nucleation, seeding, and growth). Moreover, the size range of spherical and cubic silver nanocrystals can be influenced by either physical, chemical or biological methods during the synthesis, but such forms as nanorods, nanowires and nanobars can only be synthesized by chemical or physical methods at the present time. The review covers articles comprehensively mainly published in the last 20 years.","PeriodicalId":54385,"journal":{"name":"Crystallography Reviews","volume":"25 1","pages":"54 - 75"},"PeriodicalIF":3.0,"publicationDate":"2018-12-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/0889311X.2018.1553165","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"45005794","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-11-22DOI: 10.1080/0889311X.2018.1547898
A. Liljas
Most scientists spend their life focusing on a limited number of topics and at a limited number of academic institutions. This is not the case for Venki Ramakrishnan as he describes in his memoirs....
{"title":"Gene machine. The race to decipher the secrets of the ribosome","authors":"A. Liljas","doi":"10.1080/0889311X.2018.1547898","DOIUrl":"https://doi.org/10.1080/0889311X.2018.1547898","url":null,"abstract":"Most scientists spend their life focusing on a limited number of topics and at a limited number of academic institutions. This is not the case for Venki Ramakrishnan as he describes in his memoirs....","PeriodicalId":54385,"journal":{"name":"Crystallography Reviews","volume":"25 1","pages":"76 - 77"},"PeriodicalIF":3.0,"publicationDate":"2018-11-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/0889311X.2018.1547898","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"49653151","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-10-02DOI: 10.1080/0889311X.2018.1526173
J. Helliwell
[1] Lytle FW. The EXAFS family tree: a personal history of the development of x-ray absorption fine structure. J Synchrotron Rad. 1999;6:123–134. [2] Binsted N, Pack MJ, Teller MT, Evans J. Combined EXAFS and powder diffraction analysis. J Am Chem Soc. 1996;118:11200–11210. [3] Chantler CT, Bunker BA, Abe H, Kimura M, Newville M, Welter E. A call for a round robin study of XAFS stability and platform dependence at synchrotron beamlines on well defined samples. J Synchrotron Rad. 2018;25(4):935–943. [4] Filipponi A, Di Cicco A. Atomic background in x-ray absorption spectra of fifth-period elements: evidence for double-electron excitation edges. Phys Rev A. 1995;52:1072–1078. [5] Jolliffe IT. Principal component analysis. New York: Springer-Verlag; 2002. [6] Parsons AD, Price SWT, Wadeson N, Basham M, Beale AM, Ashton AW, Mosselmans JFW, Quinn PD. Automatic processing of multimodal tomography datasets. J Synchrotron Radiat. 2017;24:248–256. [7] Rehr JJ, Albers RC. Theoretical approaches to x-ray absorption fine structure. Rev Mod Phys. 2000;72:621–654.
{"title":"X-ray nanochemistry concepts and development","authors":"J. Helliwell","doi":"10.1080/0889311X.2018.1526173","DOIUrl":"https://doi.org/10.1080/0889311X.2018.1526173","url":null,"abstract":"[1] Lytle FW. The EXAFS family tree: a personal history of the development of x-ray absorption fine structure. J Synchrotron Rad. 1999;6:123–134. [2] Binsted N, Pack MJ, Teller MT, Evans J. Combined EXAFS and powder diffraction analysis. J Am Chem Soc. 1996;118:11200–11210. [3] Chantler CT, Bunker BA, Abe H, Kimura M, Newville M, Welter E. A call for a round robin study of XAFS stability and platform dependence at synchrotron beamlines on well defined samples. J Synchrotron Rad. 2018;25(4):935–943. [4] Filipponi A, Di Cicco A. Atomic background in x-ray absorption spectra of fifth-period elements: evidence for double-electron excitation edges. Phys Rev A. 1995;52:1072–1078. [5] Jolliffe IT. Principal component analysis. New York: Springer-Verlag; 2002. [6] Parsons AD, Price SWT, Wadeson N, Basham M, Beale AM, Ashton AW, Mosselmans JFW, Quinn PD. Automatic processing of multimodal tomography datasets. J Synchrotron Radiat. 2017;24:248–256. [7] Rehr JJ, Albers RC. Theoretical approaches to x-ray absorption fine structure. Rev Mod Phys. 2000;72:621–654.","PeriodicalId":54385,"journal":{"name":"Crystallography Reviews","volume":"24 1","pages":"276 - 280"},"PeriodicalIF":3.0,"publicationDate":"2018-10-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/0889311X.2018.1526173","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"42542810","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-10-02DOI: 10.1080/0889311X.2018.1510815
P. Bombicz
{"title":"How to produce good data and how to check the quality of the data? Editorial for crystallography reviews, issue 4 of 2018","authors":"P. Bombicz","doi":"10.1080/0889311X.2018.1510815","DOIUrl":"https://doi.org/10.1080/0889311X.2018.1510815","url":null,"abstract":"","PeriodicalId":54385,"journal":{"name":"Crystallography Reviews","volume":"24 1","pages":"215 - 216"},"PeriodicalIF":3.0,"publicationDate":"2018-10-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/0889311X.2018.1510815","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48779475","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-09-12DOI: 10.1080/0889311X.2018.1518976
G. García
{"title":"X-ray absorption spectroscopy for the Chemical and Materials sciences","authors":"G. García","doi":"10.1080/0889311X.2018.1518976","DOIUrl":"https://doi.org/10.1080/0889311X.2018.1518976","url":null,"abstract":"","PeriodicalId":54385,"journal":{"name":"Crystallography Reviews","volume":"24 1","pages":"273 - 276"},"PeriodicalIF":3.0,"publicationDate":"2018-09-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/0889311X.2018.1518976","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48741785","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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