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Understanding the spatial interaction of ultrasounds based on three-dimensional dual-frequency ultrasonic field numerical simulation 基于三维双频超声场数值模拟的超声空间相互作用研究
3区 材料科学 Q2 Materials Science Pub Date : 2023-09-28 DOI: 10.1007/s41230-023-3042-1
Zhao-yang Yin, Qi-chi Le, Yan-chao Jiang, Da-zhi Zhao, Qi-yu Liao, Qi Zou
A transient 3D model was established to investigate the effect of spatial interaction of ultrasounds on the dual-frequency ultrasonic field in magnesium alloy melt. The effects of insertion depth and tip shape of the ultrasonic rods, input pressures and their ratio on the acoustic field distribution were discussed in detail. Additionally, the spacing, angle, and insertion depth of two ultrasonic rods significantly affect the interaction between distinct ultrasounds. As a result, various acoustic pressure distributions and cavitation regions are obtained. The spherical rods mitigate the longitudinal and transversal attenuation of acoustic pressure and expand the cavitation volume by 53.7% and 31.7%, respectively, compared to the plate and conical rods. Increasing the input pressure will enlarge the cavitation region but has no effect on the acoustic pressure distribution pattern. The acoustic pressure ratio significantly affects the pressure distribution and the cavitation region, and the best cavitation effect is obtained at the ratio of 2:1 (P15:P20).
建立了瞬态三维模型,研究了超声空间相互作用对镁合金熔体中双频超声场的影响。详细讨论了超声棒插入深度、尖端形状、输入压力及其比值对声场分布的影响。此外,两根超声棒的间距、角度和插入深度对不同超声之间的相互作用有显著影响。得到了不同的声压分布和空化区域。与板形杆和锥形杆相比,球形杆可减轻纵向和横向声压衰减,空化体积扩大幅度分别为53.7%和31.7%。增加输入压力会扩大空化区域,但对声压分布模式没有影响。声压比对压力分布和空化区域影响显著,当声压比为2:1 (P15:P20)时,空化效果最佳。
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引用次数: 0
Effect of slow shot speed on externally solidified crystal, porosity and tensile property in a newly developed high-pressure die-cast Al-Si alloy 慢射速对新研制的高压压铸铝硅合金外凝固结晶、孔隙率和拉伸性能的影响
3区 材料科学 Q2 Materials Science Pub Date : 2023-09-09 DOI: 10.1007/s41230-023-3037-y
Wen-ning Liu, Wei Zhang, Peng-yue Wang, Yi-xian Liu, Xiang-yi Jiao, Ao-xiang Wan, Cheng-gang Wang, Guo-dong Tong, Shou-mei Xiong
The effect of slow shot speed on externally solidified crystal (ESC), porosity and tensile property in a newly developed high-pressure die-cast Al-Si alloy was investigated by optical microscopy (OM), scanning electron microscopy (SEM) and laboratory computed tomography (CT). Results showed that the newly developed AlSi9MnMoV alloy exhibited improved mechanical properties when compared to the AlSi10MnMg alloy. The AlSi9MnMoV alloy, which was designed with trace multicomponent additions, displays a notable grain refining effect in comparison to the AlSi10MnMg alloy. Refining elements Ti, Zr, V, Nb, B promote heterogeneous nucleation and reduce the grain size of primary α-Al. At a lower slow shot speed, the large ESCs are easier to form and gather, developing into the dendrite net and net-shrinkage. With an increase in slow shot speed, the size and number of ESCs and porosities significantly reduce. In addition, the distribution of ESCs is more dispersed and the net-shrinkage disappears. The tensile property is greatly improved by adopting a higher slow shot speed. The ultimate tensile strength is enhanced from 260.31 MPa to 290.31 MPa (increased by 11.52%), and the elongation is enhanced from 3.72% to 6.34% (increased by 70.52%).
采用光学显微镜(OM)、扫描电镜(SEM)和实验室计算机断层扫描(CT)研究了慢射速对一种新研制的高压压铸铝硅合金外凝固结晶(ESC)、孔隙率和拉伸性能的影响。结果表明,与AlSi10MnMg合金相比,新制备的AlSi9MnMoV合金具有更好的力学性能。与AlSi10MnMg合金相比,添加微量多组分的AlSi9MnMoV合金表现出明显的晶粒细化效果。细化元素Ti、Zr、V、Nb、B促进初生α-Al非均相形核,减小晶粒尺寸。在较低的慢射速度下,较大的ESCs更容易形成和聚集,发展成枝晶网和净缩孔。随着慢射速度的增加,ESCs的尺寸和数量以及孔隙率显著降低。此外,ESCs分布更加分散,净收缩消失。采用较高的慢射速度,大大提高了拉伸性能。拉伸强度由260.31 MPa提高到290.31 MPa(提高11.52%),延伸率由3.72%提高到6.34%(提高70.52%)。
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引用次数: 0
Corrosion and wear properties of in situ (TiB+TiC)/TA15 composites with a high volume percentage of reinforcement 高体积百分比增强的原位(TiB+TiC)/TA15复合材料的腐蚀磨损性能
3区 材料科学 Q2 Materials Science Pub Date : 2023-09-01 DOI: 10.1007/s41230-023-2185-4
Wei-long Wang, Kun Shi, Jun Zhao, Shi-bing Liu, Jiao-jiao Cheng, Wei-chen Qiu, Tian-yu Liu, Zhi-yong Zhang
The in situ (TiC+TiB)/TA15 composites with different volume percentages of reinforcement (10%, 15%, 20% and 25%) were prepared by water-cooled copper crucible vacuum suspension melting technology. The structures and compositions of the TA15 alloy and its composites were analyzed by XRD and EDS, and their electrochemical corrosion behavior in the 3.5% NaCl solution was studied. Corrosion wear testing was conducted using a reciprocating ball-on-disc wear tester under a 10 N load. Results show that the in situ fibrous TiB phase and the granular TiC phase are uniformly distributed on the composite matrix. The microhardness can reach up to 531 HV as 10vol.% TiC+TiB reinforcement is added. Compared with the TA15 alloy, the volume wear rate decreases from (2.21±0.07)×10−4 to (1.75±0.07)×10−4 mm3·N−1·m−1 by adding 15vol.% TiC+TiB reinforcement, and the wear mechanism is adhesive wear. When the volume percentage of the reinforcement phase reaches 25%, the volume wear rate increases from (1.75±0.07)×10−4 to (2.41±0.07)·10−4 mm3·N−1·m−1, and the wear mechanism changes into abrasive wear. The volume loss resulted by the interaction between corrosion and wear accounts for more than 27% of the total wear volume. The volume loss due to wear-induced corrosion changes from 1.94% to 4.06% with different addition of reinforcement. The volume loss caused by corrosion-induced wear initially increases from 24.08% to 26.90% as the reinforcement increases from 0 to 15% due to the increase of corrosion potential, and then decreases from 26.90% to 25.68% as the reinforcement increases from 15% to 25% due to the peeling of TiC phase.
采用水冷铜坩埚真空悬浮熔炼技术制备了不同体积增强率(10%、15%、20%和25%)的原位(TiC+TiB)/TA15复合材料。采用XRD和EDS分析了TA15合金及其复合材料的结构和成分,并研究了其在3.5% NaCl溶液中的电化学腐蚀行为。在10 N载荷下,使用往复式球盘式磨损试验机进行腐蚀磨损测试。结果表明:原位纤维状TiB相和颗粒状TiC相在复合基体上均匀分布;10vol时显微硬度可达531 HV。添加了% TiC+TiB增强。与TA15合金相比,加入15vol后,体积磨损率由(2.21±0.07)×10−4降低至(1.75±0.07)×10−4 mm3·N−1·m−1。% TiC+TiB增强,磨损机制为粘着磨损。当增强相体积百分比达到25%时,体积磨损率由(1.75±0.07)×10−4增加到(2.41±0.07)·10−4 mm3·N−1·m−1,磨损机制转变为磨粒磨损。腐蚀和磨损相互作用造成的体积损失占总磨损体积的27%以上。添加不同的补强剂,磨损腐蚀的体积损失从1.94%增加到4.06%。由于腐蚀电位的增加,当增强量从0增加到15%时,腐蚀磨损引起的体积损失从24.08%增加到26.90%,当增强量从15%增加到25%时,由于TiC相的剥落,腐蚀磨损引起的体积损失从26.90%降低到25.68%。
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引用次数: 0
Simulation of inclined dendrites under natural convection by KKS phase field model based on CUDA 基于CUDA的KKS相场模型对自然对流条件下倾斜枝晶的模拟
3区 材料科学 Q2 Materials Science Pub Date : 2023-09-01 DOI: 10.1007/s41230-023-2128-0
Chang-sheng Zhu, Tian-yu Li, Bo-rui Zhao, Cang-long Wang, Zi-hao Gao
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引用次数: 1
Elastic-viscoplastic constitutive equations of K439B superalloy and thermal stress simulation during casting process K439B高温合金弹粘塑性本构方程及铸造过程热应力模拟
3区 材料科学 Q2 Materials Science Pub Date : 2023-09-01 DOI: 10.1007/s41230-023-2119-1
Da-shan Sui, Yu Shan, Dong-xin Wang, Jun-yi Li, Yao Xie, Yi-qun Yang, An-ping Dong, Bao-de Sun
K439B nickel-based superalloy is a new type of high-temperature material. There is insufficient research on its constitutive equations and numerical modeling of thermal stress. Isothermal tensile experiments of K439B superalloy at different temperatures (20 °C–1,000 °C) and strain rates (1.33×10−3 s−1–5.33×10−3 s−1) were performed by using a Gleeble-3800 simulator. The elastic moduli at different temperatures (20 °C–650 °C) were measured by resonance method. Subsequently, stress-strain curves were measured for K439B superalloy under different conditions. The elastic-viscoplastic constitutive equations were established and the correspongding parameters were solved by employing the Perzyna model. The verification results indicate that the calculated values of the constitutive equations are in good agreement with the experimental values. On this basis, the influence of process parameters on thermal stress was investigated by numerical simulation and orthogonal experimental design. The results of orthogonal experimental design reveal that the cooling mode of casting has a significant influence on the thermal stress, while pouring temperature and preheating temperature of shell mold have minimal impact. The distribution of physical fields under optimal process parameters, determined based on the orthogonal experimental design results, was simulated. The simulation results determine separately the specific positions with maximum values for effective stress, plastic strain, and displacement within the casting. The maximum stress is about 1,000.0 MPa, the plastic strain is about 0.135, and the displacement is about 1.47 mm. Moreover, the distribution states of thermal stress, strain, and displacement are closely related to the distribution of the temperature gradient and cooling rate in the casting. The research would provide a theoretical reference for exploring the stress-strain behavior and numerical modeling of the effective stress of the alloy during the casting process.
K439B镍基高温合金是一种新型高温材料。目前对其本构方程和热应力数值模拟研究不足。采用Gleeble-3800模拟装置,对K439B高温合金在不同温度(20°C - 1000°C)和应变速率(1.33×10−3 s−1-5.33×10−3 s−1)下的等温拉伸实验进行了研究。用共振法测量了不同温度(20℃~ 650℃)下的弹性模量。随后,测量了不同条件下K439B高温合金的应力-应变曲线。采用Perzyna模型建立了弹粘塑性本构方程,并求解了相应的参数。验证结果表明,本构方程计算值与实验值吻合较好。在此基础上,通过数值模拟和正交试验设计研究了工艺参数对热应力的影响。正交试验设计结果表明,铸件冷却方式对热应力影响显著,浇注温度和壳型预热温度对热应力影响最小。在正交试验设计结果的基础上,对最佳工艺参数下的物理场分布进行了模拟。模拟结果分别确定了铸件内有效应力、塑性应变和位移的最大值的具体位置。最大应力约为10000.0 MPa,塑性应变约为0.135,位移约为1.47 mm。此外,热应力、应变和位移的分布状态与铸件内温度梯度和冷却速率的分布密切相关。该研究可为探索铸造过程中合金的应力-应变行为及有效应力的数值模拟提供理论参考。
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引用次数: 0
Effect of electromagnetic stirrer centered outside the mold on steel flow field of bloom continuous casting 以模外为中心的电磁搅拌器对连铸坯流场的影响
3区 材料科学 Q2 Materials Science Pub Date : 2023-09-01 DOI: 10.1007/s41230-023-2155-x
Li-dong Xing, Yan-ping Bao, Min Wang, Yi-hong Li
Mold electromagnetic stirring technology for optimizing the flow of molten steel is now widely used in the continuous casting production process of high-quality steels. However, studies on the case that the center of the electromagnetic stirrer is located outside the mold have not been reported. Herein, the effect of the electromagnetic stirrer centered outside the mold on the steel flow field was studied in detail by means of numerical simulations. A Gauss meter was used to measure the magnetic induction intensity at different positions, currents, and frequencies. The test results were compared with the simulation results of electromagnetic stirring to calibrate and verify the accuracy of the electromagnetic model. Then, electromagnetic force was introduced into the flow field model as a source term to study its effect on the flow field under anomalous conditions. The results show that when the center of the electromagnetic stirrer is located outside the mold, the magnetic field strength is about twice as strong as that located inside the mold. This also leads to an increase in the flow velocity near the electromagnetic stirrer. As a result, the optimal electromagnetic stirring parameters (200 A, 2.5 Hz) were specified when the center of the electromagnetic stirrer is located outside the mold.
优化钢水流动的结晶器电磁搅拌技术目前已广泛应用于优质钢的连铸生产过程中。然而,关于电磁搅拌器中心位于模具外的情况的研究尚未见报道。本文采用数值模拟的方法,详细研究了以模外为中心的电磁搅拌器对钢流场的影响。用高斯计测量了不同位置、电流和频率下的磁感应强度。将试验结果与电磁搅拌仿真结果进行对比,对电磁模型的准确性进行校正和验证。然后,将电磁力作为源项引入流场模型,研究了电磁力在异常条件下对流场的影响。结果表明,当电磁搅拌器中心位于模外时,其磁场强度约为模内磁场强度的两倍。这也导致在电磁搅拌器附近的流速增加。结果表明,当电磁搅拌器中心位于模具外时,确定了最佳的电磁搅拌参数(200a, 2.5 Hz)。
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引用次数: 0
Effect of sintering temperature on microstructure and properties of 3D printing polysilazane reinforced Al2O3 core 烧结温度对3D打印聚硅氮烷增强Al2O3芯材微观结构和性能的影响
3区 材料科学 Q2 Materials Science Pub Date : 2023-08-18 DOI: 10.1007/s41230-023-2122-6
Wen-jun Dong, Qiao-lei Li, Tian-ci Chen, Ming-ke Zou, Jing-jing Liang, Li-rong Liu, Hui Mei, Jin-guo Li
Ceramic cores are the key intermediate components of hollow blades for aero-engine. Conventional processes, such as hot-press molding and gel film casting, face difficulties in fabricating complex-structured ceramic cores due to the complexity of moulds and long process cycles. Stereolithography 3D printing provides a new idea for the fabrication of complex-structured ceramic cores. The effect of sintering temperature on open porosity, bulk density, weight loss rate, shrinkage rate, flexural strength and microstructure of the Al2O3-based ceramic core doped with 10vol.% polysilazane (PSZ) was studied. The sintering mechanism of PSZ-reinforced ceramic cores was analyzed. Results show that the optimum sintering temperature of PSZ-reinforced ceramic cores is 1,450 °C. At this temperature, the open porosity of the ceramic core is 36.60%, bulk density is 2.33 g·cm−3, weight loss rate is 22.11%, shrinkage rate along the X, Y, Z directions is 5.72%, 5.01%, 9.61%, respectively; the flexural strength is 28.794 MPa at 25 °C and 13.649 MPa at 1,500 °C. Properties of 3D printing PSZ-reinforced ceramic cores can meet the casting requirement of superalloy hollow blades, which is expected to promote the industrial application of 3D printing complex structure ceramic cores.
陶瓷芯是航空发动机中空叶片的关键中间部件。传统的工艺,如热压成型和凝胶膜铸造,由于模具的复杂性和漫长的工艺周期,在制造复杂结构的陶瓷芯时面临困难。立体光刻3D打印技术为复杂结构陶瓷芯的制造提供了新的思路。研究了烧结温度对掺杂10vol的al2o3基陶瓷芯的开孔率、容重、失重率、收缩率、抗弯强度和微观结构的影响。对%聚硅氮烷(PSZ)进行了研究。分析了psz增强陶瓷芯的烧结机理。结果表明,psz增强陶瓷芯的最佳烧结温度为1450℃。在此温度下,陶瓷芯的开孔率为36.60%,容重为2.33 g·cm−3,失重率为22.11%,X、Y、Z方向收缩率分别为5.72%、5.01%、9.61%;25℃时抗弯强度为28.794 MPa, 1500℃时抗弯强度为13.649 MPa。3D打印psz增强陶瓷芯的性能可以满足高温合金空心叶片的铸造要求,有望推动3D打印复杂结构陶瓷芯的工业应用。
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引用次数: 1
Microstructure and mechanical properties of Fe/NbC composite layer prepared by in-situ reaction 原位反应制备Fe/NbC复合层的微观结构和力学性能
3区 材料科学 Q2 Materials Science Pub Date : 2023-07-01 DOI: 10.1007/s41230-023-3024-3
Le Chen, Ji-lin Li, Meng-jun Wang, Jie Zheng, Yao Zhu, Zhuo-lin Liu, Bing-gui Lü
NbC ceramic surface-reinforced steel matrix composites were prepared by an in-situ reaction method at different temperatures (1,050 °C, 1,100 °C and 1,150 °C) for different times (1 h, 2 h and 3 h). The phase constitution, microstructure and fracture morphology of NbC ceramic surface-reinforced steel matrix composites were analyzed by XRD, SEM and EDS, and the effects of the in-situ reaction temperature and time on the mechanical properties were systematically studied. The results indicate that the NbC reinforcement layer is formed through the reaction between Nb atoms and carbon atoms diffused from the steel matrix to the Nb plate. The thickness of this reinforcement layer increases as the reaction time prolongs. Additionally, an increase in reaction temperature results in a thicker reinforcement layer, although the rate of increase gradually decreases. The relationship among the thickness of the NbC reinforcement layer, the reaction time and temperature was established by data fitting. The optimal tensile performance is achieved at 1,100 °C for 1 h, with a tensile strength of 228 MPa. It is also found that the defects between the reinforcement layer and the steel matrix are related to reaction temperature. At 1,100 °C, these defects are minimal. Fracture mostly occurs in the NbC reinforced layer of the composites, and the fracture mode is characterized by typical intergranular brittle fracture.
采用原位反应法制备了NbC陶瓷表面增强钢基复合材料,反应温度分别为1050℃、1100℃和1150℃,反应时间分别为1 h、2 h和3 h。采用XRD、SEM和EDS分析了NbC陶瓷表面增强钢基复合材料的相组成、显微组织和断口形貌,并系统研究了原位反应温度和时间对复合材料力学性能的影响。结果表明,NbC强化层是由Nb原子与从钢基体扩散到Nb板的碳原子反应形成的。随着反应时间的延长,增强层的厚度增加。另外,随着反应温度的升高,增强层变厚,但增加速率逐渐减小。通过数据拟合,建立了NbC增强层厚度与反应时间、温度之间的关系。在1100℃下,拉伸时间为1 h,拉伸强度为228 MPa,达到最佳拉伸性能。同时发现增强层与钢基体之间的缺陷与反应温度有关。在1100℃时,这些缺陷是最小的。断裂主要发生在复合材料的NbC增强层,断裂方式为典型的晶间脆性断裂。
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引用次数: 0
Mechanical properties and microstructural evolution of rheocast A356 semi-solid slurry prepared by annular electromagnetic stirring 环形电磁搅拌制备A356流变铸造半固态浆料的力学性能及微观组织演变
3区 材料科学 Q2 Materials Science Pub Date : 2023-07-01 DOI: 10.1007/s41230-023-3041-2
Mohammad Taghi Asadi Khanouki
Nowadays, having an effective technique in preparing semi-solid slurries for rheocasting process seems to be an essential requirement. In this study, semi-solid slurry of A356 aluminum alloy was prepared by three-phase annular electromagnetic stirring (A-EMS) technique under different conditions. The effects of stirring current, pouring temperature and stirring time on microstructural evolution, mean particle size, shape factor and solid fraction were investigated. The rheocasting process was carried out by using a drop weight setup and to inject the prepared semi-solid slurry in optimal conditions into the step-die cavity. The filling behavior and mechanical properties of parts were studied. Microstructural evolution showed that the best semi-solid slurry which had fine spherical particles with the average size of ∼27 µm and a shape factor of ∼0.8 was achieved at the stirring current of 70 A, melt pouring temperature of 670 °C, and stirring time of 30 s. Under these conditions, the step-die cavity was completely filled at die preheating temperature of 470 °C. The hardness increases by decreasing step thickness as well as die preheating temperature. Moreover, the tensile properties are improved at lower die preheating temperatures. The fracture surface, which consists of a complex topography, indicates a typical ductile fracture.
目前,有一种有效的技术来制备半固体浆料的流变铸造工艺似乎是一个必不可少的要求。采用三相环形电磁搅拌(A-EMS)技术,在不同条件下制备了A356铝合金半固态浆料。研究了搅拌电流、浇注温度和搅拌时间对微观组织演变、平均粒径、形状因子和固相分数的影响。采用滴重装置,在最佳条件下将制备好的半固态浆料注入阶梯模腔,进行了流变铸造工艺。对零件的填充行为和力学性能进行了研究。结果表明,在搅拌电流为70 a、熔体浇注温度为670℃、搅拌时间为30 s的条件下,获得的最佳半固态浆料为平均粒径为~ 27µm、形状因子为~ 0.8的球状细颗粒。在此条件下,在470℃的模具预热温度下,阶梯模腔被完全填充。通过减小步长厚度和模具预热温度来提高硬度。此外,在较低的模具预热温度下,拉伸性能得到改善。断口形貌复杂,为典型的韧性断裂。
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引用次数: 0
Microstructure and mechanical properties of a cast heat-resistant rare-earth magnesium alloy 铸造耐热稀土镁合金的组织与力学性能
3区 材料科学 Q2 Materials Science Pub Date : 2023-07-01 DOI: 10.1007/s41230-023-2015-8
Xiao-ping Zhu, Jun-qing Yao, Hai-long Wu, Xin-wang Liu, Hua Liu, Zi-tian Fan, Shu-lin Lü, Kai Wang, Zi-dong Wang
Microstructure, mechanical properties and phase transformation of a heat-resistant rare-earth (RE) Mg-16.1Gd-3.5Nd-0.38Zn-0.26Zr-0.15Y (wt.%) alloy were investigated. The as-cast alloy is composed of equiaxed α-Mg matrix, net-shaped Mg5RE and Zr-rich phases. According to aging hardening curves and tensile properties variation, the optimized condition of solution treatment at 520 °C for 8 h and subsequent aging at 204 °C for 12 h was selected. The continuous secondary Mg5RE phase predominantly formed at grain boundaries during solidification transforms to residual discontinuous β-Mg5RE phase and fine cuboid REH2 particles after heat treatment. The annealed alloy exhibits good comprehensive tensile property at 350 °C, with ultimate tensile strength of 153 MPa and elongation to fracture of 6.9%. Segregation of RE elements and eventually RE-rich precipitation at grain boundaries are responsible for the high strength at elevated temperature.
研究了耐热稀土(RE) Mg-16.1Gd-3.5Nd-0.38Zn-0.26Zr-0.15Y (wt.%)合金的显微组织、力学性能和相变。铸态合金由等轴α-Mg基体、网状Mg5RE和富zr相组成。根据时效硬化曲线和拉伸性能变化,选择520℃固溶处理8 h, 204℃时效12 h的最佳工艺条件。凝固过程中主要在晶界处形成的连续的Mg5RE次生相在热处理后转变为残余的不连续的β-Mg5RE相和细小的长方体REH2颗粒。退火合金在350℃时具有良好的综合抗拉性能,抗拉强度为153 MPa,断裂伸长率为6.9%。稀土元素的偏析和最终在晶界处的富稀土析出是高温下高强度的原因。
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引用次数: 0
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China Foundry
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