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Real-Time Performance Optimization to Prevent Productivity Decline in Deep Offshore Producers 实时性能优化,防止深海生产商产能下降
Pub Date : 2022-02-16 DOI: 10.2118/208828-ms
B. Izgec, L. Kalfayan
This paper presents a continuous well performance analysis technique that identifies formation damage and/or productivity loss real-time. It also provides insights into expected damage mechanisms enabling successful and efficient stimulation treatments. The analytical technique recognizes damage patterns at inception. The diagnostics to drive operational decisions are then presented as simple cartesian plots that grant easy access to users of all levels of experience. During initial well ramp-ups, the diagnostic plots can be automated with high frequency data. After reaching target drawdowns, low frequency data provides optimum surveillance. Case studies from several deepwater Gulf of Mexico wells demonstrate how the technique has been successfully operationalized to eliminate productivity loss, gain early insight into damage mechanisms, and investigate the impact of well interventions. Comparisons with pressure transient analysis and numerical history matching studies with all completion details corroborate the robustness of the method. Shutting in the wells is not required for the analysis, therefore lost production and additional stress cycles on the completion are eliminated. The analysis also identifies the maximum drawdown limit, thereby helping the operator optimize well performance real-time.
本文介绍了一种连续井动态分析技术,可以实时识别地层损害和/或产能损失。它还提供了对预期损伤机制的深入了解,从而实现了成功和有效的增产措施。分析技术在一开始就识别损伤模式。然后,驱动操作决策的诊断以简单的笛卡尔图的形式呈现,使所有经验水平的用户都可以轻松访问。在最初的油井增产过程中,可以使用高频数据自动绘制诊断图。在达到目标降压后,低频数据提供最佳监测。墨西哥湾几口深水井的案例研究表明,该技术成功地消除了产能损失,获得了早期损害机制的信息,并研究了油井干预的影响。与所有完井细节的压力瞬态分析和数值历史匹配研究的比较证实了该方法的鲁棒性。分析不需要关井,因此可以消除生产损失和完井时的额外应力循环。该分析还可以确定最大压降极限,从而帮助作业者实时优化油井性能。
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引用次数: 0
A Novel Single-Stage Sandstone Acidizing Fluid 一种新型单级砂岩酸化液
Pub Date : 2022-02-16 DOI: 10.2118/208803-ms
Haiyan Zhao, M. Ziauddin, P. Abivin, T. Yusuf, O. Karazincir, Wade Williams, B. Comeaux
Sandstone acidizing operations usually include solvent and acid preflush, main acid treatment, and post-flush stages. However, the acid preflush stage needs good design and execution to prevent formation damage. Moreover, multiple-stage operations require large-volume fluids and pumping time. Therefore, it is challenging to stimulate sandstone formations, especially those with high clay and carbonate content. A novel single-stage acid has been developed to overcome these challenges and improve the stimulation success rate in a cost-effective manner. The application of the new acid system has been studied in laboratory testing. Core flow tests were performed to evaluate the stimulation performance with Berea Gray and Bandera Gray from 160° to 300°F. An inductively coupled plasma (ICP) instrument was used to analyze the ions in the spent acid effluent. The performance was compared with mud acid and organic mud acid. The acid-rock reactions were studied by batch reactor tests. Compatibility with crude oil and mutual solvent was also tested. The results of core flow tests have shown that the new acid was used to treat the sandstone cores effectively at temperatures from 160° to 300°F. The regained permeability range varies from 115% to 400% under different conditions. The new acid provided similar or better performance compared with the combination of acid preflush and mud acid or organic mud acid. High concentrations of Al and Si were observed in the spent acid effluents by ICP analysis, indicating the high dissolution capacity of clays by the new acid. The new acid is highly compatible with carbonate, which was supported by the high concentrations of Ca and Mg in the spent acid. Both core flow tests and batch reactor tests have shown that the new acid stabilizes the problematic ions (Al, Ca, Mg and Fe) in the spent acid. The new acid is compatible with mutual solvent from the core flow tests; therefore, the mutual solvent preflush can be eliminated. The new acid also has good corrosion control due to the relatively high pH compared with mud acid. Overall, the new single stage acid has been used to stimulate the sandstone cores successfully without acid preflush and solvent preflush. A differentiating characteristic of the fluid is that it greatly reduces the risk of treatment failure by reducing primary, secondary, and tertiary precipitation, while maintaining high dissolving power for clays. It uses a different, more cost-effective chemical pathway to stabilize problematic ions compared to traditional single-step sandstone acidizing systems. The new fluid simplifies operation by reducing the total treatment fluid volume, the total number of fluid stages, and the number of fluid types needed at the wellsite.
砂岩酸化作业通常包括溶剂和酸预冲、主酸处理和后冲阶段。然而,酸预冲洗阶段需要良好的设计和执行,以防止地层损坏。此外,多级作业需要大量的流体和泵送时间。因此,对砂岩地层,特别是粘土和碳酸盐含量高的砂岩地层进行增产改造具有挑战性。为了克服这些挑战,以经济有效的方式提高增产成功率,开发了一种新型的单级酸。对新酸体系的应用进行了实验室试验研究。通过岩心流动测试,评估Berea Gray和Bandera Gray在160°F至300°F范围内的增产效果。采用电感耦合等离子体(ICP)仪对废酸废水中的离子进行了分析。并与泥酸、有机泥酸进行了性能比较。采用间歇式反应器对酸岩反应进行了研究。并对其与原油和互溶溶剂的相容性进行了测试。岩心流动测试结果表明,在160°~ 300°F的温度范围内,这种新型酸可以有效地处理砂岩岩心。不同条件下,恢复渗透率范围为115% ~ 400%。与预冲酸与泥浆酸或有机泥浆酸的组合相比,新酸具有相似或更好的性能。通过ICP分析,在废酸废水中观察到高浓度的Al和Si,表明新酸对粘土的溶解能力强。废酸中含有高浓度的Ca和Mg,与碳酸盐具有良好的相容性。堆芯流动试验和间歇反应器试验均表明,新酸能稳定废酸中的问题离子(Al、Ca、Mg和Fe)。从岩心流动试验看,新型酸与相互溶剂相容;因此,可以消除相互溶剂预冲。与泥浆酸相比,新酸的pH值相对较高,具有良好的抗腐蚀性能。总的来说,新的单级酸在没有酸预冲和溶剂预冲的情况下,成功地对砂岩岩心进行了增产。该流体的一个与众不同的特点是,通过减少一次、二次和第三次降水,它大大降低了处理失败的风险,同时保持了对粘土的高溶解能力。与传统的单步砂岩酸化系统相比,它使用了一种不同的、更具成本效益的化学途径来稳定有问题的离子。新型流体通过减少处理液的总体积、流体级的总数量和井场所需的流体类型数量,简化了操作。
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引用次数: 0
From Lab to Field 2 - Assessing Impact of Fluid Density, Salinity, and Injection Rate on Fines Migration Potential in Gas Wells 从实验室到现场2——评估流体密度、盐度和注入速率对气井中细颗粒运移潜力的影响
Pub Date : 2022-02-16 DOI: 10.2118/208868-ms
Ike Mokogwu, Ewan Sheach, Sam Wilson, P. Hammonds, G. Graham
Detecting and mitigating near-wellbore fines migration is important in order to avoid formation damage in many gas wells. This has bearing not only on gas production but also carbon capture through the geological storage of Carbon dioxide (CO2), in pressurised, deep saline aquifers. Fines migration may occur because of weakened electrostatic forces caused by an introduced fluid which also makes fines more prone to movement by viscous drag, or where the drag forces are sufficient to physically break or lift clay crystals from their original location and transport them through the pore network. Potential near-wellbore fines migration is typically assessed via coreflood tests. In an ideal scenario, such tests will be conducted using reservoir core material, with reservoir gas at rates and pressures comparable to the reservoir. However, due to practicality and cost constraints, tests are often conducted using available outcrop core and scaled down reservoir conditions. Laboratory tests reduce higher field pressures down to lab scale. In certain scenarios, simulating the total gas flux in a given near-wellbore system is achieved by increasing gas flow rates. Although, in some investigations, the need to utilise field realistic pressures in the lab is also becoming more of a requirement. This paper aims to address differences in lab protocols by examining both field realistic and scaled down conditions to aid best practice for formation damage identification and remediation. The potential utility, and challenges associated with a variety of hydrocarbon gas analogues in scenarios where increased gas density is required is also discussed. The fines migration potential of a clay rich (Blaxter) sandstone was demonstrated using salinity and flux related fines migration methods, demonstrating that under certain conditions, selected cores are susceptible to fines migration. Test results with CO2 at low and medium pressure conditions demonstrated that pressure and flow rate variation in the laboratory had no notable effect on the fines migration of Blaxter sandstone samples, under the conditions examined. Additional tests conducted at higher pressures of 7250 psig did not yield fines migration although a 10% permeability loss was observed. While this was the case for Blaxter sandstone, caution is advised when testing with field substrate under these conditions, as reservoir rocks may be more susceptible to damage. Field cores typically display a well-developed crystal structure and surface area/volume ratios more normally associated with kaolinite booklets and platelets of clays, which may expose them to higher drag forces. Therefore, the minimal permeability reduction effects observed at high pressure may potentially be multiplied in field cores. Additional core flood tests were conducted to evaluate the use of hydrocarbon gas analogues (such dodecane) as a substitute for dense gases in core flood testing. This allows lower pressures than that would be r
在许多气井中,检测和减轻近井细粒运移对于避免地层破坏非常重要。这不仅关系到天然气的生产,也关系到二氧化碳的地质储存(在加压的深盐水含水层中)所产生的碳捕获。由于引入的流体所产生的静电力减弱,细颗粒可能会发生迁移,这也使得细颗粒更容易受到粘性阻力的移动,或者阻力足以物理破坏或抬升粘土晶体,使其离开原始位置并通过孔隙网络运输。潜在的近井细颗粒运移通常通过岩心驱油测试来评估。在理想情况下,此类测试将使用储层岩心材料进行,储层气体的速率和压力与储层相当。然而,由于实用性和成本限制,通常使用可用的露头岩心和缩小的油藏条件进行测试。实验室测试将较高的现场压力降低到实验室规模。在某些情况下,模拟给定近井系统中的总气体通量可以通过增加气体流速来实现。尽管在一些研究中,需要在实验室中利用现场实际压力也变得越来越必要。本文旨在通过研究现场实际情况和缩小后的条件,解决实验室方案的差异,从而为地层损害识别和修复提供最佳实践。在需要增加气体密度的情况下,还讨论了各种碳氢化合物气体类似物的潜在用途和挑战。利用盐度和通量相关的细粒运移方法,证明了富粘砂岩(Blaxter)的细粒运移潜力,表明在一定条件下,选定的岩心容易受到细粒运移的影响。在低压和中压条件下的CO2测试结果表明,在实验条件下,实验室压力和流量的变化对Blaxter砂岩样品的细粒迁移没有显著影响。在7250 psig的高压下进行的额外测试,虽然观察到10%的渗透率损失,但没有产生细粒运移。虽然Blaxter砂岩就是这种情况,但在这种条件下使用现场基质进行测试时,需要谨慎,因为储层岩石可能更容易受到损害。野外岩心通常显示出发育良好的晶体结构和表面积/体积比,通常与高岭石小块和粘土薄片有关,这可能使它们暴露在更高的阻力下。因此,在高压下观察到的最小渗透率降低效应可能会在现场岩心中成倍增加。进行了额外的岩心驱油试验,以评估在岩心驱油试验中使用碳氢化合物气体类似物(如十二烷)替代致密气体的情况。这允许比压缩气体所需的压力更低。结果表明,在适当的条件下,十二烷可以作为气体类似物。使用十二烷时需要注意的是,高压测试结果表明,在测试条件下,十二烷导致岩心渗透率降低24%。本文提出的工作旨在改进岩心驱油测试作为识别地层损害的工具,特别是在气井中。这项工作提供了有用的指导,并表明尽管在非典型压力下进行测试并不普遍,但它可以进行,并且可能需要在特定情况下进行更强大的地层损害识别程序。
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引用次数: 0
Rapid Curing Environmentally Degradable Polymeric Pill for Loss Circulation Treatment 用于失循环处理的快速固化环境可降解聚合物丸
Pub Date : 2022-02-16 DOI: 10.2118/208842-ms
M. Magzoub, S. Salehi, I. Hussein, M. Nasser, A. Ghalambor
Loss circulation is frequent while drilling in naturally fractured or depleted reservoirs, which is usually associated with high non-productive time (NPT). Moreover, naturally pre-existing fractures may propagate when fluid pressure inside the fractures exceeds the minimum principal stress. The primary objective of this paper is to investigate the operational performance of a quick applying polymeric pill to treat severe loss circulation in highly fractured formations. To strengthen the wellbore in the presence of large fractures, proper size and concentration of loss circulation materials (LCM) are required. In this paper, a crosslinked polymer comprised of inorganic crosslinker (Aluminum-Acetate) is used to cure severe loss circulation by completely sealing fractured or high permeable formations. To achieve this, the project investigated the rheological behavior, mechanical properties, gelation mechanisms, and the filtration of the crosslinked polymer through an artificial fracture. The effect of concentration, temperature, pH, and salinity on the stability and gelation process was also assessed. The rheological properties of polyacrylamide/Aluminum-Acetate (PAM/AlAc) in aqueous solutions, with concentrations varying from 1 to 3 wt.%, were highly affected by pH, time, and shear rates, while temperature changes have less impact. The Aluminum-Acetate has a broad operational window and can form a strong gel in temperatures ranging from 75°F to 260°F. Nanosilica (NS) in small quantities less than 1% was found to enhance the stability and strength of the polymer. The results revealed that the gelation time of the Aluminum-Acetate is controllable at pH conditions between 3.5 and 8.5, and the most stable gel was formed in the temperature range from 65°F to 212°F. Fracture sealing experiments demonstrated the ability of (PAM/AlAc) to form a strong plug with sealing pressure of up to 700 psi. In general, the Aluminum-Acetate reinforced with nanosilica has great potential applications in curing severe loss circulation in high fractured formations under a wide temperature range. This paper describes a detailed method of mixing and preparing stable and functioning polyacrylamide/Aluminum-Acetate pill for curing a severe loss of circulation. The new proposed aluminum-based salt was investigated as a potential environmentally friendly replacement for the conventional chromium acetate as crosslinkers for polyacrylamide. The paper provides a good understanding of the rheological, mechanical properties, and gelation characteristics, which are important factors affecting the spotting of these pills.
在天然裂缝或衰竭油藏中钻井时,漏失循环经常发生,这通常与高非生产时间(NPT)有关。此外,当裂缝内的流体压力超过最小主应力时,自然存在的裂缝可能会扩展。本文的主要目的是研究一种快速应用的聚合物丸剂在处理高度裂缝地层中严重漏失的作业性能。为了在存在大裂缝的情况下加固井筒,需要适当尺寸和浓度的漏失循环材料(LCM)。本文采用一种由无机交联剂(醋酸铝)组成的交联聚合物,通过完全密封裂缝或高渗透地层来解决严重漏失的问题。为了实现这一目标,该项目研究了交联聚合物的流变行为、机械性能、凝胶机制以及通过人工裂缝的过滤情况。还评估了浓度、温度、pH和盐度对凝胶稳定性和凝胶过程的影响。聚丙烯酰胺/醋酸铝(PAM/AlAc)在浓度为1 ~ 3 wt.%的水溶液中的流变性能受pH、时间和剪切速率的影响较大,而温度变化的影响较小。醋酸铝具有宽的操作窗口,可以在75°F到260°F的温度范围内形成强凝胶。少量的纳米二氧化硅(NS)(小于1%)被发现可以提高聚合物的稳定性和强度。结果表明,在pH为3.5 ~ 8.5的条件下,醋酸铝的凝胶时间是可控的,在65 ~ 212°F的温度范围内凝胶形成最稳定。裂缝密封实验表明,(PAM/AlAc)能够在高达700 psi的密封压力下形成坚固的桥塞。综上所述,纳米二氧化硅增强的醋酸铝在宽温度范围内的高裂缝地层中具有很大的应用潜力。本文详细介绍了一种用于治疗严重漏失的聚丙烯酰胺/醋酸铝丸的混合制备方法。研究了新提出的铝基盐作为传统醋酸铬交联剂的潜在环保替代品。本文提供了一个很好的了解流变学,力学性能和凝胶特性,这是重要的因素,影响这些药丸的斑点。
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引用次数: 0
Improving Fluid Loss Control During Well Intervention; A Case Study on the Use of Innovative Salt System 改善修井过程中的失液控制创新盐体系应用的案例研究
Pub Date : 2022-02-16 DOI: 10.2118/208833-ms
M. Hussein, Hamad Al-Rashedi, A. Al-Naqi, S. González, Abdulaziz Erhamah, Reeham Najaf, Satinder Malik, D. Bosilca, Mohamed Ali, K. Tresco, M. Luyster
Kuwait heavy oil development target reservoir is a shallow, sub-hydrostatic and unconsolidated sandstone with relatively high porosity and permeability. Due to nature of this reservoir, well intervention operations in North Kuwait Heavy Oil Asset exhibit a higher risk of significant fluid loss that causes wellbore impairment, incremental operational costs, excess brine volume usage, and more importantly a significant impact on production deferment. The latter is due to formation damage and the time required to produce the completion fluid that is lost to the reservoir during any well intervention. The objective of using a cost-effective and less non-damaging fluid is achieved by the application of a novel customized salt system that was successfully trialed in the field. A systematic research was employed to find a suitable product/system that could be used in sub- hydrostatic conditions, able to effectively control fluid loss while retaining as near the original permeability. This new system and subsequent formulation adhered to the following criteria: Readily available Cost effective Easy to formulate and pump Easy to circulate out No long-term formation damage thus retaining original formation permeability The success of this fluid loss control material is indicated by a constant fluid level at surface after application thereby confirming its effectiveness in meeting the desired objectives. This salt system application was successfully field tested, and the results were satisfactory. During well intervention operations, the system effectively arrested fluid loss as confirmed by the fluid level measured at surface. Post operation, the well was brought back immediately to its original rate thereby confirming little to no permanent reduction to reservoir permeability. Historically, during well interventions in Kuwait Heavy Oil field, dynamic loss rates measured were in the 100 to 120 bbl per hour range. Post application of this salt system showed fluid loss rates ranging from 3 to 4 bbl per hour. To date no post acid stimulations were required to restore well production to original levels. This system was readily adapted for thermal application and compatibility with existing fluids, good bridging characteristics, as well as flow-back enhancement. This approach eliminated additional AFE costs by minimizing dynamic losses.
科威特稠油开发目标储层是一种孔隙度和渗透率相对较高的浅层、亚静水松散砂岩。由于该油藏的性质,北科威特重油资产的油井干预作业存在较大的流体漏失风险,这会导致井眼受损,增加作业成本,过量使用盐水,更重要的是对生产延迟产生重大影响。后者是由于地层损坏和在任何修井过程中生产完井液到储层所需的时间。采用了一种新型定制盐体系,并在现场进行了成功的试验,从而实现了使用成本效益高且无害的流体的目标。通过系统的研究,找到了一种合适的产品/系统,可以在亚流体静力条件下使用,能够有效地控制流体漏失,同时保持接近原始渗透率。这种新体系及其后续配方遵循以下标准:易于获得,成本效益高,易于配制和泵送,易于循环排出,不会对地层造成长期损害,从而保持了原有的地层渗透率。应用后,地面的液位保持不变,表明这种降滤失材料的成功,从而证实了其达到预期目标的有效性。该盐体系的应用已成功进行了现场测试,取得了满意的效果。在修井作业期间,该系统有效地阻止了流体漏失,并通过地面测量得到了证实。作业结束后,该井立即恢复到原始速率,从而证实储层渗透率几乎没有永久性降低。从历史上看,在科威特重油油田的修井过程中,测量到的动态损失率在每小时100到120桶之间。应用该盐体系后,流体损失率为每小时3至4桶。到目前为止,还不需要进行酸处理就能将油井产量恢复到原来的水平。该系统很容易适应热应用,与现有流体兼容,具有良好的桥接特性,并增强了返排。这种方法通过最小化动态损失消除了额外的AFE成本。
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引用次数: 0
Novel Approach in Deploying Filter Cake Breaker Post Open Hole Gravel Pack with Non-Aqueous Gravel Pack Carrier Fluid in Reservoir with Reactive Shales 在含反应性页岩油藏中,采用非含水砾石充填载体液进行裸眼滤饼破碎后砾石充填的新方法
Pub Date : 2022-02-16 DOI: 10.2118/208827-ms
Tint Htoo Aung, Romain Djenani, A. Byrd, Matt Beavers, Cedric Manzoleloua, Sarah Green, B. Gadiyar
Non-aqueous gravel pack carrier fluids (GPCF) have been introduced into the industry to eliminate the risks associated with the water-based carrier fluids in the presence of reactive shale interbeds in the reservoir. However, non-aqueous GPCF pose a significant barrier to the effective deployment of post-gravel pack filter cake breaker (FCB) application because all FCB systems are water-based. Therefore, a novel approach was developed for FCB application in non-aqueous GPCF environment to improve the efficiency of the FCB and the overall well performance. The non-aqueous GPCF was redesigned from ground up to promote the better diffusion of the FCB. This was accomplished by introducing a reversible emulsifier package into the non-aqueous GPCF design which allows the gravel to change wettability from an oil-wet state to a water-wet state when a low pH solution i.e., breaker is spotted inside the sand screens after the open hoel gravel pack (OHGP). To complement this, the FCB design was deconstructed, and the in-situ breaker component was blended with the gravel. The concept was to incorporate the in-situ breaker component into the gravel pore space which would promote better diffusion of FCB through the reversible non-aqueous GPCP. The in-situ breaker component is inert to the carrier fluid until it is activated by the temperature and water posing no threat to the stability of the carrier fluid while pumping. The innovative approach was tested in the laboratory setting using ceramic disks and return to flow method to prove the concept before conducting an elaborate return permeability testing with the reservoir core plugs for the final validation. Return to flow method indicated that the novel approach could improve the results by at least 10% compared to the baseline test with no breaker application. In the return permeability tests with reservoir core plugs, the novel approach resulted in 76% of the initial permeability whereas the baseline test was only 50%. Both the tests with ceramic disks and full-sequence formation damage tests with actual reservoir cores highlighted the benefits of the novel approach for gravel packing with non-aqueous GPCF and post-gravel pack FCB scenario. Non-aqueous GPCFs are relatively new to the industry and no record of the filter cake breaker application in such environment exists. This novel approach makes the filter cake breaker application possible in non-aqueous environment and pushes the existing boundaries of filter cake breaker chemistries.
非水砾石充填携砂液(GPCF)已被引入该行业,以消除油藏中存在活性页岩互层时水基携砂液带来的风险。然而,非水相GPCF对砾石充填后滤饼分离器(FCB)的有效部署构成了重大障碍,因为所有FCB系统都是水基的。因此,开发了一种在非水GPCF环境中应用FCB的新方法,以提高FCB的效率和整体井性能。对非水GPCF进行了从头到尾的重新设计,以促进FCB更好的扩散。这是通过在非水GPCF设计中引入可逆乳化剂来实现的,当打开式砾石充填(OHGP)后,在筛管内发现低pH溶液(即破胶剂)时,可以将砾石的润湿性从油湿状态转变为水湿状态。为了补充这一点,FCB设计被解构,并将原位破碎组件与砾石混合。其理念是在砾石孔隙空间中加入原位破碎组分,这将促进FCB通过可逆非水GPCP更好地扩散。在被温度和水激活之前,原位断路器组件对携带液是惰性的,在泵送过程中不会对携带液的稳定性构成威胁。该创新方法在实验室环境中进行了测试,使用陶瓷盘和回流法来验证该概念,然后使用储层岩心塞进行了详细的回流渗透率测试,以进行最终验证。回归流动方法表明,与不使用断路器的基线测试相比,这种新方法可以将结果提高至少10%。在储层岩心桥塞的渗透率测试中,新方法的渗透率达到了初始渗透率的76%,而基线测试仅为50%。无论是陶瓷盘测试,还是实际储层岩心的全层序地层损伤测试,都强调了采用非水GPCF和砾石充填后FCB方案进行砾石充填的新方法的优势。非水相GPCFs是一个相对较新的行业,没有在这种环境下应用的滤饼破碎机的记录。这种新颖的方法使滤饼分离器在非水环境中的应用成为可能,并突破了滤饼分离器化学的现有界限。
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引用次数: 0
Smart Drill-In Fluid and Breaker Design for a Limestone Reservoir for Persian Gulf Offshore Wells 波斯湾海上油井石灰石储层智能入井液与破井器设计
Pub Date : 2022-02-16 DOI: 10.2118/208862-ms
Gianna Pietrangeli, M. Barry, Daniel Alvarez, Laurie Hayden, Ajay Addagalla
Offshore reservoirs in the Southwest Persian Gulf are commonly oil-wet limestone with an average permeability of 10 md. High production of hydrogen sulfide and carbon dioxide is often encountered in the oil producer wells. The tight reservoirs are commonly drilled with water-based reservoir drill-in fluid (DIF) with high concentrations of lubricants. DIFs based on sodium chloride or calcium chloride brines with corresponding optimal breakers to remove the filter cakes were formulated and evaluated to optimize production in newly drilled wells. Fluid displacement by return permeability (RP) testing was used to evaluate the fluid/limestone rock interaction. This paper discusses the compatibility of a sodium chloride-based and a calcium chloride-based DIF with limestone formation and the necessity of introducing an optimal breaker to maximize the opportunity to achieve high production rates. RP tests are widely used to determine the potential damage caused by the DIF and production enhancement after removing the DIF filter cake with a breaker. Desired results for RP tests performed with the brine-based DIF in limestone cores were a minimum of 75% regain permeability to oil production. The cores used for the RP tests were from an analogue limestone outcrop from a Mississippian formation with permeability between 9-16 md and 14-18% porosity. DIF properties were determined following API RP-13I recommended practices. Emulsion tendency for the fluids was determined by using emulsion tendency testing with a high-speed mixer to mimic shear at the pore throat. A 10.0 lb/gal sodium chloride water-based DIF with a high content of ester-based lubricant was designed for drilling a limestone formation. A high pH close to 10 was necessary to control H2S and CO2 corrosion. The return permeability of the 10.0 lb/gal fluid was 44% using LVT-200 oil as an analogue for the native hydrocarbon permeating fluid. The low return permeability was likely caused by emulsion blockages generated by the saponification of the ester-based lubricant used in the sodium chloride-based DIF. Emulsion tendency was observed between the DIF filtrate and permeating fluid in a fluid/fluid compatibility evaluation. Therefore, a breaker system was formulated and customized to enhance RP from 44% to a minimum of 75%. In contrast, a 11.0 lb/gal calcium chloride-based DIF with pH of 9.0 and same ester-based lubricant content was evaluated using a comparable limestone analogue core and demonstrated a high return permeability (>80%). Filtrate of the calcium chloride-based DIF did not form emulsions during fluid displacement in the RP test. Compatibility evaluation (return permeability) between drill-in fluids and reservoir rock is essential for oil producer wells in order to determine and avoid potential problems caused by interactions between them.
波斯湾西南部的海上储层通常为油湿石灰岩,平均渗透率为10md。在采油井中经常遇到高硫化氢和二氧化碳产量的问题。致密储层通常使用含有高浓度润滑剂的水基油藏钻井液(DIF)进行钻井。以氯化钠或氯化钙盐水为基础的DIFs,配以相应的最佳破冰剂来去除滤饼,并对其进行了配方和评估,以优化新钻井的产量。通过反渗透(RP)测试流体驱替来评估流体/石灰岩相互作用。本文讨论了氯化钠基和氯化钙基DIF与石灰石地层的相容性,以及引入最佳破胶剂的必要性,以最大限度地提高产量。RP试验被广泛用于确定DIF的潜在危害,以及用破碎机去除DIF滤饼后的增产效果。在石灰石岩心中使用盐水基DIF进行RP测试时,期望的结果是至少恢复75%的原油生产渗透率。用于RP测试的岩心来自密西西比地层的模拟石灰岩露头,渗透率为9- 16md,孔隙度为14-18%。DIF属性是按照API RP-13I推荐的做法确定的。采用高速混合器模拟孔喉处剪切,进行乳化倾向测试,确定了流体的乳化倾向。设计了一种10.0 lb/gal氯化钠水基DIF,具有高含量的酯基润滑剂,用于钻井石灰岩地层。为了控制H2S和CO2腐蚀,需要接近10的高pH值。使用LVT-200油作为原生烃渗透液的模拟物,10.0 lb/gal流体的回渗率为44%。低回流渗透率可能是由于在氯化钠基DIF中使用的酯基润滑剂在皂化过程中产生乳液堵塞造成的。在流体/流体相容性评价中,观察到DIF滤液与渗透流体之间存在乳化倾向。因此,制定并定制了一种断路器系统,将RP从44%提高到至少75%。相比之下,使用类似的石灰石模拟岩心评估了11.0 lb/gal的氯化钙基DIF, pH为9.0,相同的酯基润滑剂含量,显示出高的回渗性(>80%)。在RP试验中,氯化钙基DIF滤液在流体置换过程中未形成乳状液。为了确定和避免钻入流体与储层岩石之间的相互作用带来的潜在问题,钻入流体与储层岩石之间的相容性评价(回渗性)对采油井至关重要。
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引用次数: 0
Subband Characteristics of the Two-Dimensional Inversion Carrier System in p-InSb Bicrystals p-InSb双晶中二维反转载流子体系的子带特性
Pub Date : 1986-12-31 DOI: 10.1515/9783112493182-057
W. Braune, N. Kubicki, N. Pruß, R. Herrmann
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引用次数: 0
On the Mechanism of Charge Carrier Scattering in Germanium with Point Defects under Cyclotron Resonance 回旋共振下点缺陷锗中载流子散射机理的研究
Pub Date : 1986-12-31 DOI: 10.1515/9783112493182-055
V. Gatalskaya
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引用次数: 0
Thallium-Related Isoelctronic Bound Excitons in Silicon. A Bistable Defect at Low Temperatures 硅中铊相关等电子束缚激子。低温双稳态缺陷
Pub Date : 1986-12-31 DOI: 10.1515/9783112493182-027
H. Conzelmann, A. Hangleiter, J. Weber
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引用次数: 0
期刊
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