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Cumulative Fatigue of Nitinol due to Multiple Applied Cyclic Strains 多次循环应变作用下镍钛诺的累积疲劳
Paul L. Briant, Louis G. Malito, J. Schaffer, T. Hamilton
Typical S/N type testing to determine the fatigue limit of Nitinol is done over a range of strain amplitudes; however, each specimen sees only a single peak strain amplitude during cycling. The effect of variable loading on Nitinol is therefore not understood. The purpose of this study was to evaluate any potential cumulative fatigue effect of combining low strain amplitude cycles with high strain amplitudes cycles on Nitinol wire apex specimens. A series of fatigue tests were performed to evaluate the fatigue response of Nitinol to variable loading. The results demonstrated that fatigue cycles at lower strain amplitudes can limit the number of higher amplitude cycles to failure in a variable loading scenario. However, the results also indicate that a small number of higher amplitude cycles can dominate the fatigue damage; almost all fractures occurred shortly after completing a section of higher amplitude cycles.
确定镍钛诺疲劳极限的典型S/N型试验是在一定的应变幅值范围内进行的;然而,在循环过程中,每个试样只看到一个峰值应变幅度。因此,不了解可变载荷对镍钛诺的影响。本研究的目的是评估低应变幅值循环与高应变幅值循环相结合对镍钛诺丝顶点试件的潜在累积疲劳效应。通过一系列的疲劳试验来评价镍钛诺合金在变载荷下的疲劳响应。结果表明,在可变加载情况下,较低应变幅值的疲劳循环可以限制较高应变幅值的疲劳循环次数。然而,结果也表明,少量的高振幅循环可以主导疲劳损伤;几乎所有裂缝都是在完成一段高振幅循环后不久发生的。
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引用次数: 0
Thermodynamical Model of NiTi SMA Including Plastic Deformation Mechanisms 含塑性变形机制的NiTi SMA热力学模型
P. Sedlák, M. Frost, H. Seiner, L. Heller, P. Šittner
This paper presents an extension of a well-established constitutive model for NiTi covering both reversible (elastic, martensitic transformation, martensite reorientation) and irreversible (plastic) deformation mechanisms. Besides the inclusion of mechanisms of plastic deformation in both austenitic and martensitic phases in an independent manner, the model also newly captures more complex coupled phenomena of martensitic transformation and plastic deformation, such as transformation-induced plasticity, stabilization of martensite by plastic deformation, or plasticity-induced microstrain heterogeneity leading to functional fatigue. Despite a large number of different mechanisms involved in the model, which is reflected by a considerable number of internal parameters introduced for the description of the evolving microstructure of the material, the model still brings a basic, simple phenomenological understanding of the coupled transformation-plasticity proceeding in NiTi. After successful implementation to FEM software, the model provides new possibilities for simulations of NiTi components' behavior and processing.
本文提出了一个已建立的镍钛本构模型的扩展,该模型涵盖了可逆(弹性、马氏体转变、马氏体再取向)和不可逆(塑性)变形机制。除了独立地包含奥氏体和马氏体相的塑性变形机制外,该模型还捕获了马氏体相变和塑性变形更复杂的耦合现象,如相变诱导塑性、塑性变形对马氏体的稳定或塑性诱导的微应变非均质性导致的功能疲劳。尽管该模型涉及大量不同的机制,这反映在为描述材料微观结构演变而引入的大量内部参数上,但该模型仍然对NiTi中耦合相变-塑性过程提供了基本的、简单的现象学理解。该模型在有限元软件上成功实现后,为镍钛构件的行为和加工过程的仿真提供了新的可能性。
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引用次数: 0
Influence of Active Af on the Fatigue Performance of Peripheral Stents Subjected to Physiological Loading Conditions 生理载荷条件下主动Af对周围支架疲劳性能的影响
M. Frotscher, M. Kiekbusch, S. Mews, A. Knopp, D. Serowietzki
The temperature difference between active austenite finish temperature, Af, and the intended operating temperature in the range of 3.2 °C to 20.8 °C. has been reported to have an influence on the fatigue lifetime of a pseudoelastic shape-memory device. The negative effect on fatigue life increases with the temperature difference between active Af and, in case of a biomedical device, 37 °C body temperature. In this study, samples were prepared and processed in a manner to replicate aspects of the complex manufacturing process, device design, and geometry of state-of-the-art stents, and physiological loading conditions. Following explantation from the mock vessels after fatigue testing, the stents were inspected using optical microscopy to detect and document the location and number of strut fractures. The fatigue results were compared and assessed for statistical significance between the groups with various active Af temperatures. The variations in the heat treatments, as part of the manufacturing process, resulted in three distinct groups of samples with varying target active Af temperatures. These variances corresponded to differences in fatigue damage.
活性奥氏体表面温度Af与预期工作温度之间的温差在3.2°C至20.8°C之间。已被报道对假弹性形状记忆装置的疲劳寿命有影响。对疲劳寿命的负面影响随着主动Af与生物医学设备37℃体温之间的温差而增加。在这项研究中,样品的制备和处理方式复制了复杂的制造过程、设备设计、最先进支架的几何形状和生理负载条件。在疲劳测试后,从模拟血管中取出支架后,使用光学显微镜检查支架,以检测并记录支柱断裂的位置和数量。对不同活动温度组间的疲劳结果进行比较和评估,有无统计学意义。热处理的变化,作为制造过程的一部分,导致三组不同的样品具有不同的目标活性Af温度。这些差异对应于疲劳损伤的差异。
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引用次数: 0
SMAnalytics – An Automated Software for the Analysis of Shape Memory Alloy Test Data SMAnalytics -形状记忆合金测试数据分析的自动化软件
G. Bigelow, O. Benafan, Zachary D. Toom
This presentation reports on work to create user friendly software to aid in automated data analysis of tests to characterize the shape memory response of alloys. This effort has developed and produced software capable of automated analysis of test data produced using standard test methods and variations of these methods. This software provides a uniform method for analyzing data, which reduces analysis time and reduces error/variation due to different user and organization analysis methods. The software will allow analyzed data to be reported in the ASTM format for material certification, or as compiled data that can be directly imported into the NASA Shape Memory Material Database.
本报告报告了创建用户友好软件的工作,以帮助测试的自动数据分析,以表征合金的形状记忆响应。这项工作已经开发并产生了能够自动分析使用标准测试方法和这些方法的变体产生的测试数据的软件。该软件提供了统一的数据分析方法,减少了分析时间,减少了由于不同用户和组织分析方法而导致的错误/变化。该软件将允许分析数据以ASTM格式报告材料认证,或作为可直接导入NASA形状记忆材料数据库的编译数据。
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引用次数: 1
Nitinol Continuously Flat-Rolled Sheet and their Properties 镍钛诺连续轧制薄板及其性能
A. Keck, Katarzyna Plaskonka-Weisenburger, S. Knoll, J. Ulmer, A. Pelton
The continuous rolling of Nitinol alloys is a metalworking process with the ability to produce large quantities of sheet with uniform properties for the use in actuation applications in motion systems with cyclic loads. Great advantages of continuous rolling in comparison with other manufacturing methods are the cold work and heat treatment steps and their ability to influence the properties of the product and keep them in a very tight window over the width and the length of the process. Those tightly controlled properties are key-requirements to use the continuous rolled Nitinol material for subsequent automated processes like stamping in progressive dies or deep- drawing. It is also required for efficient reel-to-reel laser or EDM cutting. The primary objective of this work is to evaluate and obtain the properties of Nitinol continuously flat-rolled sheets and optimization of the process parameters by fatigue evaluation.
镍钛诺合金的连续轧制是一种金属加工工艺,能够生产大量具有均匀性能的板材,用于具有循环载荷的运动系统的驱动应用。与其他制造方法相比,连续轧制的最大优点是冷加工和热处理步骤,以及它们影响产品性能的能力,并使它们在过程的宽度和长度上保持在一个非常紧密的窗口内。这些严格控制的性能是使用连续轧制镍钛诺材料进行后续自动化加工的关键要求,如在级进模中冲压或深拉深。它也需要有效的卷对卷激光或电火花切割。本工作的主要目的是通过疲劳评价来评价和获得镍钛诺连续平轧薄板的性能,并对工艺参数进行优化。
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引用次数: 0
Elastocaloric Potential in Copper-Based SMAs through a Combinatorial Approach 基于组合方法的铜基sma弹性热势研究
G. Ouyang, Benjamin Hilliard, Jun Cui
Elastocaloric applications exploit the latent heat from a shape memory alloy (SMA) through its stress-induced phase transformation. The elastocaloric potential of a SMA depends on its latent heat, critical transformation stress, hysteresis, heat capacity and conductivity, and, most importantly, its cost-effectiveness. Increasing the latent heat and improving the transformation characteristics are critical to increasing the elastocaloric potential in copper-based SMAs, which depend heavily on their compositions and processing conditions. This paper reports on a comprehensive compositional optimization effort to maximize latent heat while maintaining the near room temperature transition window and minimizing hysteresis for copper-based SMAs. The effort uses a high throughput combinatorial approach to prepare and scan multiple samples with different compositions. The transformation characteristics of grouped samples were determined simultaneously using a novel differential thermal analysis (DTA) method via thermal imaging. Differential scanning calorimetry (DSC) was used to examine the down-selected compositions for verification.
弹性热应用利用形状记忆合金(SMA)的潜热,通过其应力诱导的相变。SMA的弹性热势取决于它的潜热、临界转变应力、滞后、热容和电导率,最重要的是,它的成本效益。增加潜热和改善相变特性是提高铜基sma弹性热势的关键,这在很大程度上取决于其成分和加工条件。本文报道了一项全面的成分优化工作,以最大限度地提高潜热,同时保持接近室温的转变窗口,并尽量减少铜基sma的滞后。该工作使用高通量组合方法制备和扫描具有不同成分的多个样品。采用一种新颖的热成像差热分析(DTA)方法同时测定了分组样品的转变特征。采用差示扫描量热法(DSC)对所选成分进行验证。
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引用次数: 0
Constitutive Model for Ni-Ti-Fe Shape Memory Alloys Exhibiting Pronounced R-Phase Transformation 具有明显r相变的Ni-Ti-Fe形状记忆合金的本构模型
M. Frost, P. Sedlák, A. Jury, L. Heller
Specific heat treatment or addition of a ternary element may induce a two-stage transformation sequence in NiTi shape memory alloys (SMA). A typical example of intermediating phases is so-called R-phase, a rhombohedral distortion of the cubic austenitic phase, which exhibits much lower transformation strain and thermal hysteresis than the subsequent transition to monoclinic martensite. In specific alloys, e.g., in NiTi slightly enriched by iron, the temperature and stress intervals in which R-phase is stable are quite broad. Hence, the influence of R-phase on the macroscopic (thermo)mechanical response should be considered when developing and designing products from these alloys. Within this context, tailored constitutive models allowing to reproduce the response in complex loading scenarios without additional experimental effort can be extremely beneficial. This paper presents an enhanced constitutive model for NiTi SMA featuring the R-phase transition. The model recognizes R-phase as a distinct phase, respects the coupled influence of stress and temperature on any phase transformation, and covers reorientation (reconfiguration) of both martensite and R-phase with applied stress. The core of the model consists of two material functions: one captures the energy stored in the material at a given thermodynamic state, the other defines the energy released during dissipative processes, which are considered rate-independent. The model was validated through a direct comparison of experimental tests (isothermal tensile tests, isobaric thermal tests, recovery stress tests) with simulated counterparts.
特定热处理或三元元素的加入可诱导NiTi形状记忆合金(SMA)的两阶段转变序列。中间相的一个典型例子是所谓的r相,它是立方奥氏体相的一种菱形变形,与随后向单斜马氏体的转变相比,它表现出更低的转变应变和热滞后。在特定的合金中,例如在少量富铁的NiTi中,r相稳定的温度和应力区间相当宽。因此,在开发和设计这些合金的产品时,应考虑r相对宏观(热)力学响应的影响。在这种情况下,量身定制的本构模型可以在没有额外实验的情况下重现复杂加载场景下的响应,这是非常有益的。提出了一种具有r相变的NiTi SMA增强本构模型。该模型承认r相是一个独立的相,尊重应力和温度对任何相变的耦合影响,并涵盖了马氏体和r相在外加应力作用下的重取向(重配置)。该模型的核心由两个材料函数组成:一个捕获在给定热力学状态下储存在材料中的能量,另一个定义在耗散过程中释放的能量,这被认为是速率无关的。通过将实验测试(等温拉伸测试、等压热测试、恢复应力测试)与模拟测试进行直接比较,验证了该模型。
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引用次数: 0
Compression Behaviors of Different Geometry-Designed NiTi Refrigerants 不同几何形状设计的NiTi制冷剂的压缩性能
Guoan Zhou, Q. Sun
A promising elastocaloric cooling technology (one of the solid-state cooling technologies) does not require any potentially harmful vaporous refrigerants. Its basic working principle, the martensitic transformation and its reverse transformation of shape memory alloys (SMAs) such as NiTi, NiTiCu, and NiFeGaC is one of the first-order non-diffusible phase transitions between a high-temperature phase (the austenite phase) of a B2 cubic structure and a low-temperature phase (the martensite phase) of a B19' monoclinic structure. This paper investigates the compression behaviors of different NiTi regenerator structures through fatigue tests. An optimized 3-layer sample shows promise to be used in elastocaloric cooling prototypes and gives insight into the structural optimization of regenerators.
一种很有前途的弹性热冷却技术(固态冷却技术之一)不需要任何潜在有害的蒸汽制冷剂。NiTi、NiTiCu和NiFeGaC等形状记忆合金(sma)的马氏体相变及其反向相变的基本工作原理是B2立方结构的高温相(奥氏体相)和B19'单斜结构的低温相(马氏体相)之间的一级非扩散相变。通过疲劳试验研究了不同镍钛再生结构的压缩性能。优化后的三层样品有望用于弹性热冷却原型,并为蓄热器的结构优化提供了见解。
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引用次数: 0
Shape Memory Alloy Actuated Vortex Generators: Development and Flight Test 形状记忆合金驱动涡发生器:研制和飞行试验
F. Calkins, D. Nicholson, A. Fassmann, P. Vijgen, Christopher Yeeles, O. Benafan, G. Bigelow, D. Gaydosh
Conventional vortex generators (VG) in aeronautical applications are static vanes mounted on aircraft surfaces used to improve aircraft efficiency during low speed operations. However, during the cruise phase of flight, these static devices are always deployed and produce drag penalties. With the goal of improving aircraft efficiency, Boeing in collaboration with NASA Glen Research Center have developed and successfully flight tested environmentally activated SMART-VGs that repeatedly and accurately retract during cruise and deploy during take- off and landing. This application is distinctively enabled by the ability of shape memory alloy (SMA) actuation to produce large work outputs in compact volumes and operate as both a sensor and actuator. The SMART-VG project highlighted here was built upon recent advancements in SMA rotary actuation technology that included improved alloy systems, design tools, best practices, published standards and high-level wind tunnel and flight test demonstrations. This program successfully matured and validated the targeted alloy development and associated design processes in a unique way by demonstrating shape memory alloy reconfigurable technology (SMART) in-flight. The data from this flight test is being used to optimize a next generation design of the SMART-VGs that will be tested in 2022.
航空应用中的传统涡发生器(VG)是安装在飞机表面的静态叶片,用于提高飞机在低速运行时的效率。然而,在飞行的巡航阶段,这些静态装置总是被部署并产生阻力。为了提高飞机效率,波音公司与美国宇航局格伦研究中心合作开发了环境激活的smart - vg,并成功进行了飞行测试,该系统可以在巡航过程中反复准确地缩回,并在起飞和降落过程中展开。该应用的独特之处在于形状记忆合金(SMA)的驱动能力,可以在紧凑的体积中产生大的工作输出,同时可以作为传感器和执行器。SMART-VG项目建立在SMA旋转驱动技术的最新进展基础上,包括改进的合金系统、设计工具、最佳实践、发布的标准以及高水平风洞和飞行测试演示。该项目通过在飞行中展示形状记忆合金可重构技术(SMART),以独特的方式成功成熟并验证了目标合金开发和相关设计过程。此次飞行试验的数据将用于优化下一代smart - vg的设计,该设计将于2022年进行测试。
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引用次数: 1
The Coefficient of Refrigeration Performance and Stress-Assisted Magnetocaloric Effect in Meta-Magnetic Shape Memory Alloys 超磁形状记忆合金的制冷性能系数及应力辅助磁热效应
N. Bruno
Meta-magnetic shape memory alloys (MMSMAs) exhibit multi-physical couplings across a reversible first-order martensitic transition which leads to their potential applications in solid-state cooling, thermally or magnetically driven precision actuation, energy harvesting, and magnetic memory storage. Through their magneto-structural transitions and simultaneous transformation latent heat, MMSMAs are capable of the magnetocaloric effect (MCE) at two distinct operating temperatures (i.e., the critical martensitic transformation temperature and the ferromagnetic Curie point of either the austenite or martensite phase). In this study, the Refrigeration Capacity (RC) and Coefficient of Refrigeration Performance (CRP) in MMSMAs are shown to depend on the critical martensite transformation temperatures and, by extension, uniaxial mechanical stress. A loading sequence, namely the stress-assisted magnetic field-induced phase transformation (SAMFIT) is described, whereby mechanical stress and magnetic field are applied to an MMSMA specimen in sequence to effectively increase the thermal operating range and CRP for a single MMSMA composition.
超磁形状记忆合金(mmsma)在可逆的一阶马氏体转变中表现出多物理耦合,这使得它们在固态冷却、热或磁驱动的精密驱动、能量收集和磁记忆存储方面具有潜在的应用前景。通过其磁结构转变和同步转变潜热,mmsma能够在两个不同的工作温度下(即临界马氏体转变温度和奥氏体或马氏体相的铁磁居里点)产生磁热效应。在这项研究中,mmsma的制冷能力(RC)和制冷性能系数(CRP)取决于临界马氏体转变温度,进而取决于单轴机械应力。本文描述了一种加载顺序,即应力辅助磁场诱导相变(SAMFIT),即依次对MMSMA试样施加机械应力和磁场,以有效地增加单一MMSMA成分的热工作范围和CRP。
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引用次数: 0
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SMST 2022: Extended Abstracts from the International Conference on Shape Memory and Superelastic Technologies
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