Pub Date : 2018-04-24DOI: 10.30526/2017.IHSCICONF.1788
K. Al-Badri
High Q-factor based on absorption can be achieved by tuning (the reflection and the transition percentage). In this work, the simple design and simulated in S-band have been investigated. The simulation results of G-shape resonator are shown triple band of absorption peaks 60%, 91.5%, and 70.3%) at resonance frequency 2.7 GHz, 3.26 GHz, and 4.05 GHz respectively. The results exhibited very high of the Q-factor ( 271 ) at resonance frequency ( 3.26 GHz ). The high Q-factor can be used to enhance the sensor sensing, narrowband band filter and image sensing.
{"title":"Very High Q-Factor Based On G-Shaped Resonator Type Metamaterial Absorber","authors":"K. Al-Badri","doi":"10.30526/2017.IHSCICONF.1788","DOIUrl":"https://doi.org/10.30526/2017.IHSCICONF.1788","url":null,"abstract":"High Q-factor based on absorption can be achieved by tuning (the reflection and the transition percentage). In this work, the simple design and simulated in S-band have been investigated. The simulation results of G-shape resonator are shown triple band of absorption peaks 60%, 91.5%, and 70.3%) at resonance frequency 2.7 GHz, 3.26 GHz, and 4.05 GHz respectively. The results exhibited very high of the Q-factor ( 271 ) at resonance frequency ( 3.26 GHz ). The high Q-factor can be used to enhance the sensor sensing, narrowband band filter and image sensing.","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"148 1","pages":"159-166"},"PeriodicalIF":0.0,"publicationDate":"2018-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"72676571","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-24DOI: 10.30526/2017.IHSCICONF.1794
Taghreed M. Musa, M. Al-Jibouri, B. F. Abbas
The present paper describes the synthesis and structural studies of new transition metal complexes of cobalt(II), nickel(II), copper(II) and cadmium(II) with two bi dentate ligands derived from quinoxaline-2,3-dione. The two ligands were fully identified by elemental analyses, FT-IR, NMR and UV-Visible spectra. The metal complexes of Co(II), Ni(II), Cu(II) and Cd(II) were isolated in the solid state after reactions of their metal chlorides with the ligands in 2:1 mole ratio. The isolated solid metal complexes were characterized with the help of elemental analyses, NMR, FT-IR and UV-Visible spectra. As well as the thermal stability of the coordinated quinoxaline polymers were tested by TG-DSC analysis and it is found that cleavage of terminal moiety was investigated, the strong coordinated bonds between oxygen donor atoms in L1 while nitrogen donor atoms of quinoxaline ring in the L2 with the metal ions. Furthermore, the thermal stability of cobalt(II), nickel(II), copper(II) and Cd(II) complexes were screened by TG-DSC analysis and the results helped us in the investigation of the proposed structure of the prepared complexes in the formula [M(L)2Cl2].XH2O and [Cd(L)2]Cl2 where L= L1 and L2 ligands derived from quinoxaline-2,3-dione.
{"title":"Synthesis, Characterization and Thermal Study of Some Transition Metal Complexes Derived from Quinoxaline-2,3-Dione","authors":"Taghreed M. Musa, M. Al-Jibouri, B. F. Abbas","doi":"10.30526/2017.IHSCICONF.1794","DOIUrl":"https://doi.org/10.30526/2017.IHSCICONF.1794","url":null,"abstract":"The present paper describes the synthesis and structural studies of new transition metal complexes of cobalt(II), nickel(II), copper(II) and cadmium(II) with two bi dentate ligands derived from quinoxaline-2,3-dione. The two ligands were fully identified by elemental analyses, FT-IR, NMR and UV-Visible spectra. The metal complexes of Co(II), Ni(II), Cu(II) and Cd(II) were isolated in the solid state after reactions of their metal chlorides with the ligands in 2:1 mole ratio. The isolated solid metal complexes were characterized with the help of elemental analyses, NMR, FT-IR and UV-Visible spectra. As well as the thermal stability of the coordinated quinoxaline polymers were tested by TG-DSC analysis and it is found that cleavage of terminal moiety was investigated, the strong coordinated bonds between oxygen donor atoms in L1 while nitrogen donor atoms of quinoxaline ring in the L2 with the metal ions. Furthermore, the thermal stability of cobalt(II), nickel(II), copper(II) and Cd(II) complexes were screened by TG-DSC analysis and the results helped us in the investigation of the proposed structure of the prepared complexes in the formula [M(L)2Cl2].XH2O and [Cd(L)2]Cl2 where L= L1 and L2 ligands derived from quinoxaline-2,3-dione.","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"14 1","pages":"206-220"},"PeriodicalIF":0.0,"publicationDate":"2018-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73182979","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-24DOI: 10.30526/2017.ihsciconf.1800
Shaima Ibrahim Chyad Al-khazraji, B. Mohammed, S. AL-Salihi
The objective of this study is to test In Vitro the twenty chemical compounds that contains Schiff base or oxazepine, indoline, imidazolo units in concentrations( 50, 100, 150) mg / dl as antifungal activity, against three pathogenic Candida species that occur in humans. We tested one isolates of ) Candida albicans ,Candida glabrata and Candida krusei). All these species affect human health . The study was carried out in the Laboratory of Public Health , directly of health for the period from May 2016 to April 2017 , Candida spp isolates used in this study were collected from patients admitted at some private clinical in Kirkuk city . All isolates were identified using CHROM agar and stored at -70 0C. Preparation of Schiff base ( 1-7 ) from amino pyridine derivatives with aromatic aldehyde by nucleophilic addition reactions preparation of 1,3 – oxazepine 4,7 – dione ( 8-13 ) were carried out by cyclization of appropriate Schiff bases with malic anhydride and phthalic anhydride , preparation of compounds ( 14 – 17) from reaction of a mixture aminopyridine derivative with potassium hydroxide then chloroacetic acid was added , preparation of compounds ( 18 – 20 ) from reaction of amino pyridine derivative and 4- phenyl phenacyl bromide , all these compounds were characterized by melting points and FT.IR spectroscopy. Some of them were characterized by H1- NMR and C13-NMR spectroscopy .Some compounds contain Schiff base group in compounds ( 1-7) showed inhibitory effect Candida albicans and Candida krusei .This study demonstrates that the three Candida species were resistant to a range of compounds (8-13) containing oxazepine and as antifungal against , while the compound(14-17) contain Indolin show low inhabition zon for Candida albicans and the compound (18-20) contain imidazo group showed inhibited effect against three Candida species.
{"title":"Synthesis and Antifungal Activity Against of Candida Species for Some New Heterocyclic Compounds Containing Schiff Base , Oxazepine , Indoline or Imidazolo Units and Their Spectral Characterization","authors":"Shaima Ibrahim Chyad Al-khazraji, B. Mohammed, S. AL-Salihi","doi":"10.30526/2017.ihsciconf.1800","DOIUrl":"https://doi.org/10.30526/2017.ihsciconf.1800","url":null,"abstract":"The objective of this study is to test In Vitro the twenty chemical compounds that contains Schiff base or oxazepine, indoline, imidazolo units in concentrations( 50, 100, 150) mg / dl as antifungal activity, against three pathogenic Candida species that occur in humans. We tested one isolates of \u0000 ) Candida albicans ,Candida glabrata and Candida krusei). All these species affect human health . The study was carried out in the Laboratory of Public Health , directly of health for the period from May 2016 to April 2017 , Candida spp isolates used in this study were collected from patients admitted at some private clinical in Kirkuk city . All isolates were identified using CHROM agar and stored at -70 0C. Preparation of Schiff base ( 1-7 ) from amino pyridine derivatives with aromatic aldehyde by nucleophilic addition reactions preparation of 1,3 – oxazepine 4,7 – dione ( 8-13 ) were carried out by cyclization of appropriate Schiff bases with malic anhydride and phthalic anhydride , preparation of compounds ( 14 – 17) from reaction of a mixture aminopyridine derivative with potassium hydroxide then chloroacetic acid was added , preparation of compounds ( 18 – 20 ) from reaction of amino pyridine derivative and 4- phenyl phenacyl bromide , all these compounds were characterized by melting points and FT.IR spectroscopy. Some of them were characterized by H1- NMR and C13-NMR spectroscopy .Some compounds contain Schiff base group in compounds \u0000( 1-7) showed inhibitory effect Candida albicans and Candida krusei .This study demonstrates that the three Candida species were resistant to a range of compounds (8-13) containing oxazepine and as antifungal against , while the compound(14-17) contain Indolin show low inhabition zon for Candida albicans and the compound (18-20) contain imidazo group showed inhibited effect against three Candida species.","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"15 1","pages":"273-293"},"PeriodicalIF":0.0,"publicationDate":"2018-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80775797","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-24DOI: 10.30526/2017.IHSCICONF.1793
S. Al-Taweel, S. Isa, R. Al-Ani
The adsorption of cephalexin.H2O from aqueous solution on attapulgite, bentonite and kaolin has been studied at the human body temperature (37.5˚C) and at 5, 27, 47˚C in 0.1M hydrochloric acid (pH 1.2). The value of pH 1.2 has been chosen to simulate the pH of stomach fluid. The clays show the following order: Bentonite > attapulgite > kaolin, for their activity to adsorb cephalexin.H2O. The charged clay particles can attract molecules either by electrostatic forces, for the molecules of oppositely charged, or by inducing dipole formation in the neutral molecule. The L-shaped adsorption isotherm indicated that drug molecules arrangement in a flat geometry on the clay surface. The results indicated the applicability of Langmuir isotherm for adsorption of drug on three clays. The amount of cephalexin.H2O adsorbed on the three clays was increased with increasing pH value from 1.2 to 5. At the acidic pH, the competition between cephalexin.H2O molecules and hydronium ions results in a reduction in adsorption process. At fixed temperature and pH, the adsorption of cephalexin.H2O on the three clays was increased with increasing the ionic strength of solution. The data showed a little increase in the amount of drug adsorbed by attapulgite and bentonite with increasing temperature, so the adsorption process appeared endothermic. The reverse was observed with adsorption of cephalexin.H2O on kaolin surface (exothermic).The extent of desorption of cephalexin.H2O from the clays increased when the concentration of drug increased. This result may refer to the difficulty of desorption of the drug at low concentrations, which reflects a relatively higher adsorbate - adsorbent interaction.
{"title":"Three Locally Clays as A Surfaces for Adsorption of Cephalexin Monohydrate From Aqueous Solution: Thermodynamic and Desorption Equilibrium","authors":"S. Al-Taweel, S. Isa, R. Al-Ani","doi":"10.30526/2017.IHSCICONF.1793","DOIUrl":"https://doi.org/10.30526/2017.IHSCICONF.1793","url":null,"abstract":"The adsorption of cephalexin.H2O from aqueous solution on attapulgite, bentonite and kaolin has been studied at the human body temperature (37.5˚C) and at 5, 27, 47˚C in 0.1M hydrochloric acid (pH 1.2). The value of pH 1.2 has been chosen to simulate the pH of stomach fluid. The clays show the following order: Bentonite > attapulgite > kaolin, for their activity to adsorb cephalexin.H2O. The charged clay particles can attract molecules either by electrostatic forces, for the molecules of oppositely charged, or by inducing dipole formation in the neutral molecule. The L-shaped adsorption isotherm indicated that drug molecules arrangement in a flat geometry on the clay surface. The results indicated the applicability of Langmuir isotherm for adsorption of drug on three clays. The amount of cephalexin.H2O adsorbed on the three clays was increased with increasing pH value from 1.2 to 5. At the acidic pH, the competition between cephalexin.H2O molecules and hydronium ions results in a reduction in adsorption process. At fixed temperature and pH, the adsorption of cephalexin.H2O on the three clays was increased with increasing the ionic strength of solution. The data showed a little increase in the amount of drug adsorbed by attapulgite and bentonite with increasing temperature, so the adsorption process appeared endothermic. The reverse was observed with adsorption of cephalexin.H2O on kaolin surface (exothermic).The extent of desorption of cephalexin.H2O from the clays increased when the concentration of drug increased. This result may refer to the difficulty of desorption of the drug at low concentrations, which reflects a relatively higher adsorbate - adsorbent interaction.","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"93 1","pages":"195-205"},"PeriodicalIF":0.0,"publicationDate":"2018-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85145769","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-24DOI: 10.30526/2017.IHSCICONF.1799
Aesha Sh. Sh. Baban, Sabah H. Korsheed, A. Y. A. Hayawi
Polycystic ovary syndrome (PCOS) is an endocrine disorder in women during fertilization age that reflects changing clinical symptoms. The genetic concept of PCOS is unclear and no significant genetic association with PCOS has been established. The level of Follicle stimulating hormone FSH is encoded by FSH receptor (FSHR) and abnormal FSHR affects follicle cogenesis and ovary and consist of 9 introns, 10 exons, and the region of chromosome promoter at 2p21. Sample of 93PCOS patients and 52 controls were collected from Province of Erbil in north of Iraq. Genomic DNA was extracted from the blood and genotype dissected was improved for the two population of study using PCR-RFLP with the restriction enzyme Eam1105I. The genotype distributions and allele frequency of Ala307Thr polymorphisms of FSHR were not statistically various between the controls and the PCOS patients. Significant elevation of body mass index with all genotype of PCOS was found when compared with controls. There were statistical differences in the BMI and most of the serum hormone and lipid profile parameters including LH, total testosterone, fasting glucose, Cholesterol, HDL and LDL, there were significant various in FSH and LH levels of hormones and HDL, LDL and VLDL with PCOS group conveying different genotypes of Ala307Thr polymorphisms. The variant of Ala307Thr was not associated with PCOS in Kurdistan women; there was no relationship between the POCS and gene of FSHR polymorphism at codons 307. There was a significant difference in FSH and LH levels with PCOS patients conveying different genotypes of Ala307Thr polymorphism.
{"title":"The FSHR Polymorphisms Association With Polycystic Ovary Syndrome in Women of Erbil, Kurdistan in North of Iraq","authors":"Aesha Sh. Sh. Baban, Sabah H. Korsheed, A. Y. A. Hayawi","doi":"10.30526/2017.IHSCICONF.1799","DOIUrl":"https://doi.org/10.30526/2017.IHSCICONF.1799","url":null,"abstract":"Polycystic ovary syndrome (PCOS) is an endocrine disorder in women during fertilization age that reflects changing clinical symptoms. The genetic concept of PCOS is unclear and no significant genetic association with PCOS has been established. The level of Follicle stimulating hormone FSH is encoded by FSH receptor (FSHR) and abnormal FSHR affects follicle cogenesis and ovary and consist of 9 introns, 10 exons, and the region of chromosome promoter at 2p21. Sample of 93PCOS patients and 52 controls were collected from Province of Erbil in north of Iraq. Genomic DNA was extracted from the blood and genotype dissected was improved for the two population of study using PCR-RFLP with the restriction enzyme Eam1105I. The genotype distributions and allele frequency of Ala307Thr polymorphisms of FSHR were not statistically various between the controls and the PCOS patients. Significant elevation of body mass index with all genotype of PCOS was found when compared with controls. There were statistical differences in the BMI and most of the serum hormone and lipid profile parameters including LH, total testosterone, fasting glucose, Cholesterol, HDL and LDL, there were significant various in FSH and LH levels of hormones and HDL, LDL and VLDL with PCOS group conveying different genotypes of Ala307Thr polymorphisms. The variant of Ala307Thr was not associated with PCOS in Kurdistan women; there was no relationship between the POCS and gene of FSHR polymorphism at codons 307. There was a significant difference in FSH and LH levels with PCOS patients conveying different genotypes of Ala307Thr polymorphism.","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"52 1","pages":"257-272"},"PeriodicalIF":0.0,"publicationDate":"2018-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80368711","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-24DOI: 10.30526/2017.IHSCICONF.1789
A. K. Ali, Nihad Ali Shafeek
{"title":"Fabrication and study the effect of the laser on the properties of the compound Tl2-xHgxBa2-ySryCa2Cu3O10+δ superconductor","authors":"A. K. Ali, Nihad Ali Shafeek","doi":"10.30526/2017.IHSCICONF.1789","DOIUrl":"https://doi.org/10.30526/2017.IHSCICONF.1789","url":null,"abstract":"","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"22 1","pages":"168"},"PeriodicalIF":0.0,"publicationDate":"2018-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88885204","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-24DOI: 10.30526/2017.ihsciconf.1801
Saja S Al-Samarra’ay, I. Al-Hitti, Omur H Al-oubaydi
It was confirmed in this research that the ligand calcichrome formed stable complex with calcium ion at pH of 8.5 which verified by UV/Vis and FTIR spectral analysis and the complexation occurred via hydroxyl groups. The stoichiometric ratio of the formed complex was found to be 1:1 by mole ratio and continuous variation methods. Dry ashing method of the complex and flame emission photometric analysis offered a calcium percentage in calcium complex equal 4.5% with an error of 2.41% due to experimental errors. Keyword: Calcichrome, Stoichiometry, Mole ration method, Continuous Variation method, Selective reagent. IHSCICONF 2017 Special Issue Ibn Al-Haitham Journal for Pure and Applied science https://doi.org/ 10.30526/2017.IHSCICONF.1801 For more information about the Conference please visit the websites: http://www.ihsciconf.org/conf/ www.ihsciconf.org Chemistry |322
本研究通过紫外/可见光谱和红外光谱分析证实了配体钙铬酸盐在pH为8.5时与钙离子形成稳定的配合物，并通过羟基进行络合。通过摩尔比法和连续变分法，发现所形成的络合物的化学计量比为1:1。配合物的干灰化法和火焰发射光度法分析表明，配合物中钙的含量为4.5%，由于实验误差，误差为2.41%。关键词:钙铬，化学计量，摩尔比法，连续变分法，选择性试剂。IHSCICONF 2017特刊Ibn Al-Haitham Journal for Pure and Applied science https://doi.org/ 10.30526/2017.IHSCICONF.1801有关会议的更多信息，请访问以下网站:http://www.ihsciconf.org/conf/ www.ihsciconf.org Chemistry |322
{"title":"Spectrophotometric and Potentiometric Analysis of Calcichrome and Its Complex With Calcium Ion","authors":"Saja S Al-Samarra’ay, I. Al-Hitti, Omur H Al-oubaydi","doi":"10.30526/2017.ihsciconf.1801","DOIUrl":"https://doi.org/10.30526/2017.ihsciconf.1801","url":null,"abstract":"It was confirmed in this research that the ligand calcichrome formed stable complex with calcium ion at pH of 8.5 which verified by UV/Vis and FTIR spectral analysis and the complexation occurred via hydroxyl groups. The stoichiometric ratio of the formed complex was found to be 1:1 by mole ratio and continuous variation methods. Dry ashing method of the complex and flame emission photometric analysis offered a calcium percentage in calcium complex equal 4.5% with an error of 2.41% due to experimental errors. Keyword: Calcichrome, Stoichiometry, Mole ration method, Continuous Variation method, Selective reagent. IHSCICONF 2017 Special Issue Ibn Al-Haitham Journal for Pure and Applied science https://doi.org/ 10.30526/2017.IHSCICONF.1801 For more information about the Conference please visit the websites: http://www.ihsciconf.org/conf/ www.ihsciconf.org Chemistry |322","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"19 1","pages":"323"},"PeriodicalIF":0.0,"publicationDate":"2018-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81940285","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-24DOI: 10.30526/2017.IHSCICONF.1795
H. Ali, Sumayha muhammed
Simple and rapid spectrophotometric determination of furosemide (FUR) has been investigated .The method is based on acid hydrolysis of FUR to free primary aromatic amine and diazotization followed by coupling with 3, 5 di methyl phenol (3, 5-DMPH) at basic medium. The absorbance was measured at 434 nm, the method was optimized for best condition, and beers’ law is obeyed over the range of 0.4-50 µg.mL-1 with molar absorptivity and sandal’s sensitivity 1.3899 x104 L moL-1 .cm-1 and 0.0238x104 µg.cm-2 respectively. Analysis of solution containing nineteen different concentrations of FUR gave a correlation coefficient of (0.9999) and limit of detection, limit of quantitation were 0.127, 0.464µg.mL-1 respectively. The reaction stoichiometry was evaluated by Job’s and mole ratio method was found to be 1:1(diazotized FUR: 3, 5-DMPH) .The method was applied in synthetic urine and pharmaceutical formulation. The recovery of FUR in spiked urine was satisfactory resulting in the values of (99±3.32) %, the results of the suggested method was compared with available official literature method.
{"title":"Use of Acidic Hydrolysis and Diazo Coupling Reaction for Spectrophotometric Determination of Furosemide in Urine and Pharmaceutical Formulation.","authors":"H. Ali, Sumayha muhammed","doi":"10.30526/2017.IHSCICONF.1795","DOIUrl":"https://doi.org/10.30526/2017.IHSCICONF.1795","url":null,"abstract":"Simple and rapid spectrophotometric determination of furosemide (FUR) has been investigated .The method is based on acid hydrolysis of FUR to free primary aromatic amine and diazotization followed by coupling with 3, 5 di methyl phenol (3, 5-DMPH) at basic medium. The absorbance was measured at 434 nm, the method was optimized for best condition, and beers’ law is obeyed over the range of 0.4-50 µg.mL-1 with molar absorptivity and sandal’s sensitivity 1.3899 x104 L moL-1 .cm-1 and 0.0238x104 µg.cm-2 respectively. Analysis of solution containing nineteen different concentrations of FUR gave a correlation coefficient of (0.9999) and limit of detection, limit of quantitation were 0.127, 0.464µg.mL-1 respectively. The reaction stoichiometry was evaluated by Job’s and mole ratio method was found to be 1:1(diazotized FUR: 3, 5-DMPH) .The method was applied in synthetic urine and pharmaceutical formulation. The recovery of FUR in spiked urine was satisfactory resulting in the values of (99±3.32) %, the results of the suggested method was compared with available official literature method.","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"9 1","pages":"221-234"},"PeriodicalIF":0.0,"publicationDate":"2018-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75797925","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-23DOI: 10.30526/2017.IHSCICONF.1765
R. Hussein, A. Hussein
Diarrhea is an important public health problem worldwide, several causes associated with diarrhea especially in population live under poverty and unsafe water use. Different methods are available and use in diagnosis. This study was carried out to compare of various techniques for Giardia lamblia detection and study the association with E coil and Shigella in patients with diarrhea. A total of 100 children with diarrhoea were enrolled into the study, 57 were males and 43 were females, aged from 2 months -16 years were attendant to AL-Imamin AL-Kadhimin Medical City, during the period from May 2014 to February 2015. Stool samples were collected and analysed for Giardia lamblia presence by used light microscopy, enzyme linked immunosorbant assay and polymerase chain reaction as well as used bacterial culture and one-step colored chromatographic immunoassay for E coil and Shigella detection. Socio-demographic features of the study subjects were also included. Parasitic infection was the most common than bacterial infection. Most intestinal infection were recorded in age group 5-10 years and among males. Comparative analysis of various techniques for Giardia lamblia detection show that microscopy detected only 24 cases, while enzyme linked immunosorbant assay detected 32 cases. However, polymerase chain reaction assay detected 42 cases. Statistical analysis showed significant differences. The sensitivities was 57.14% for microscopy and 76.19% for enzyme linked immunosorbant assay, whereas polymerase chain reaction assay had sensitivity of 100% (42/42) and specificity was100%. Bacterial culture and immunochromatography assay show positive result for E. coli (12%), and Shigella (6%). Co-infection between three microorganisms which revealed that 5 patients with Giardia lamblia positive test had co-infection with E. coli and 4 patients with Giardia lamblia positive test had co-infection with Shigella. Polymerase chain reaction highly sensitive and specific than other methods for Giardia lamblia detection, direct examination exhibited many false positive and negative results with parasitic infection.
{"title":"Comparative Analysis of Various Techniques for Giardia lamblia Detection and Association with E coil and Shigella Among Children Attending AL-Imamin AL-Kadhimin Medical City","authors":"R. Hussein, A. Hussein","doi":"10.30526/2017.IHSCICONF.1765","DOIUrl":"https://doi.org/10.30526/2017.IHSCICONF.1765","url":null,"abstract":"Diarrhea is an important public health problem worldwide, several causes associated with diarrhea especially in population live under poverty and unsafe water use. Different methods are available and use in diagnosis. This study was carried out to compare of various techniques for Giardia lamblia detection and study the association with E coil and Shigella in patients with diarrhea. A total of 100 children with diarrhoea were enrolled into the study, 57 were males and 43 were females, aged from 2 months -16 years were attendant to AL-Imamin AL-Kadhimin Medical City, during the period from May 2014 to February 2015. Stool samples were collected and analysed for Giardia lamblia presence by used light microscopy, enzyme linked immunosorbant assay and polymerase chain reaction as well as used bacterial culture and one-step colored chromatographic immunoassay for E coil and Shigella detection. Socio-demographic features of the study subjects were also included. Parasitic infection was the most common than bacterial infection. Most intestinal infection were recorded in age group 5-10 years and among males. Comparative analysis of various techniques for Giardia lamblia detection show that microscopy detected only 24 cases, while enzyme linked immunosorbant assay detected 32 cases. However, polymerase chain reaction assay detected 42 cases. Statistical analysis showed significant differences. The sensitivities was 57.14% for microscopy and 76.19% for enzyme linked immunosorbant assay, whereas polymerase chain reaction assay had sensitivity of 100% (42/42) and specificity was100%. Bacterial culture and immunochromatography assay show positive result for E. coli (12%), and Shigella (6%). Co-infection between three microorganisms which revealed that 5 patients with Giardia lamblia positive test had co-infection with E. coli and 4 patients with Giardia lamblia positive test had co-infection with Shigella. Polymerase chain reaction highly sensitive and specific than other methods for Giardia lamblia detection, direct examination exhibited many false positive and negative results with parasitic infection.","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"241 1","pages":"1-11"},"PeriodicalIF":0.0,"publicationDate":"2018-04-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75760622","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2018-04-23DOI: 10.30526/2017.IHSCICONF.1782
A. A. Al-Tae, A. L. Al-Rubaie
The literature reviews of all reports of parasites fauna cats Felis catus in Iraq species of including 15 protozoa (Babesia spp., Crptosporidium spp., C. muris, C. parvum, Cytauxzoon felis, Eimeria cati, Entamoeba spp., Giardia sp., Giardia spp., Isospora ssp., I. felis., I. rivolta, Leishmania tropica and Toxoplasma gondii), five trematoda (Heterophyes aequalis, H. heterophyes, Opisthorchis felineus, O. tenuicollis and Paragonimus killicotti), 17 cestoda (Diphyllobothrium sp., D. latum, Diplopylidium acanthotetra, D. nolleri, Dipylidium spp., D. caninum, D. sexcoronatum, Hydatigera taeniaeformis, Joyeuxiella echinorhyncoides, J. pasqualei, Mesocestoides variabilis, Spirometra sp., S. erinaceieuropaei, S. mansonoides, Taenia sp., Taenia spp. and T. taeniaeformis), 18 nematoda) Aelurostrongylus abstrusus, Ancylostoma spp., A. paraduodenale, A. tubaeforme, Capillaria spp., C. arophilia, C. felis, Dioctophyma renale, Dirofilaria immitis, Ganathostoma sp., Ollulanus tricuspis, Physaloptera praeputiale, Pterygodermatites cahirensis, Rictularia cahirensis, Strongyloides spp., Toxascaris leonine, Toxocara sp. and T. cati) and seven arthropoda (Ctenocephalides felis, Felicola subrostratus, Ixodes spp., Otodectes cynotis, Rhipicephalus sp., R. sanguineus and R. turanicus).
{"title":"Checklists of Parasites Stray Cats Felis Catus of Iraq","authors":"A. A. Al-Tae, A. L. Al-Rubaie","doi":"10.30526/2017.IHSCICONF.1782","DOIUrl":"https://doi.org/10.30526/2017.IHSCICONF.1782","url":null,"abstract":"The literature reviews of all reports of parasites fauna cats Felis catus in Iraq species of including 15 protozoa (Babesia spp., Crptosporidium spp., C. muris, C. parvum, Cytauxzoon felis, Eimeria cati, Entamoeba spp., Giardia sp., Giardia spp., Isospora ssp., I. felis., I. rivolta, Leishmania tropica and Toxoplasma gondii), five trematoda (Heterophyes aequalis, H. heterophyes, Opisthorchis felineus, O. tenuicollis and Paragonimus killicotti), 17 cestoda (Diphyllobothrium sp., D. latum, Diplopylidium acanthotetra, D. nolleri, Dipylidium spp., D. caninum, D. sexcoronatum, Hydatigera taeniaeformis, Joyeuxiella echinorhyncoides, J. pasqualei, Mesocestoides variabilis, Spirometra sp., S. erinaceieuropaei, S. mansonoides, Taenia sp., Taenia spp. and T. taeniaeformis), 18 nematoda) Aelurostrongylus abstrusus, Ancylostoma spp., A. paraduodenale, A. tubaeforme, Capillaria spp., C. arophilia, C. felis, Dioctophyma renale, Dirofilaria immitis, Ganathostoma sp., Ollulanus tricuspis, Physaloptera praeputiale, Pterygodermatites cahirensis, Rictularia cahirensis, Strongyloides spp., Toxascaris leonine, Toxocara sp. and T. cati) and seven arthropoda (Ctenocephalides felis, Felicola subrostratus, Ixodes spp., Otodectes cynotis, Rhipicephalus sp., R. sanguineus and R. turanicus).","PeriodicalId":13236,"journal":{"name":"Ibn Al-Haitham Journal For Pure And Applied Science","volume":"17 1","pages":"143-151"},"PeriodicalIF":0.0,"publicationDate":"2018-04-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91529808","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
京公网安备 11010802042870号
京ICP备2023020795号-1
扫码关注我们
求助内容：
应助结果提醒方式：