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Determination of viscosity and critical concentrations of commercial low methoxyl pectin 商品低甲氧基果胶粘度和临界浓度的测定
4区 农林科学 Pub Date : 2023-09-15 DOI: 10.1515/ijfe-2023-0058
Eko Hari Purnomo, Uray Ulfah Nabilah, Azis Boing Sitanggang
Abstract Determining viscosity and critical concentrations is essential for industrial application of pectin solution. Critical concentration can be determined rheologically based on zero shear viscosity , apparent viscosity, specific viscosity, and consistency index of dilute polymer solution. Direct experimental comparison of the aforementioned methods for critical concentration determination is still lacking. Therefore, this study aims to experimentally compare different viscosity methods to determine critical concentration of three different pectin solutions (sun flower, citrus, and apple). The three pectin sources at concentrations of 0.1–3.0 % (w/v) showed Newtonian to shear thinning behavior. The critical concentration ranges of pectin, from the lowest to highest, was sunflower (0.6792−0.9589 % (w/v)), citrus (0.7172−1.0347 % (w/v)), and apple (0.7645−1.1233 % (w/v)). Critical concentration determined based on consistency index was relatively close to the result obtained from zero shear viscosity. Whereas critical concentrations of the pectin solutions determined from specific viscosity and apparent viscosity were significantly different from critical concentration determined from zero shear viscosity.
摘要测定果胶溶液的粘度和临界浓度是果胶工业应用的关键。临界浓度可以根据零剪切粘度、表观粘度、比粘度和稀聚合物溶液的稠度指数从流变学角度确定。目前还缺乏对上述临界浓度测定方法的直接实验比较。因此,本研究旨在通过实验比较不同的粘度方法来确定三种不同果胶溶液(向日葵、柑橘和苹果)的临界浓度。在浓度为0.1 ~ 3.0% (w/v)的情况下,三种果胶源均表现出牛顿-剪切稀释行为。果胶临界浓度从低到高依次为向日葵(0.6792 ~ 0.9589 % (w/v))、柑橘(0.7172 ~ 1.0347% (w/v))、苹果(0.7645 ~ 1.1233 % (w/v))。根据稠度指数确定的临界浓度与零剪切粘度计算结果较为接近。而由比粘度和表观粘度确定的果胶溶液的临界浓度与由零剪切粘度确定的临界浓度有显著差异。
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引用次数: 0
Effects of steam explosion on physicochemical, functional and structural properties of soluble dietary fiber from pomelo peel 蒸汽爆炸对柚皮可溶性膳食纤维理化、功能和结构特性的影响
4区 农林科学 Pub Date : 2023-09-13 DOI: 10.1515/ijfe-2023-0099
Zhining Yuan, Jiatian Yan, Qian Zhang, Jie Zheng, Aijun Hu
Abstract The effects of steam explosion (SE) on the physicochemical, functional and structural characteristics of soluble dietary fiber (SDF) extracted from pomelo peel were evaluated. At the treatment condition of 0.9 MPa,120 s, the extraction yield of SDF increased by 156.7 %, and the water holding capacity, oil holding capacity, and swelling capacity increased by 36.6 %, 42.7 %, and 21.4 %, respectively. Additionally, in vitro hypoglycemic capacity, cation exchange capacity, nitrite ion adsorption capacity, and antioxidant capacity were all improved. It was observed that a large number of cracks in the SDF, and the structure of SDF became loose and porous and specific surface area of SDF increased to 1.41 times. In addition, the results from differential scanning calorimetry indicated that SDF treated with SE had better thermal stability, and the degradation temperature increased from 311.93 °C to 316.28 °C. So, SE could be used as an effective method for modifying dietary fiber.
摘要研究了蒸汽爆炸处理(SE)对柚皮可溶性膳食纤维(SDF)理化、功能和结构特性的影响。在0.9 MPa、120 s的处理条件下,SDF的提取率提高了156.7%,持水能力、持油能力和溶胀能力分别提高了36.6%、42.7%和21.4%。体外降糖能力、阳离子交换能力、亚硝酸盐离子吸附能力和抗氧化能力均有提高。结果表明,SDF中出现大量裂纹,结构疏松多孔,比表面积增加到1.41倍。差示扫描量热分析结果表明,经SE处理的SDF具有较好的热稳定性,降解温度从311.93℃提高到316.28℃。因此,硒可以作为一种有效的膳食纤维改性方法。
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引用次数: 0
Effect of fermentation of Danisco mixed lactic acid bacteria and single Bifidobacterium lactis HCS04-001 on metabolites of soy yogurt 丹尼斯科混合乳酸菌与单乳双歧杆菌HCS04-001发酵对大豆酸奶代谢物的影响
4区 农林科学 Pub Date : 2023-09-12 DOI: 10.1515/ijfe-2023-0085
Xu Xinyue, Cui Huaitian, Xu Jiaxin, Yuan Zhiheng, Li Jun, Liu Jun, He Liu, Zhu Danshi
Abstract In this study, the effects of Danisco mixed lactic acid bacteria and single Bifidobacterium lactis HCS04-001 fermentation on metabolites in soy yogurt were investigated. The main volatile metabolites in sample D fermented by Danisco mixed lactic acid bacteria were aldehydes, followed by alcohols and ketones. In contrast, the main flavor substances in sample SQ fermented by single Bifidobacterium lactis HCS04-001 were alcohols followed by aldehydes. L-Arginine, S-Adenosylhomocysteine, Glutamyltyrosine, Gly-Trp, Ser-Trp, Ile-Ser-Leu, Pro-Val-Leu etc. and D-Ornithine, Citrulline, Glutamylproline, organic acid were the main non-volatile differential metabolites that distinguished the soy yogurt samples. Arginine biosynthesis and glutathione metabolism were important pathways leading to differences in metabolic profiles. This study provides detailed insight into the metabolic properties of commercial Danisco mixed lactic acid bacteria and single Bifidobacterium lactis HCS04-001 fermentations, which will contribute to the development of soy yogurt with good nutritional and sensory qualities.
摘要本试验研究了Danisco混合乳酸菌和单乳双歧杆菌HCS04-001发酵对大豆酸奶中代谢物的影响。丹斯科混合乳酸菌发酵的D样品挥发性代谢物主要为醛类,其次为醇类和酮类。单株乳酸双歧杆菌HCS04-001发酵的SQ样品中风味物质主要为醇类,其次为醛类。l-精氨酸、s -腺苷同型半胱氨酸、谷氨酰基酪氨酸、Gly-Trp、Ser-Trp、Ile-Ser-Leu、Pro-Val-Leu等和d -鸟氨酸、瓜氨酸、谷氨酰脯氨酸、有机酸是区分大豆酸奶样品的主要非挥发性差异代谢物。精氨酸生物合成和谷胱甘肽代谢是导致代谢谱差异的重要途径。本研究为商业化Danisco混合乳酸菌和单一乳酸双歧杆菌HCS04-001发酵的代谢特性提供了详细的了解,为开发具有良好营养品质和感官品质的大豆酸奶提供了依据。
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引用次数: 0
Effect of defatted rice bran addition on properties of texturized soy and rice protein products 脱脂米糠添加量对大豆和大米蛋白质地化产品性能的影响
IF 1.6 4区 农林科学 Pub Date : 2023-09-01 DOI: 10.1515/ijfe-2023-0041
Thanaporn Pengjun, C. Sringarm, T. Kunanopparat, S. Rungchang, S. Ditudompo, S. Siriwattanayotin
Abstract The objective of this work was to produce low moisture-texturized vegetable protein (LM-TVP). Firstly, SPI:DRB at ratio of 50:50, 65:35 and 80:20 (w/w) was blended to produce TVP with 50–70 % protein (TSP50–70), respectively. In addition, RPI:DRB was also blended at the same ratio to produce non beany odor TVP with 50–70 % protein (TRP50–70). All samples were extruded using twin screw extruder. Extrusion condition was fixed at 25 % of feed moisture, 400 rpm of screw speed and 130 °C of die temperature. Next, properties of TSP50–70 and TRP50–70 before and after rehydration were characterized. For TSP50–70, studied properties consisting of expansion ratio, density, WAC, WHC and OHC of TSP50–70 were 2.20–2.27 %, 0.26–0.34 kg/m3, 414–446 %, 2.87–4.88 g H2O/g and 2.55–2.73 g oil/g respectively. These properties values were closed and in the same range of commercial-TVP (C-TVP). However, texture of TSP50 and TSP70 was significantly different, as decreasing DRB content from 50 (TSP50) to 20 % (TSP70) improved texture in terms of hardness (from 0.51 to 1.88 N), springiness (from 0.73 to 0.96) and cohesiveness (from 0.46 to 0.81) of TSP. Therefore, to add value to DRB, TSP70 (80 % SPI and 20 % DRB) was proposed to produce TSP. For TRP, expansion ratio, density, WAC, hardness, springiness and cohesiveness of TRP50–70 were 1.07–1.34 %, 0.63–0.88 kg/m3, 78–158 %, 1.03–9.10 N, 0.71–0.85 and 0.27–0.29 which were out of range compared to C-TVP.
摘要本工作的目的是生产低水分质地化植物蛋白(LM-TVP)。首先,将SPI:DRB按50:50、65:35和80:20(w/w)的比例混合,以生产50-70的TVP % 蛋白(TSP50-70)。此外,RPI:DRB也以相同的比例混合,以产生50–70的无豆腥味TVP % 蛋白质(TRP50-70)。所有样品均使用双螺杆挤出机挤出。挤压条件固定为25 % 饲料水分,400 螺杆转速rpm和130 模具温度°C。接下来,对再水化前后TSP50-70和TRP50-70的性质进行了表征。对于TSP50–70,所研究的由TSP50-70的膨胀比、密度、WAC、WHC和OHC组成的性能为2.20–2.27 %, 0.26–0.34 kg/m3,414–446 %, 2.87–4.88 g H2O/g和2.55–2.73 g油/g。这些特性值是闭合的,并且在商业TVP(C-TVP)的相同范围内。然而,TSP50和TSP70的质地显著不同,DRB含量从50(TSP50)降低到20 % (TSP70)改善了硬度方面的纹理(从0.51到1.88 N) TSP的弹性(从0.73到0.96)和内聚性(从0.46到0.81)。因此,为了增加DRB的价值,TSP70(80 % SPI和20 % DRB)来产生TSP。对于TRP,TRP50–70的膨胀比、密度、WAC、硬度、弹性和内聚性为1.07–1.34 %, 0.63–0.88 kg/m3,78–158 %, 1.03–9.10 N、 0.71–0.85和0.27–0.29,与C-TVP相比超出范围。
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引用次数: 0
Frontmatter 头版头条
4区 农林科学 Pub Date : 2023-09-01 DOI: 10.1515/ijfe-2023-frontmatter9
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引用次数: 0
Adsorption and desorption characteristics of flavonoids extracted from hawthorn (Crataegus pinnatifida) on macroporous resin 山楂黄酮在大孔树脂上的吸附与解吸特性
4区 农林科学 Pub Date : 2023-08-31 DOI: 10.1515/ijfe-2022-0263
Xin Huang, Mingxing Zhang, Suhong Li, Tuoping Li
Abstract In this work, the adsorption and desorption capacities of six resins (HP-20, AB-8, X-5, DM130, HPD100, D4006) for the purification of hawthorn flavonoids were investigated. HP-20 resin was screened out that has the best adsorption capacity, with an adsorption capacity of 24.2 mg/g. Langmuir and Freundlich isotherm model, pseudo first-order and pseudo second-order kinetics and intra particle diffusion model were used to fit the adsorption process. The results indicated that the adsorption process of hawthorn flavonoids by HP-20 was in accordance with the Langmuir isotherm model and pseudo second-order model, and the optimal adsorption temperature was 298 K. The adsorption process was spontaneously exothermic as indicated by thermodynamic parameters. After purification, hawthorn flavonoids showed high acetylcholinesterase inhibitory activities.
摘要研究了6种树脂(HP-20、AB-8、X-5、DM130、HPD100、D4006)对山楂黄酮的吸附解吸性能。筛选出的HP-20树脂吸附量最佳,吸附量为24.2 mg/g。采用Langmuir和Freundlich等温模型、拟一阶和拟二阶动力学模型和颗粒内扩散模型拟合吸附过程。结果表明,HP-20对山楂黄酮的吸附过程符合Langmuir等温模型和拟二阶模型,最佳吸附温度为298 K。热力学参数表明,吸附过程是自发放热的。纯化后的山楂黄酮具有较高的乙酰胆碱酯酶抑制活性。
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引用次数: 0
Effects of extrusion treatment on the physical and emulsifying properties of wheat germ protein 挤压处理对小麦胚芽蛋白物理及乳化特性的影响
IF 1.6 4区 农林科学 Pub Date : 2023-08-31 DOI: 10.1515/ijfe-2023-0124
Chaofan Gao, Jun-qiang Jia, Su Zhang, Xinyu Song, Yi Yang, Qiong-ying Wu, Xiudie Cui
Abstract This study investigated the impact of the extrusion of defatted wheat germ (DWG) on the physical properties of wheat germ protein (WGP) and its efficacy as a novel emulsifier in terms of emulsion stability. Compared with the untreated sample, the particle size of extruded WGP (E-WGP) was decreased by 56.22 %, while the absolute zeta-potential was increased by 40.07 %; the enthalpy increased from 0.013 J/g to 0.078 J/g, and the structure became more orderly. The amount of protein required to produce stable emulsions was much lower for E-WGP than for untreated WGP. Moreover, The E-WGP emulsions showed good storage stability after 7 day of storage at 4 °C, which had higher absolute zeta-potential (24.65 %), emulsifying activity (200.00 %), and turbidity (139.09 %) than the untreated sample. After the freeze-thaw cycle, the E-WGP emulsions had smaller particle sizes and higher turbidity, and their flocculation degree was lower than that of the untreated sample. These findings demonstrate E-WGP can be used as a new innovative emulsifier.
摘要本研究探讨了脱脂小麦胚芽(DWG)的挤压对小麦胚芽蛋白(WGP)物理性质的影响及其作为新型乳化剂的乳化稳定性。与未处理的样品相比,挤出的WGP(E-WGP)的颗粒尺寸减小了56.22 %, 而绝对ζ电位增加了40.07 %; 焓从0.013增加 J/g至0.078 J/g,结构变得更加有序。E-WGP产生稳定乳液所需的蛋白质量远低于未处理的WGP。此外,E-WGP乳液在7 存放日期:4 °C,具有更高的绝对ζ电位(24.65 %), 乳化活性(200.00 %), 和浊度(139.09 %) 与未处理的样品相比。冻融循环后,E-WGP乳液的粒径较小,浊度较高,絮凝度低于未处理样品。这些发现表明E-WGP可以作为一种新的创新乳化剂。
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引用次数: 0
Heat and mass transfer in vacuum drying process of fructooligosaccharides syrup 低聚果糖糖浆真空干燥过程中的传热传质
IF 1.6 4区 农林科学 Pub Date : 2023-08-30 DOI: 10.1515/ijfe-2022-0264
Lijuan Zhao, Hui Xie, Yuxuan Liu, Chenxi Ran, Zhonghua Wu
Abstract Fructooligosaccharides (FOS) is a functional food additive. FOS syrup produced by biological methods can be easily transported, stored and used after drying. In this study, the effects of operating pressure, heating temperature and initial moisture content of FOS syrup on the drying characteristics during vacuum drying were studied. With a visual system, the state changes of the material during the drying process were recorded. The specific heat, viscosity and thermal conductivity of the FOS at different temperatures and moisture contents were measured. From the perspective of drying characteristics, the whole drying process can be divided into four periods: the increasing drying rate period AB, the first falling drying rate period BC, the second falling drying rate period CD and the third falling drying rate period DE. The heat transfer mode in AB and BC was boiling heat transfer, with the material viscosity less than 267.9 Pa·s. In CD period, the heat transfer mode was convection heat transfer with the material viscosity of 267.9 Pa·s to 501.6 Pa·s. In DE period, the material viscosity was greater than 501.6 Pa·s and did not have fluidity, and the heat transfer mode was heat conduction. A multivariate model for the convection heat transfer coefficient was obtained based on the heat balance. The maximum error between the simulation value by the model and the experimental value of the material moisture content during the vacuum drying process was 4.18 %.
摘要低聚果糖(FOS)是一种功能性食品添加剂。生物法生产的果寡糖糖浆易于运输、储存和干燥后使用。在真空干燥过程中,研究了操作压力、加热温度和果糖浆初始含水量对果糖浆干燥特性的影响。用视觉系统记录了物料在干燥过程中的状态变化。测定了不同温度和含水率下FOS的比热、粘度和导热系数。从干燥特性来看,整个干燥过程可分为4个阶段:干燥速率增加期AB、第一干燥速率下降期BC、第二干燥速率下降期CD和第三干燥速率下降期DE。AB和BC阶段的传热方式均为沸腾传热,物料粘度小于267.9 Pa·s。CD期换热方式为对流换热,物料粘度为267.9 Pa·s ~ 501.6 Pa·s。DE期物料粘度大于501.6 Pa·s,不具有流动性,传热方式为热传导。基于热平衡理论,建立了对流换热系数的多元模型。真空干燥过程中物料含水率的模型模拟值与实验值的最大误差为4.18 %。
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引用次数: 0
Quality enhancement of spray-dried pumpkin powder by mixing with mulberry leaf and oat bran powders 用桑叶和燕麦麸粉混合提高喷雾干燥南瓜粉的质量
IF 1.6 4区 农林科学 Pub Date : 2023-08-18 DOI: 10.1515/ijfe-2023-0054
Ying Lyu, Qinqin Chen, Mingyang Gou, Gege Liu, Jin-feng Bi
Abstract To solve the delamination & precipitation phenomena and to improve the quality of the spray-dried pumpkin powder (PP), the effects of adding mulberry leaf powder (MLP) and oat bran powder (OBP) on the PP quality were investigated. Results showed that POBP (PP + OBP, w:w = 2:1) had lower hygroscopicity (≤42.96 %), which was more homogeneous and stickiness after being brewed, effectively alleviating delamination & precipitation phenomena. Besides, PMLP (PP + MLP, w:w = 2:1) had the highest total phenolic content and total flavonoid content, with the values of 96.92 and 90.50 mg/100 g, respectively. PMLP also exhibited about ten times the antioxidant activity of PP. Furthermore, nine regression equations predicted the antioxidant properties of powders based on soluble solid values and bitterness. Overall, this study indicated that the addition of OBP and MLP improved the stability and nutritional quality of PP, respectively.
摘要为了解决喷雾干燥南瓜粉(PP)的分层沉淀现象,提高其质量,研究了添加桑叶粉(MLP)和燕麦麸粉(OBP)对PP质量的影响。结果表明,POBP(PP+OBP,w:w=2:1)吸湿性较低(≤42.96%),酿造后更均匀、更粘稠,有效缓解了分层沉淀现象。此外,PMLP(PP+MLP,w:w=2:1)的总酚含量和总黄酮含量最高,分别为96.92和90.50mg/100g。PMLP的抗氧化活性也是PP的十倍左右。此外,根据可溶性固形物值和苦味,九个回归方程预测了粉末的抗氧化性能。总之,本研究表明,添加OBP和MLP分别提高了PP的稳定性和营养质量。
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引用次数: 0
Impact of fat types on the visual, textural, and sensory properties of Nanberenji (a traditional gluten-free cookie) 脂肪类型对南贝仁记(一种传统的无麸质饼干)视觉、质地和感官特性的影响
IF 1.6 4区 农林科学 Pub Date : 2023-08-16 DOI: 10.1515/ijfe-2023-0013
A. Heydari, M. Mohebbi, Arash Ghaitaranpour
Abstract The objective of this research was to evaluate the effects of various fat types (Bakery fat, Ghee, and Olive oil) on visual characteristics, baking behavior, textural, and sensory properties of a traditional gluten-free rice-based cookie (Nanberenji). The ability of image analysis for measuring some quality properties of prepared samples were also assessed. The obtained data demonstrated that the dough prepared with bakery and olive oil had maximum and minimum hardness values, respectively. However, after baking, the samples prepared with olive oil showed the highest hardness, meaningfully. The given outputs from image processing depicted that cookie prepared with bakery fat (NBF) and samples prepared with olive oil (NOO) had the highest and lowest surface color uniformity, respectively. Over baking time, the intensity and changes in the behavior of image textural features of NG and NBF samples were the same, while NOO samples showed a different behavior. Based on sensory analysis results, olive oil, as a healthy unsaturated fat, is advised to be used in the formulation of Nanberenji to produce a gluten-free cookie with a desirable texture, color, and flavor.
摘要本研究的目的是评估各种脂肪类型(面包脂肪、酥油和橄榄油)对传统无麸质米基饼干(Nanberenji)的视觉特征、烘焙行为、质地和感官特性的影响。还评估了图像分析测量制备样品的一些质量特性的能力。所获得的数据表明,用烘焙油和橄榄油制备的面团分别具有最大和最小硬度值。然而,烘焙后,用橄榄油制备的样品显示出最高的硬度,这是有意义的。图像处理的给定输出显示,用烘焙脂肪(NBF)制备的饼干和用橄榄油(NOO)制备样品的表面颜色均匀性分别最高和最低。随着烘焙时间的推移,NG和NBF样品的图像纹理特征的强度和行为变化是相同的,而NOO样品表现出不同的行为。根据感官分析结果,建议将橄榄油作为一种健康的不饱和脂肪用于南贝伦吉的配方中,以生产出具有理想质地、颜色和风味的无麸质饼干。
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引用次数: 0
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International Journal of Food Engineering
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