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Factors dictating the extent of low elongation in high sulfur-containing bainitic steels 决定高含硫贝氏体钢低延伸程度的因素
IF 0.8 4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-17 DOI: 10.1515/ijmr-2022-0078
B. Dong, Tingping Hou, Peter Hodgson, O. Isayev, O. Hress, S. Yershov, Kaiming Wu
Abstract The elongation of two low temperature bainitic steels with different sulfur contents was compared under the same heat treatment. Elongations of 1.0 ± 0.5 % and 11.4 ± 1.5 % were achieved for the high- and low-S steels, respectively. A high carbon concentration and fine grain size leading to over stability of the retained austenite in the high-S steel is the main reason for the poor elongation. The differences in carbon concentration and grain size between the two steels can be attributed to pinning by MnS, where the existence of a large number of long slivers of MnS in the high-S steel was responsible for the pinning. The stability of retained austenite was also analyzed by the local tensile elongation and hardness, and the volume fraction of retained austenite that transformed to martensite during the tensile process.
摘要 比较了硫含量不同的两种低温贝氏体钢在相同热处理条件下的伸长率。高硫钢和低硫钢的伸长率分别为 1.0 ± 0.5 % 和 11.4 ± 1.5 %。碳浓度高和晶粒细小导致高S钢中残留奥氏体过度稳定,是伸长率较差的主要原因。两种钢在碳浓度和晶粒尺寸上的差异可归因于 MnS 的钉扎作用,其中高 S 钢中大量长条状 MnS 的存在是造成钉扎作用的原因。此外,还通过局部拉伸伸长率和硬度以及拉伸过程中转变为马氏体的残留奥氏体的体积分数分析了残留奥氏体的稳定性。
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引用次数: 0
Experimental study of the phase relations of the Fe–Pt–Ho ternary system at 500 °C 500 °C 下 Fe-Pt-Ho 三元体系相关系的实验研究
IF 0.8 4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-17 DOI: 10.1515/ijmr-2022-0437
Ling Peng, YiFan Zhou, Bo Xu, Xinqiang Gao, Zheng-Fei Gu, Cheng-Fu Xu
Abstract The phase relations of the Fe–Pt–Ho ternary system at 500 °C have been studied by using X-ray diffraction, scanning electron microscopy and energy dispersive spectroscopy techniques. The Ho3Pt4 phase is stable at 500 °C, and the introduction of Fe does not cause the Ho3Pt4 phase to be decomposed into the two neighbouring phases HoPt and HoPt2. The single phase ranges of α-Fe, Fe3Pt, FePt, FePt3 and Pt in Fe–Pt binary system are from 0 to 10 at.% Pt, 14 to 32 at.% Pt, 33 to 63 at.% Pt, 66 to 78 at.% Pt, and 82 to 100 at.% Pt, respectively. The highest solid solubility of Ho in the α-Fe, Fe3Pt, FePt, FePt3 and (Pt, Fe) phases is less than 1.5 at.% Ho, 2 at.% Ho, 2 at.% Ho, 1.5 at.% Ho and 1.5 at.% Ho, respectively. The isothermal section at 500 °C of the Fe–Pt–Ho ternary alloy phase diagram has been constructed, which consists of 19 single-phase regions, 35 two-phase regions and 17 three-phase regions. No new ternary compounds were found.
摘要 利用 X 射线衍射、扫描电子显微镜和能量色散光谱技术研究了 500 ℃ 下 Fe-Pt-Ho 三元体系的相关系。在 500 ℃ 下,Ho3Pt4 相是稳定的,而且铁的引入不会导致 Ho3Pt4 相分解成相邻的两个相 HoPt 和 HoPt2。在铁铂二元体系中,α-Fe、Fe3Pt、FePt、FePt3 和 Pt 的单相范围分别为 0 至 10 % Pt、14 至 32 % Pt、33 至 63 % Pt、66 至 78 % Pt 和 82 至 100 % Pt。在 α-Fe、Fe3Pt、FePt、FePt3 和(Pt,Fe)相中,Ho 的最高固溶度分别小于 1.5%Ho、2%Ho、2%Ho、1.5%Ho 和 1.5%Ho。在 500 °C 时,构建了 Fe-Pt-Ho 三元合金相图的等温段,其中包括 19 个单相区、35 个两相区和 17 个三相区。没有发现新的三元化合物。
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引用次数: 0
Critical systematic investigation of the Cd–Ce system: phase stability and Gibbs energies of formation and equilibria via thermodynamic description Cd-Ce体系的关键系统研究:通过热力学描述的相稳定性和吉布斯形成能和平衡能
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-10 DOI: 10.1515/ijmr-2021-8214
Jinming Liu, Xiaolong Huang, Quan Du, Lingyu Ouyang, Jian Xiao, Yong Li
Abstract The CALPHAD (CAlculation of PHAse Diagrams) technique is used in the critical remodeling of the Cd–Ce system. On the basis of new experimental data in the literature, the excess Gibbs energies of the solution phase expression (liquid, bcc, fcc, and hcp_A3) are described using the Redlich–Kister equation. Four compounds (Cd3Ce, Cd6Ce, Cd11Ce, and Cd17Ce2) are treated as stochiometric compounds. Two intermetallic compounds (Cd2Ce and Cd58Ce13), which exhibit a little homogeneity range, are treated as a two-sublattice model. Two thermodynamic models are used for the CdCe and bcc. Model I is to model the compound CdCe and bcc-Ce separately. Model II is to use the formula (Cd, Ce)0.5(Cd, Ce)0.5(Va)3 to describe the compound CdCe with a CsCl-type structure (B2) and cope with the disorder–order transition from bcc-A2 to bcc-B2. The present work shows that four eutectic reactions, three peritectic reactions, two eutectoid reactions, one peritectoid transformation and three congruent reactions are observed, and the stoichiometric compound Cd17Ce2 is only stable from 804 to 882 °C in the Cd–Ce system.
CALPHAD(计算相图)技术用于Cd-Ce系统的关键重构。在文献新实验数据的基础上,用Redlich-Kister方程描述了液相(liquid, bcc, fcc, hcp_A3)的过量吉布斯能。四种化合物(cd3ce、cd6ce、cd11ce和cd17ce 2)被视为化学计量化合物。两种金属间化合物(cd2ce和cd58ce13)均质范围较小,采用双亚晶格模型。CdCe和bcc采用了两种热力学模型。模型1分别对化合物CdCe和bcc-Ce进行建模。模型II是用公式(Cd, Ce) 0.5 (Cd, Ce) 0.5 (Va) 3描述具有cscl型结构(B2)的化合物CdCe,并处理从bcc-A2到bcc-B2的无序-有序转变。研究表明,在Cd - Ce体系中,共发生了4次共晶反应、3次包晶反应、2次共晶反应、1次包晶转变和3次全等反应,化学计量化合物cd17ce2仅在804 ~ 882℃范围内稳定。
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引用次数: 0
Effect of laser power on microstructure and tribological behavior of laser clad NiCr coating 激光功率对激光熔覆NiCr涂层显微组织和摩擦学性能的影响
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-09 DOI: 10.1515/ijmr-2022-0498
Sun Chengwen, Li Wei, Kong Dejun
Abstract NiCr coatings were prepared on H13 steel by laser cladding with different laser power. The microstructure and phases of the obtained coatings were analyzed using a super depth of field microscope and X-ray diffraction, respectively, and the effect of laser power on the friction–wear performance at high-temperature was investigated using a friction tester. The results show that the laser clad NiCr coatings fabricated at the different laser powers are composed of Cr 2 Ni 3 and FeNi 3 phases, and the porosity is decreased from 1.28 % to 0.48 % with the increase of laser power. The average coefficients of friction of NiCr coatings are decreased with the increase of laser power, and the wear rate of NiCr coating fabricated at the laser power of 1400 W power is the lowest among the three kinds of coatings, showing that the suitable laser power can improve the surface quality and wear resistance of NiCr coating.
摘要采用不同激光功率的激光熔覆方法在H13钢表面制备了NiCr涂层。利用超景深显微镜和x射线衍射分析了涂层的显微组织和物相,并利用摩擦试验机研究了激光功率对涂层高温摩擦磨损性能的影响。结果表明:在不同激光功率下制备的激光熔覆NiCr涂层主要由Cr 2 Ni 3和FeNi 3相组成,孔隙率随激光功率的增加从1.28%降低到0.48%;NiCr涂层的平均摩擦系数随激光功率的增加而减小,在1400 W激光功率下制备的NiCr涂层的磨损率最低,说明适当的激光功率可以改善NiCr涂层的表面质量和耐磨性。
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引用次数: 0
DGM – Deutsche Gesellschaft für Materialkunde (德国情报协会
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-11-07 DOI: 10.1515/ijmr-2023-2012
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引用次数: 0
Design of fixture for ultrasonic assisted gas tungsten arc welding using an integrated approach 超声辅助钨气弧焊夹具的一体化设计
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-10-20 DOI: 10.1515/ijmr-2022-0159
Dhilip A, Jayakrishnan Nampoothiri, Anand K
Abstract The welding fixture greatly impacts the weld quality matrixes. In this work, the welding fixture for ultrasonic-assisted gas tungsten arc welding to reduce the hot cracking behaviour in weldments was designed using the finite element analysis approach. A three-level, five-factor central composite design-based response surface methodology analysis was followed to vary the dimensions of the fixture for the modal and harmonic analysis of the fixture using Ansys software. The optimum fixture dimensions to achieve maximum displacement amplitude and minimum von-Mises stress have been optimized using a genetic algorithm approach. The model predictions for maximum displacement amplitude and minimum von-Mises stress were compared to the experimental findings at optimal conditions. A strong consensus between the model prediction by genetic algorithm and experimental findings indicates the correctness of the developed model.
焊接夹具对焊缝质量的影响很大。本文采用有限元分析方法,设计了超声辅助钨极气体保护焊的焊接夹具,以减少焊缝的热裂行为。采用基于三层次、五因素中心复合设计的响应面分析方法,利用Ansys软件改变夹具的尺寸,对夹具进行模态和谐波分析。采用遗传算法对实现最大位移振幅和最小von-Mises应力的最佳夹具尺寸进行了优化。将模型预测的最大位移幅值和最小von-Mises应力与最佳条件下的实验结果进行了比较。遗传算法的预测结果与实验结果吻合较好,表明所建模型是正确的。
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引用次数: 0
Influence of process parameters on ageing and free vibration characteristics of fiber-reinforced polymer composites by fusion filament fabrication process 工艺参数对熔融长丝制备纤维增强聚合物复合材料老化及自由振动特性的影响
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-10-01 DOI: 10.1515/ijmr-2022-0271
Vigneshwaran Karupaiah, Venkateshwaran Narayanan
Abstract Fused filament fabrication is a promising additive manufacturing technology and an alternative to traditional processes for the fabrication of polymer and fiber-reinforced polymer composites. In this work, the effects of process parameters such as layer thickness, infill density, and infill pattern on the ageing and free vibration characteristics of three-dimensional printed composites were investigated. It was observed that the water absorption rate is higher in acrylonitrile butadiene styrene (ABS) printed specimens compared to carbon fiber reinforced acrylonitrile butadiene styrene (CF/ABS) specimens due to the effect of carbon fiber which acts as a strong hydrophobic material. The free vibration characteristic of the printed composite specimen is found as per American Society for Testing Materials standards. From the results, it is found that the 5 % addition of carbon fiber, hexagonal pattern, and 0.30 mm layer thickness show an increase in the vibration behaviour of the composites compared to the specimen printed without reinforcement. Experimental modal analysis was carried out on a cantilever beam-like sample and revealed that the addition of fiber has enhanced natural frequencies and damping ratio.
摘要熔融长丝制造是一种很有前途的增材制造技术,是传统聚合物和纤维增强聚合物复合材料制造工艺的替代方案。本文研究了层厚、填充密度和填充方式等工艺参数对三维打印复合材料老化和自由振动特性的影响。结果表明,由于碳纤维作为强疏水材料的作用,ABS(丙烯腈-丁二烯-苯乙烯)打印样品的吸水率高于碳纤维增强丙烯腈-丁二烯-苯乙烯(CF/ABS)样品。根据美国材料试验学会的标准,确定了打印复合材料试样的自由振动特性。结果表明,碳纤维添加量为5%、六角形图案和0.30 mm层厚时,复合材料的振动性能比未增强的样品有所提高。对悬臂梁样试样进行了模态分析,结果表明纤维的加入提高了固有频率和阻尼比。
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引用次数: 0
Desirability function analysis approach for optimization of fused deposition modelling process parameters 优选熔融沉积建模工艺参数的可取函数分析方法
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-10-01 DOI: 10.1515/ijmr-2022-0266
Hariprasad Tarigonda, Koyyagura Lakshmi Kala, Peedinti Gnanaprakash, Doddipalli Raghurami Reddy, Konareddy Harsha Vardhan Reddy
Abstract This study uses desirability function analysis to optimize the process parameters namely layer thickness, fill pattern, fill density, and build orientation for fused deposition modelling on polyethylene terephthalate glycol material. The Taguchi-desirability function analysis is one of the optimization techniques for the multi-objective decision-making process. Taguchi L 9 orthogonal array is employed in the test trials during the fused deposition modelling process. The output responses measured are dimension error, ductility, and tensile strength. The goal of process parameter optimization is to attain the best of the trials for minimal dimension error and maximum tensile strength and ductility. The best feasible amalgamation of input variables is discovered for the investigated and assessed response features utilizing desirability function analysis. As per the results obtained from experiments, it is concluded that the optimal combination of parameters is layer thickness of 0.1 mm, build orientation of 0°, fill density of 90 % and hexa fill pattern. By following this combination, the error in the dimensions was slightly increased which needed to be reduced, but both tensile strength and ductility were increased which are more desirable characteristics.
摘要本研究利用可取函数分析优化聚对苯二甲酸乙二醇酯材料熔融沉积建模的工艺参数,即层厚、填充模式、填充密度和构建方向。田口期望函数分析是多目标决策过程的优化技术之一。在熔融沉积建模过程中,采用田口l9正交阵列进行试验。测量的输出响应是尺寸误差、延展性和抗拉强度。工艺参数优化的目标是获得最小尺寸误差和最大拉伸强度和延展性的最佳试验。利用期望函数分析,为所调查和评估的响应特征发现了最佳可行的输入变量合并。实验结果表明,最优的参数组合为层厚0.1 mm,构筑方向0°,填充密度90%,六边形填充模式。通过遵循这种组合,尺寸误差略有增加,这需要减少,但抗拉强度和延展性都增加了,这是更理想的特性。
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引用次数: 0
Fused filament fabricated PEEK based polymer composites for orthopaedic implants: a review 熔融长丝制备PEEK基聚合物复合材料用于骨科植入物的研究进展
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-10-01 DOI: 10.1515/ijmr-2022-0225
Sathishkumar Sankar, Jawahar Paulraj, Prasun Chakraborti
Abstract Additive manufacturing has become a cutting-edge technique to produce biomaterials for various clinical applications. Recent investigations have shown their significance and highlighted their future requirements. Many additive manufacturing technologies are mostly related to manufacturing polyether ether ketone (PEEK) based implants. Among them, fused filament fabrication (FFF) or fused deposition modelling (FDM) is the preferred method. Specifically, FFF builds complex scaffolds for tissue engineering and customized implants, which are not achievable with traditional fabrication methods. PEEK is a rigid, tissue-compatible, lightweight polymer with good wear characteristics and a long implant life. In general, PEEK has many valuable properties and the potential to solve many medical problems, especially orthopaedic implantation. This paper provides a brief study that gives an overview of PEEK-based biomaterials for FFF-based orthopaedic procedures, materials evolution, recent advancements, and the current research progress is also addressed systematically.
摘要增材制造已成为生产各种临床应用的生物材料的前沿技术。最近的调查显示了它们的重要性,并突出了它们未来的需要。许多增材制造技术主要与制造聚醚醚酮(PEEK)基植入物有关。其中,熔融长丝制造(FFF)或熔融沉积建模(FDM)是首选的方法。具体来说,FFF为组织工程和定制植入物构建复杂的支架,这是传统制造方法无法实现的。PEEK是一种刚性、组织相容性好、重量轻的聚合物,具有良好的耐磨性和较长的植入寿命。总的来说,PEEK具有许多有价值的性能和解决许多医疗问题的潜力,特别是骨科植入。本文提供了一项简要的研究,概述了基于peek的生物材料用于基于fff的骨科手术,材料的演变,最近的进展,以及当前的研究进展也进行了系统的讨论。
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引用次数: 0
Behaviour of glass fiber reinforced polymer (GFRP) structural profile columns under axial compression 玻璃纤维增强聚合物(GFRP)结构型材柱在轴压作用下的性能
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2023-10-01 DOI: 10.1515/ijmr-2022-0169
Sanjana S. Kumar, Rahul Kumar Sonker, Senthilkumar Rajendran
Abstract Glass fiber-reinforced plastic (GFRP) structural profiles in the construction industry are a promising alternative to conventional building materials due to their high strength-to-weight ratio, high tensile strength, insulation properties, chemical resistance, fatigue properties, and lower maintenance cost. This study aims to evaluate the compression behaviour of semi-compact and slender glass fiber-reinforced plastic I-sections. Short, intermediate, and long columns of both slender and semi-compact I-sections were subjected to axial compression, and the experimental capacity was compared to available theoretical results. It was found that the experimental capacity of short, semi-compact, and long columns were 27 %, 49 %, and 40 % lower than the theoretical capacity of semi-compact I-sections. Short slender sections had an ultimate experimental capacity 55 % greater than the theoretical results. However, lower ultimate capacities were achieved for intermediate and long columns in the case of slender sections when compared to the theoretical capacity. Slender sections were prone to both global and local buckling, whereas semi-compact sections failed by global buckling alone. The study also concludes the need for proper section classification of glass fiber-reinforced plastic sections to consider buckling characteristics. The existing theoretical equations to estimate the load-carrying capacity was found to be overly conservative; hence it is necessary to conduct numerical and parametric studies to develop equations that are more in agreement with the experimental results.
摘要:玻璃纤维增强塑料(GFRP)结构型材因其高强度、高抗拉强度、高绝缘性能、耐化学性、抗疲劳性能和较低的维护成本,在建筑行业中是传统建筑材料的一个很有前途的替代品。本研究旨在评估半致密和细长玻璃纤维增强塑料工字截面的压缩性能。细长和半紧凑的i型截面的短、中间和长柱受到轴向压缩,并将实验能力与现有的理论结果进行了比较。结果表明,短柱、半密实柱和长柱的试验承载力分别比半密实工字截面的理论承载力低27%、49%和40%。较短的细长截面的极限承载力比理论结果大55%。然而,与理论容量相比,在细长截面的情况下,中长柱的极限容量较低。细长截面容易发生整体屈曲和局部屈曲,而半致密截面仅受整体屈曲破坏。研究还得出结论,考虑屈曲特性,需要对玻璃纤维增强塑料截面进行适当的截面分类。现有的承载能力估算理论公式过于保守;因此,有必要进行数值和参数研究,以建立更符合实验结果的方程。
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引用次数: 0
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