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Comparison of the viscoelastic properties and viscosity of suspensions determined by oscillation and creep testing 通过振荡试验和蠕变试验测定的悬浮液粘弹性能和粘度的比较
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-27 DOI: 10.2355/isijinternational.isijint-2024-078
Kento Nakanishi, Takehiro Sumita, Noritaka Saito, Kunihiko Nakashima

Knowledge of the viscoelastic properties of suspensions is essential for many industrial processes. Although oscillation and creep testing are widely used to measure the viscoelastic properties of complex fluids, few studies on the correlation between the viscoelastic properties measured using these methods have been published. This study aims to provide insights into the differences between these methods and determine which method is better suited for a particular application. The room-temperature viscoelastic properties of a suspension composed of polyethylene beads dispersed in a silicone oil matrix were measured by oscillation and creep testing and compared. The results of oscillation testing indicated that the suspension showed weakly elastic deformation, whereas the results of creep testing revealed that the suspension was relatively elastic, with the liquid phase showing lower viscosity. In addition, the viscosity measured by oscillation testing was lower than that measured by creep testing. When the imposed flow causes microstructural changes, such as when the shear flow and particle‒particle contact induce aggregation, the analyzed flow property considerably differs between testing methods.

了解悬浮液的粘弹性能对许多工业流程至关重要。尽管振荡测试和蠕变测试被广泛用于测量复杂流体的粘弹性能,但有关使用这些方法测量的粘弹性能之间的相关性的研究却鲜有发表。本研究旨在深入探讨这两种方法之间的差异,并确定哪种方法更适合特定应用。通过振荡测试和蠕变测试测量了由分散在硅油基质中的聚乙烯珠组成的悬浮液的室温粘弹性能,并进行了比较。振荡测试结果表明,悬浮液表现出弱弹性变形,而蠕变测试结果表明,悬浮液具有相对弹性,液相粘度较低。此外,振荡测试测得的粘度低于蠕变测试测得的粘度。当外加流动导致微观结构发生变化时,例如当剪切流动和颗粒与颗粒之间的接触引起聚集时,不同测试方法所分析的流动特性会有很大不同。
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引用次数: 0
Microstructure and mechanical properties of gas metal arc-welded Fe-Mn-Si seismic damping alloy 气体金属弧焊铁锰硅减震合金的微观结构和力学性能
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-19 DOI: 10.2355/isijinternational.isijint-2024-174
Tomoya Nagira, Terumi Nakamura, Fumiyoshi Yoshinaka, Takahiro Sawaguchi, Yasuhiko Inoue

A brace-type seismic damper made of an Fe-15Mn-11Cr-7.5Ni-4Si alloy solidified in the ferrite-austenite (FA) mode and SN490B steel, which can be constructed via welding, was proposed. To realize the proposed seismic damper, gas metal arc welding was applied to produce similar FMS/FMS fillet welds and dissimilar FMS/SN490B fillet weld joints. Based on the Schaeffler diagram, similar and dissimilar welding consumables were designed such that the fillet weld metal solidified in the FA mode without solidification cracking. Sound similar fillet welded joints were obtained using two types of welding consumables with different Cr/Ni equivalent ratios although both the similar fillet weld metals had a coarse columnar austenite grain structure. These displayed higher tensile strengths (716–736 MPa) and marginally lower elongations (67–70%) than the FMS alloy. Moreover, a similar fillet weld metal with a chemical composition almost identical to that of the FMS alloy exhibited a remarkable low-cycle fatigue life (5740 cycles). This was shorter than that of the FMS alloy (9351 cycles) owing to the easier formation of α'-martensite. A dissimilar fillet welded joint with a chemical composition within the austenite region was produced without solidification cracking. The dissimilar fillet weld metal showed high tensile strength (867 MPa) and total elongation (61%). These were comparable to those of similar fillet weld metals.

提出了一种由铁素体-奥氏体(FA)模式下凝固的 Fe-15Mn-11Cr-7.5Ni-4Si 合金和 SN490B 钢制成的支撑型地震阻尼器,该阻尼器可通过焊接构建。为了实现所提出的地震阻尼器,采用了气体金属弧焊来生产相似的 FMS/FMS 角焊缝和不相似的 FMS/SN490B 角焊缝。根据舍弗勒图表,设计了相似和不相似的焊材,使角焊缝金属在 FA 模式下凝固而不会产生凝固裂纹。尽管两种相似的角焊缝金属都具有粗大的柱状奥氏体晶粒结构,但使用两种具有不同铬/镍当量比的焊材获得了声音相似的角焊缝。与 FMS 合金相比,它们的抗拉强度更高(716-736 兆帕),伸长率(67-70%)略低。此外,化学成分几乎与 FMS 合金相同的类似角焊缝金属的低循环疲劳寿命(5740 次)也非常出色。由于α'-马氏体更容易形成,因此比 FMS 合金的低循环疲劳寿命(9351 次)更短。生产出的化学成分在奥氏体区域内的异种角焊缝接头没有出现凝固裂纹。异种角焊缝金属显示出较高的抗拉强度(867 兆帕)和总伸长率(61%)。这些指标与同类角焊缝金属相当。
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引用次数: 0
Current trends on deep learning techniques applied in iron and steel making field: A review 钢铁制造领域应用深度学习技术的当前趋势:综述
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-19 DOI: 10.2355/isijinternational.isijint-2024-098
Kazumasa Tsutsui, Tokinaga Namba, Kengo Kihara, Junichi Hirata, Shohei Matsuo, Kazuma Ito

Recently, remarkable advances have been made in statistical analyses based on deep-learning techniques. Applied studies of deep learning have been reported in various industrial fields, including the iron and steel-making industries. The production of iron and steel requires a variety of processes, such as the processing of ingredients, iron-making, casting, and rolling. Consequently, the data acquired from them are diverse, and various tasks exist that can be assisted by deep-learning algorithms. Hence, providing a summary of the application is helpful for researchers specializing in information science to grasp the current trend of applied studies on deep learning techniques and for researchers specializing in each field of the iron and steel-making industry to understand what types of deep learning techniques are being utilized in other specialized fields. Therefore, in this study, we summarize the current studies on the application of deep learning in the iron- and steel-making fields by organizing them into several categories of processes and analytical methodologies. Furthermore, based on the results, we discuss future perspectives on the development of deep-learning techniques in this field.

最近,基于深度学习技术的统计分析取得了显著进展。深度学习在各个工业领域的应用研究都有报道,其中包括钢铁行业。钢铁生产需要多种工序,如原料加工、炼铁、铸造和轧制。因此,从中获取的数据多种多样,深度学习算法可以帮助完成各种任务。因此,对应用情况进行总结有助于信息科学专业的研究人员掌握当前深度学习技术应用研究的趋势,也有助于钢铁行业各领域的专业研究人员了解其他专业领域正在使用哪些类型的深度学习技术。因此,在本研究中,我们将深度学习在炼铁和炼钢领域的应用研究归纳为几类流程和分析方法。此外,基于研究结果,我们还讨论了深度学习技术在该领域的未来发展前景。
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引用次数: 0
Solidification microstructure and mechanical properties of B1-type TiC in Fe-Ti-C ternary alloys 铁-钛-碳三元合金中 B1 型 TiC 的凝固微观结构和力学性能
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-19 DOI: 10.2355/isijinternational.isijint-2024-166
Shuntaro Ida, Kengo Watanabe, Kyosuke Yoshimi

The microstructure of the B1-type TiC formed during solidification and its mechanical properties were investigated using arc-melted Fe–Ti–C ternary alloys. The TiC formed at relatively high temperatures in the liquid as the primary phase exhibited a dendritic shape. With decreasing temperature and/or decreasing Ti and C content in the liquid, the morphology of the TiC changed to a cubic shape with a {001}TiC habit plane, a plate shape with a {011}TiC habit plane, and a needle shape with a preferential growth direction of <001>TiC. The morphology of the TiC was characterized by the anisotropy of its surface energy and its growth rate. The cubic shape with a {001}TiC habit plane was formed as a result of the {001}TiC surface exhibiting the lowest surface energy among the TiC surfaces. However, the plate shape with a {011}TiC habit plane and the needle shape with a <001>TiC preferential growth direction likely formed because the slowest and fastest growth rates corresponded to the <011>TiC and <001>TiC directions, respectively. At room temperature, the alloy with dendritic TiC was fractured in the elastic deformation region because TiC exhibited no plastic deformation. However, the results obtained at 800°C suggested that the TiC exhibited plastic deformability and that the alloy with the dendritic TiC was also plastically deformed.

使用电弧熔化的铁-钛-碳三元合金研究了凝固过程中形成的 B1 型 TiC 的微观结构及其机械性能。在相对较高的温度下,作为主相在液体中形成的 TiC 呈树枝状。随着温度的降低和/或液体中 Ti 和 C 含量的减少,TiC 的形态转变为具有{001}TiC 惯性面的立方体形状、具有{011}TiC 惯性面的板状形状以及具有 <001>TiC优先生长方向的针状形状。TiC 的形态特征是其表面能和生长速度的各向异性。由于{001}TiC 表面的表面能在 TiC 表面中最低,因此形成了具有{001}TiC 习惯面的立方体形状。然而,具有{011}TiC习性面的板状形状和具有<001>TiC优先生长方向的针状形状的形成可能是因为最慢和最快的生长速度分别对应于<011>TiC和<001>TiC方向。在室温下,带有树枝状 TiC 的合金在弹性变形区断裂,因为 TiC 没有塑性变形。然而,在 800°C 时获得的结果表明,TiC 具有塑性变形能力,带有树枝状 TiC 的合金也发生了塑性变形。
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引用次数: 0
Rapid Identification of Liquid Steel Temperature in Tundish Based on Blackbody Cavity Sensor 基于黑体空腔传感器快速识别钢包中的液态钢温度
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-10 DOI: 10.2355/isijinternational.isijint-2023-499
Jiaocheng Ma, Linghui Meng, Zhendong Liu, Xin Zhao

In the continuous casting process, the temperature of liquid steel in tundish determines the casting speed and secondary cooling conditions, and then influences the billet quality. It's very important to measure the temperature of liquid steel in tundish quickly and accurately. However, the initial response lag of blackbody cavity sensor is inevitable since the time is required for the sensor inner wall and the liquid steel reaching thermal equilibrium by heat transfer. In this paper, in order to eliminate the initial response lag of sensor, a heat transfer model of sensor is established. The heat transfer characteristics and cavity integral emissivity of sensor with different depths immersed into liquid steel are analyzed. The analytical solution of sensor temperature is derived by separation of variables method and superposition principle, and is verified by the actual temperature measurement data. Then an innovative method of liquid steel temperature rapid identification is deduced and validated by the actual measurement data. The results show that the initial response lag of sensor is greatly shortened and the temperature measurement efficiency is improved. This study provides a theoretical method for improving the initial response speed of sensor.

在连铸过程中,中间包内钢液的温度决定了浇铸速度和二次冷却条件,进而影响钢坯质量。快速、准确地测量连铸机中钢液的温度非常重要。然而,黑体空腔传感器的初始响应滞后是不可避免的,因为传感器内壁和钢液通过热传导达到热平衡需要一定的时间。为了消除传感器的初始响应滞后,本文建立了传感器的传热模型。分析了传感器浸入钢液不同深度时的传热特性和腔体积分发射率。通过变量分离法和叠加原理得出了传感器温度的解析解,并通过实际温度测量数据进行了验证。然后推导出一种创新的液态钢温度快速识别方法,并通过实际测量数据进行了验证。结果表明,传感器的初始响应滞后大大缩短,温度测量效率得到提高。本研究为提高传感器的初始响应速度提供了一种理论方法。
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引用次数: 0
Effect of Fluoride Ions in Slag on the Dynamic Change of the Interfacial Tension between Liquid Iron and Molten Slag 炉渣中的氟离子对铁液与熔融炉渣之间界面张力动态变化的影响
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-09 DOI: 10.2355/isijinternational.isijint-2024-134
Masanori Suzuki, Kenta Iwakura, Yuichi Tsukaguchi, Kazuaki Mishima

The interfacial tension between the liquid steel and molten slag is one of the key properties to control the entrapment of mold flux in molten steel in the continuous casting process. A dynamic change of the interfacial tension is observed when deoxidized iron and silicate slag are in contact, which can be explained by the oxygen absorption and desorption at the iron/slag interface. However, the dynamic change of the interfacial tension is influenced by other surfactant components of the molten iron and slag. Fluoride ions are fundamental component of mold flux, and recognized as the surface active component of molten slag. The effect of fluoride ions in slag on the interfacial tension has not been critically evaluated. Here, the effect of fluoride ions in slag on the interfacial tension between molten iron and molten silicate slag was evaluated at 1823 K, where the fluoride-containing slag compositions were designed to exhibit the same SiO2 activity and slag viscosity as those of the fluoride-free slag. Compared with the case of molten iron and fluoride-free slag, the interfacial tension between the molten iron and fluoride-containing slag was initially lower. Except the effect of oxygen adsorption, fluoride ion was considered to directly decrease the interfacial tension. However, as the fluoride content in slag was higher, the interfacial tension tended to show the higher value at the final state. This behavior was attributed mainly to fluoride vaporization as SiF4, which reduce the SiO2 activity in slag and thus equivalent oxygen content at the iron/slag interface.

在连铸过程中,钢液与熔渣之间的界面张力是控制钢液中夹带结晶器助熔剂的关键特性之一。当脱氧铁和硅酸盐熔渣接触时,会观察到界面张力的动态变化,这可以用铁/熔渣界面的吸氧和解吸来解释。然而,界面张力的动态变化受到铁水和炉渣中其他表面活性剂成分的影响。氟离子是熔模助熔剂的基本成分,也是公认的熔渣表面活性成分。熔渣中的氟离子对界面张力的影响尚未得到严格评估。在此,我们评估了熔渣中的氟离子在 1823 K 下对铁水与熔融硅酸盐熔渣之间界面张力的影响,其中含氟熔渣成分被设计为具有与无氟熔渣相同的 SiO2 活性和熔渣粘度。与铁水和无氟炉渣的情况相比,铁水和含氟炉渣之间的界面张力最初较低。除了氧气吸附的影响外,氟离子被认为会直接降低界面张力。然而,随着炉渣中氟含量的增加,最终状态下的界面张力趋向于显示出更高的值。这种行为主要归因于氟化物汽化为 SiF4,降低了炉渣中 SiO2 的活性,从而降低了铁/炉渣界面的等效氧含量。
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引用次数: 0
Reduction degradation of lump, sinter, and pellets in blast furnace with hydrogen injection 高炉喷氢可降低块料、烧结矿和球团矿的降解率
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-08 DOI: 10.2355/isijinternational.isijint-2024-114
Muhammad Irfan Ahadian Barustan, Evan Copland, Thi Bang Tuyen Nguyen, Damien O’dea, Tom Honeyands

The increase of hydrogen usage in a blast furnace is expected to affect the reduction degradation of ferrous burden materials and influence the gas permeability inside the furnace. Previous studies show a disagreement on the effect of H2 on reduction degradation, with the extent of degradation depending on the H2 content and type of ferrous burden materials. In this study, the reduction degradation of sinter, lump, and pellet was compared using the reduction degradation test under different gas mixtures containing CO and H2, covering the gas composition of conventional and H2 injection blast furnaces. Lump (Newman Blend Lump NBLL) and pellets show a lower RDI-2.8 than sinter under all the gas compositions tested. Higher RDI-2.8 values were obtained for all burden materials with a reducing gas containing both CO and H2 compared to CO or H2 only. The addition of H2 to CO increases the pore diffusion rate allowing reducing gas to reach the centre part of the particles, leading to the reduction of hematite to magnetite and subsequent crack formation across the whole particles. Compared to the conventional blast furnace case, NBLL lump and sinter show a lower degradation for the H2 injection case while it was the opposite for the pellet, suggesting the necessity of reviewing overall burden materials to optimise the hydrogen injection in the blast furnace.

高炉中氢气用量的增加预计会影响黑色包袱材料的还原降解,并影响炉内气体渗透性。以往的研究表明,氢气对还原降解的影响存在分歧,降解程度取决于氢气含量和铁料类型。本研究使用还原降解试验比较了烧结矿、块矿和球团矿在含有 CO 和 H2 的不同混合气体条件下的还原降解情况,涵盖了传统高炉和喷射 H2 高炉的气体成分。在所有测试的煤气成分下,块料(纽曼混合块料 NBLL)和球团矿的 RDI-2.8 均低于烧结矿。在同时含有 CO 和 H2 的还原气体中,所有炉料的 RDI-2.8 值均高于仅含有 CO 或 H2 的炉料。在 CO 中加入 H2 增加了孔隙扩散率,使还原气体能够到达颗粒中心部分,导致赤铁矿还原为磁铁矿,随后在整个颗粒上形成裂纹。与传统的高炉情况相比,NBLL 块料和烧结矿在注入 H2 的情况下降解程度较低,而球团矿则相反,这表明有必要对整体负担材料进行审查,以优化高炉中的氢气注入。
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引用次数: 0
Estimation of True Hardness and Quantitative Evaluation of Auto-Tempering in As-Quenched Martensitic Steels 淬火马氏体钢的真实硬度估算和自动回火定量评估
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-05 DOI: 10.2355/isijinternational.isijint-2024-140
Osamu Idohara, Youhei Hiyama, Yoshitaka Misaka, Setsuo Takaki, Toshihiro Tsuchiyama

The hardness of martensitic steels with high Ms temperatures is reduced by auto-tempering after transformation, therefore the true hardness of martensite with carbon in fully solid solution is not known. In this study, we investigated a method to quantitatively evaluate the true hardness of quenched martensite unaffected by auto-tempering and the effect of auto-tempering was quantitatively evaluated by the diffusion area of carbon in bcc iron at temperatures below 400°C. As a result, it was clarified that the effect of auto-tempering is more pronounced in steels with an M50 temperature higher than 300°C and that the softening behavior of martensitic steels can be uniformly evaluated regardless of the carbon content if the activation energy of carbon diffusion is known. Furthermore, it was clarified that the degree of auto-tempering can be quantitatively evaluated by calculating the integral diffusion area S (= ∑Dt) below the M50 temperature during quenching.

Ms 温度较高的马氏体钢的硬度在转变后会因自动回火而降低,因此完全固溶的含碳马氏体的真实硬度尚不清楚。在本研究中,我们研究了一种定量评估不受自动回火影响的淬火马氏体真实硬度的方法,并通过温度低于 400°C 时碳在 bcc 铁中的扩散面积定量评估了自动回火的影响。结果表明,在 M50 温度高于 300°C 的钢材中,自动回火的影响更为明显,而且如果知道碳扩散的活化能,无论碳含量多少,都可以统一评估马氏体钢的软化行为。此外,通过计算淬火过程中低于 M50 温度的整体扩散面积 S (= ∑Dt),可以对自回火程度进行定量评估。
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引用次数: 0
Hydrogen embrittlement properties of rapid tempered high-Si steel and effects of the carbide and retained austenite on its properties 快速回火高硅钢的氢脆特性以及碳化物和残余奥氏体对其特性的影响
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-05 DOI: 10.2355/isijinternational.isijint-2024-181
Manami Sunako, Masataka Mizumoto, Azusa Ooi, Eiji Tada

Automotive suspension springs are required to be high-strength and lightweight, and currently have a maximum strength of 2000 MPa. In addition, they must have high resistance to hydrogen embrittlement in the service environment. From previous research, Si addition or rapid tempering improves the hydrogen embrittlement resistance of low alloy steel. In this study, we investigated the hydrogen embrittlement properties of steel samples with different Si contents and tempering rates and the effects of the fine iron carbides and retained austenite on its properties for 2000 MPa suspension spring steel. JISSUP7 (2.0Si) and SAE9254 (1.4Si) spring steels were tempered at different tempering rates by induction (IH) and furnace heating (FH) methods. Four-point bending tests under corrosion cycles were performed on these steels, and the time to failure was measured. The results show that the 2.0Si-IH steel with higher Si content and higher tempering rate has the longest fracture life and highest resistance to hydrogen embrittlement, even with relatively high diffusible hydrogen content. The size and volume fraction of iron carbides and retained austenite were evaluated by TEM, EBSD, and synchrotron XRD, and the 2.0Si-IH steels were found to have the smallest size and the highest volume fraction of fine iron carbides Fe2-3C(ε) and the highest amount of retained austenite. It is considered that the fine iron carbides of Fe2-3C(ε) work as hydrogen trap sites and that their high dispersion suppresses dislocation movement. They suppress hydrogen accumulation in stress concentrated areas and are expected to improve resistance to hydrogen embrittlement.

汽车悬架弹簧必须具有高强度和轻质的特点,目前的最大强度为 2000 兆帕。此外,它们还必须具有在使用环境中抗氢脆的能力。根据以往的研究,加硅或快速回火可提高低合金钢的抗氢脆性能。在本研究中,我们研究了不同含硅量和回火速率钢样的氢脆性能,以及细小碳化铁和残余奥氏体对 2000 兆帕悬挂弹簧钢性能的影响。采用感应(IH)和炉加热(FH)方法,以不同的回火速率对 JISSUP7(2.0Si)和 SAE9254(1.4Si)弹簧钢进行回火。对这些钢材进行了腐蚀循环下的四点弯曲试验,并测量了失效时间。结果表明,硅含量较高、回火速率较高的 2.0Si-IH 钢具有最长的断裂寿命和最高的抗氢脆性能,即使扩散氢含量相对较高。通过 TEM、EBSD 和同步辐射 XRD 评估了碳化铁和残余奥氏体的尺寸和体积分数,发现 2.0Si-IH 钢中细小碳化铁 Fe2-3C(ε) 的尺寸最小,体积分数最高,残余奥氏体量最高。据认为,Fe2-3C(ε)的细小碳化铁可作为氢捕获位点,其高度分散性可抑制位错运动。它们可抑制应力集中区域的氢积累,并有望提高抗氢脆能力。
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引用次数: 0
Effect of Deformation-induced α’-martensite and Serrated Grain Boundaries on The Deformation and Fracture Behavior of 201 Austenitic Stainless Steel at Low Temperature 变形诱导的 α'-马氏体和铁素体晶界对 201 奥氏体不锈钢低温变形和断裂行为的影响
IF 1.8 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-07-05 DOI: 10.2355/isijinternational.isijint-2024-091
Pham Mai Khanh, Hoang Thi Ngoc Quyen

This study focuses on the fracture mode of 201 austenitic steel at room temperature (RT) and at -40 °C for one hour and three hours. The results reveal that at room temperature, the fracture is dominated by ductile behavior. At - 40 °C, the fracture mode is a mix of ductile and brittle behavior. Type 201 austenitic stainless steel has a low stacking fault energy value (about 16 mJ.m-2 at RT), leading to the activation of the transformation-induced plasticity (TRIP) effect. When the sample is soaked at -40 °C for three hours, deformation-induced martensite transition (DIMT) formation with the volume fraction rises significantly to 19.9 %. At -40 °C for 3 hours, the alloy's impact energy absorption is reduced by 39%. The interaction of deformed austenite grains with previous austenite grain boundaries results in the formation of serrated grain boundaries in samples soaked at -40 °C. Serrated grain boundaries prevent crack propagation and reduce crack expansion at the grain boundary during the fracture of this alloy. The width of the crack at serrated grain boundaries is 38% less than that of the straight grain boundary.

本研究主要探讨了 201 奥氏体钢在室温(RT)和 -40 ° C 下 1 小时和 3 小时的断裂模式。结果表明,在室温下,断裂以韧性行为为主。在-40 °C时,断裂模式是韧性和脆性行为的混合。201 型奥氏体不锈钢的堆叠断层能值较低(在室温下约为 16 mJ.m-2),导致了转化诱导塑性(TRIP)效应的激活。将样品在 -40 °C 下浸泡 3 小时后,会形成变形诱导马氏体转变(DIMT),其体积分数显著上升至 19.9%。在 -40 °C 下浸泡 3 小时后,合金的冲击能量吸收率降低了 39%。变形奥氏体晶粒与先前奥氏体晶界的相互作用导致在-40 °C下浸泡的样品中形成锯齿状晶界。锯齿状晶界可阻止裂纹扩展,并减少该合金断裂时晶界处的裂纹扩展。锯齿状晶界的裂纹宽度比直晶界的裂纹宽度小 38%。
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引用次数: 0
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