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Polymer-Particle Enhanced Visible Light Range Photocatalytic Activity on Textile Applications 聚合物颗粒增强可见光范围光催化活性在纺织品中的应用
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021011
Asena Cerhan Haink, G. Basim
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引用次数: 0
Mechanochemical Preparation of Mineral Based Adsorbent and Its Effective Purification Ability for Wastewater 矿物基吸附剂的机械化学制备及其对废水的有效净化能力
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021012
Huimin Hu, Qiwu Zhang
With the economic development, environmental pollution is getting worse in many developing countries including China. Traditional processing as CaO neutralization of acidic solutions is still a burden to many local governments of China and development of new process with lower cost is highly required. Mining exploitation produces large amounts of tailings in which industrial minerals such as carbonates, silicates and others have been left without proper utilization. Based on the intensive investigations in the field of mechanochemistry, we propose to use these mineral samples to deal with the purification of heavy metal polluted water by enhancing their reactivity through mechanochemical activation. The industrial minerals such as silicates (serpentine and kaolinite), carbonates (calcite) have been studied for the purposes on removal of contaminants from solution. In addition, the synergistic effects from mixtures of calcite with other material have been investigated to give their excellent adsorbent performance for purification of the wastewater. This review summarizes the recent progresses for mechanochemical preparation of mineral based adsorbent and its effective purification ability for toxic matter-containing wastewater.
随着经济的发展,包括中国在内的许多发展中国家的环境污染越来越严重。作为酸性溶液中和CaO的传统工艺对中国许多地方政府来说仍然是负担,迫切需要开发成本更低的新工艺。采矿开采产生了大量的尾矿,其中的工业矿物如碳酸盐、硅酸盐等未得到合理利用。在机械化学领域深入研究的基础上,我们提出利用这些矿物样品通过机械化学活化提高其反应活性来处理重金属污染水的净化。对工业矿物如硅酸盐(蛇纹石和高岭石)、碳酸盐(方解石)等进行了去除溶液中污染物的研究。此外,还研究了方解石与其他材料混合后的协同作用,使其具有良好的吸附净化废水的性能。综述了近年来机械化学法制备矿物基吸附剂的研究进展及其对含有毒废水的有效净化能力。
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引用次数: 3
Particle Preparation and Morphology Control with Mutual Diffusion Across Liquid-Liquid Interfaces 液-液界面相互扩散的粒子制备和形态控制
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021006
Kazunori Kadota, Y. Shirakawa
Advanced functional materials require sophisticated control of particle characteristics. The bottom-up process has been extensively used to produce functional materials for controlling the particle properties of composite particles. We propose crystallization at liquid-liquid interfaces as an advanced particle formation method. This review introduces crystallization at a liquid-liquid interface based on several case studies used in various applications. Conventional crystallization has been generally used to produce crystals and particles with homogeneous particle properties. Liquid-liquid interfacial crystallization makes it possible to create composite particles with hetero-phase structures and interfaces. Liquid-liquid interfacial crystallization with an inkjet technique can control the droplet size accurately, and the shape and particle size distribution are successfully controlled in inorganic-organic composite particles. In addition, we succeed in creating organic-organic composite particles using the interfacial crystallization by an ultrasonic spray nozzle. The coating efficiency of organic particles on the particles is enhanced using the ultrasonic spray nozzle in comparison with anti-solvent crystallization. In this study, the fabrication of inorganic-organic composite particles using a coaxial tube reactor on the liquid-liquid interfacial crystallization is proven successful. These findings suggest that liquid-liquid interfacial crystallization is a promising means of efficiently producing composite particles because of their applicability to infusion in various processes.
先进的功能材料需要对颗粒特性进行精密的控制。自底向上工艺已被广泛应用于控制复合颗粒颗粒性能的功能材料的生产。我们提出在液-液界面上结晶作为一种先进的粒子形成方法。这篇综述介绍了在液-液界面的结晶基于几个案例研究在各种应用。常规结晶通常用于生产具有均匀颗粒性质的晶体和颗粒。液-液界面结晶使制备具有异相结构和界面的复合粒子成为可能。采用喷墨技术进行液-液界面结晶可以精确地控制液滴的大小,成功地控制了无机-有机复合颗粒的形状和粒径分布。此外,我们还成功地利用超声波喷嘴的界面结晶制备了有机-有机复合颗粒。与反溶剂结晶相比,超声波喷嘴可提高有机颗粒在颗粒上的包覆效率。在本研究中,利用同轴管反应器在液-液界面结晶上成功制备了无机-有机复合颗粒。这些发现表明,液-液界面结晶是一种很有前途的高效生产复合颗粒的方法,因为它适用于各种工艺的灌注。
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引用次数: 2
Scaling-up the Calcium-Looping Process for CO2 Capture and Energy Storage 二氧化碳捕获和能量储存的钙循环过程的放大
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021005
Carlos Ortiz, J. Valverde, R. Chacartegui, L. Pérez-Maqueda, Pau Gimenez-Gavarrell
The Calcium-Looping (CaL) process has emerged in the last years as a promising technology to face two key challenges within the future energy scenario: energy storage in renewable energy-based plants and CO 2 capture from fossil fuel combustion. Based on the multicycle calcination-carbonation reaction of CaCO 3 for both thermochemical energy storage and post-combustion CO 2 capture applications, the operating conditions for each application may involve remarkably different characteristics regarding kinetics, heat transfer and material multicycle activity performance. The novelty and urgency of developing these applications demand an important effort to overcome serious issues, most of them related to gas-solids reactions and material handling. This work reviews the latest results from international research projects including a critical assessment of the technology needed to scale up the process. A set of equipment and methods already proved as well as those requiring further demonstration are discussed. An emphasis is put on critical equipment such as gas-solids reactors for both calcination and carbonation, power block integration, gas and solids conveying systems and auxiliary equipment for both energy storage and CO 2 capture CaL applications.
在过去的几年里,钙循环(CaL)工艺作为一种有前途的技术出现了,它面临着未来能源情景中的两个关键挑战:可再生能源工厂的能量储存和化石燃料燃烧产生的二氧化碳捕获。基于用于热化学储能和燃烧后co2捕集的caco3多循环煅烧-碳化反应,每种应用的操作条件在动力学、传热和材料多循环活性性能方面可能涉及显著不同的特征。开发这些应用的新颖性和紧迫性要求我们努力克服一些严重的问题,其中大多数与气固反应和材料处理有关。这项工作审查了国际研究项目的最新成果,包括对扩大该过程所需技术的关键评估。讨论了一套已验证的设备和方法,以及需要进一步验证的设备和方法。重点放在关键设备上,如用于煅烧和碳化的气固反应器、电源块集成、气体和固体输送系统以及用于储能和CO 2捕获CaL应用的辅助设备。
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引用次数: 32
Fabrication and Characterization of Prussian Blue-Derived Iron Carbide-Iron Oxide Hybrid on Reduced Graphene Oxide Nanosheets 还原氧化石墨烯纳米片上普鲁士蓝衍生碳化铁-氧化铁杂化物的制备与表征
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021015
Alowasheeir Azhar, Jacob Earnshaw, Mohamed B Zakaria, Mohamed B Zakaria, P. Cheng, Y. V. Kaneti, M. S. Hossain, S. Alshehri, T. Ahamad, Y. Yamauchi, Y. Yamauchi, Jongbeom Na, Jongbeom Na
This work demonstrates the fabrication of a nanoporous iron carbide-iron oxide/reduced graphene oxide (IC-IO/ rGO) hybrid via a controlled one-step thermal treatment of Prussian blue (PB)/GO hybrid at 450 °C under N2 flow. The PB/GO hybrid is initially prepared through the in-situ deposition of PB nanoparticles on the GO sheets through electrostatic interactions. The morphological analysis of the hybrid reveals the uniform coverage of the rGO sheets by IC-IO nanoparticles and the even distribution of carbon (C), oxygen (O), and iron (Fe) on the rGO nanosheets. As a result of the hybrid composition and controlled morphology, the surface area of the obtained IC-IO/rGO hybrid (~40 m2/g) is significantly enhanced compared to those of the calcined GO sheets and PB nanoparticles (without GO).
这项工作展示了通过在450°C的氮气流下对普鲁士蓝(PB)/氧化石墨烯杂化物进行一步热处理,制备纳米多孔碳化铁-氧化铁/还原性氧化石墨烯(IC-IO/ rGO)杂化物。通过静电相互作用将PB纳米颗粒原位沉积在氧化石墨烯薄片上,初步制备了PB/GO杂化物。形貌分析表明,IC-IO纳米颗粒在氧化石墨烯纳米片上均匀覆盖,碳(C)、氧(O)和铁(Fe)在氧化石墨烯纳米片上均匀分布。由于杂化的组成和控制的形貌,得到的IC-IO/rGO杂化物的表面积(~40 m2/g)比煅烧的氧化石墨烯片和PB纳米颗粒(不含氧化石墨烯)的表面积显著增强。
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引用次数: 3
A Semi-Automated DEM Parameter Calibration Technique of Powders Based on Different Bulk Responses Extracted from Auger Dosing Experiments 基于螺旋钻加药实验中不同体积响应的粉末半自动化DEM参数标定技术
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021010
B. Kassem, Nizar Salloum, T. Brinz, Y. Heider, B. Markert
Discrete Element Method (DEM) proved to be an essential tool to optimize the industrial auger dosing process for pharmaceutical powders. During the DEM parameter calibration process of a certain powder, several parameter combinations might lead to a similar bulk response, which could also vary for other bulk responses. Therefore, a methodology is needed in order to narrow down the number of combinations and be at once close to reality representation. In this study, a vertical auger dosing setup is used as a standard calibration device to extract three different bulk responses, i.e., angle of repose, bulk density, and mass flow rate. Simulations using LIGGGHTS software package are performed based on Design of Experiments (DoE) by varying four input factors, i.e., auger speed, particle-particle and particle-wall static friction coefficients, and particle-particle rolling friction coefficient. The successful application of multivariate regression analysis (MVRA) results in predicting the bulk behavior within the studied ranges of parameters. In this regard, clustering the different predicted behaviors of the three responses together allows to dramatically reduce the admissible parameter combinations. Consequently, an optimized set of calibrated DEM parameters is chosen, where the simulation results accurately match the experimental reference data. This simple dynamic calibration tool proves to strongly verify and predict the flowability of free-flowing bulk materials.
离散元法(DEM)已被证明是优化工业螺杆给药工艺的重要工具。在某一粉体的DEM参数标定过程中,几种参数组合可能会导致相似的体响应,其他体响应也可能不同。因此,需要一种方法来缩小组合的数量,并立即接近现实的表现。在本研究中,使用垂直螺旋加药装置作为标准校准装置来提取三种不同的体积响应,即休止角、体积密度和质量流量。基于实验设计(Design of Experiments, DoE),通过改变螺旋钻速度、颗粒-颗粒和颗粒-壁面静摩擦系数、颗粒-颗粒滚动摩擦系数4个输入因素,利用lighghts软件包进行了模拟。多变量回归分析(MVRA)的成功应用,可以在研究的参数范围内预测块体行为。在这方面,将三个响应的不同预测行为聚类在一起可以大大减少可接受的参数组合。因此,选择一组优化的校准DEM参数,使模拟结果与实验参考数据准确匹配。这个简单的动态校准工具被证明可以有效地验证和预测自由流动的散装材料的流动性。
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引用次数: 7
Recent Progress in Efficient Gas–Solid Cyclone Separators with a High Solids Loading for Large-scale Fluidized Beds 大型流化床高固载高效气固旋风分离器研究进展
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021001
C. Fushimi, Kentaro Yato, M. Sakai, T. Kawano, Teruyuki Kita
Circulating fluidized beds (CFB)s are important technical equipment to treat gas–solid systems for fluid catalytic cracking, combustion, gasification, and high-temperature heat receiving because their mass and heat transfer rates are large. Cyclones are important devices to control the performance of CFBs and ensure their stable operation; heat-carrying and/or solid catalyst particles being circulated in a CFB should be efficiently separated from gas at a reduced pressure loss during separation. In commercial CFBs, a large amount of solids (> 1 kg-solid (m 3 -gas) –1 or > 1 kg-solid (kg-gas) –1 ) is circulated and should be treated. Thus, gas–solid cyclones with a high solids loading should be developed. A large number of reports have been published on gas–solid separators, including cyclones. In addition, computational fluid dynamics (CFD) technology has rapidly developed in the past decade. Based on these observations, in this review, we summarize the recent progress in experimental and CFD studies on gas– solid cyclones. The modified pressure drop model, scale-up methodology, and criteria for a single large cyclone vs. multiple cyclones are explained. Future research perspectives are also discussed.
循环流化床(CFB)由于其传质和传热速率大,是处理流体催化裂化、燃烧、气化和高温吸热等气固系统的重要技术设备。旋流器是控制循环流化床性能、保证循环流化床稳定运行的重要装置;在循环流化床中循环的载热和/或固体催化剂颗粒应在分离过程中减少压力损失的情况下有效地从气体中分离出来。在商业循环流化床中,有大量的固体(> 1kg -solid (m3 -gas) -1或> 1kg -solid (kg-gas) -1)循环,需要进行处理。因此,应开发具有高固体负荷的气固旋风分离器。已经发表了大量关于气固分离器的报告,包括旋风分离器。此外,计算流体力学(CFD)技术在过去十年中得到了迅速发展。在此基础上,本文综述了近年来气固旋流器的实验和CFD研究进展。修正的压降模型,放大的方法,和标准的一个大旋风与多个旋风的解释。展望了未来的研究方向。
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引用次数: 8
Static and Dynamic Stickiness Tests to Measure Particle Stickiness 用于测量颗粒粘性的静态和动态粘性测试
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021017
J. G. S. Erik, Fuweng Zhang, van Steijn Volkert, V.H.O Ruud, M. H. M. Gabrie
Sticking of particles has a tremendous impact on powder-processing industries, especially for hygroscopic amorphous powders. A wide variety of experimental methods has been developed to measure at what combinations of temperature and moisture content material becomes sticky. This review describes, for each method, how so-called stickiness curves are determined. As particle velocity also plays a key role, we classify the methods into static and dynamic stickiness tests. Static stickiness tests have limited particle motion during the conditioning step prior to the measurement. Thus, the obtained information is particularly useful in predicting the long-term behavior of powder during storage or in packaging. Dynamic stickiness tests involve significant particle motion during conditioning and measurement. Stickiness curves strongly depend on particle velocity, and the obtained information is highly relevant to the design and operation of powder production and processing equipment. Virtually all methods determine the onset of stickiness using powder as a starting point. Given the many industrial processes like spray drying that start from a liquid that may become sticky upon drying, future effort should focus on developing test methods that determine the onset of stickiness using a liquid droplet as a starting point.
颗粒的粘着对粉末加工工业,特别是吸湿性非晶粉末产生了巨大的影响。已经开发了各种各样的实验方法来测量在什么温度和水分含量的组合下材料变得粘稠。这篇综述描述了每种方法如何确定所谓的粘性曲线。由于粒子速度也起着关键的作用,我们将这种方法分为静态和动态粘性测试。静态粘性测试在测量前的调节步骤中具有有限的颗粒运动。因此,所获得的信息在预测粉末在储存或包装期间的长期行为时特别有用。动态粘性测试在调节和测量过程中涉及明显的颗粒运动。黏性曲线与颗粒速度有很大关系,所得信息与粉体生产加工设备的设计和运行密切相关。几乎所有的方法都用粉末作为起始点来确定粘性的开始。考虑到许多工业过程,如喷雾干燥,从可能在干燥时变得粘稠的液体开始,未来的努力应该集中在开发测试方法上,以液滴作为起点来确定粘稠的开始。
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引用次数: 4
General Information 一般信息
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021024
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引用次数: 0
3rd International Hosokawa Powder Technology Symposium Held in China 第三届细川粉体技术国际研讨会在中国召开
IF 4.1 4区 材料科学 Q3 ENGINEERING, CHEMICAL Pub Date : 2021-01-10 DOI: 10.14356/kona.2021022
As the special event aiming at the globalization in Asia of the Hosokawa Powder Technology Foundation, the 3rd International Hosokawa Powder Technology Symposium took place on Tuesday, November 19, 2019, at the Shanghai Institute of Ceramics of the Chinese Academy of Sciences (SICCAS) in China. This International Hosokawa Powder Technology Symposium was held abroad for the third time after the first one (2014, at Hosokawa Alpine AG in Augsburg, Germany) and the second (2017, at Hosokawa Micron Powder Systems Div. in New Jersey, U.S.A.) organized by the Hosokawa Powder Technology Foundation (HPTF). It was co-organized by the SICCAS and the Society of Powder Technology, Japan (SPTJ) and supported by the Hosokawa Micron Corporation (HMC) and Hosokawa Micron (Shanghai) Powder Machinery Co., Ltd. (HMS). At the symposium, five lectures were given on the theme of “Powder and Particle Technology for Advanced Materials” after the opening remarks of President Yoshio Hosokawa. In the first lecture, high-purity, ultra-fine powder production and processing technologies for advanced materials such as ultra-high temperature heat-resistant rocket members, reflectors, and transparent materials were presented. Then the new nanoparticle size measuring devices, and the in-situ and real-time nanoparticle measurement using this device was introduced. The third lecture was concerning the functional materials based on the form of natural organisms to create new innovative functionalities. After the lectures by the Chinese professors, two presentations were given from the Hosokawa Group on the application of powder processing technology to various industrial product fields, and the devel opment and commercialization of cosmetics and pharmaceuticals using PLGA nanoparticles. Finally, Mr. Uchida of HMS closed the conference with the closing remarks. The symposium
2019年11月19日(星期二),作为细川粉体技术基金会面向亚洲全球化的特别活动,第三届细川粉体技术国际研讨会在中国科学院上海陶瓷研究所隆重举行。本届国际细川粉体技术研讨会是继第一届(2014年在德国奥格斯堡的细川高山股份公司)和第二届(2017年在美国新泽西州细川美光粉体系统公司)之后,第三次在国外举行的。会议由中国科学院和日本粉末技术学会(SPTJ)共同主办,细川美光株式会社(HMC)和细川美光(上海)粉末机械有限公司(HMS)共同支持。研讨会上,细川义夫会长致开幕词后,以“先进材料的粉末与颗粒技术”为主题进行了五场演讲。第一讲介绍了超高温耐热火箭构件、反射镜、透明材料等先进材料的高纯度、超细粉体生产和加工技术。然后介绍了新型纳米颗粒尺寸测量装置,以及利用该装置进行纳米颗粒的原位实时测量。第三讲的是基于自然生物形态的功能材料,创造新的创新功能。在中国教授的讲座之后,细川集团做了两个报告,分别是粉末加工技术在各个工业产品领域的应用,以及使用PLGA纳米粒子的化妆品和药品的开发和商业化。最后,内田先生以闭幕词结束了会议。《会饮篇》
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引用次数: 0
期刊
KONA Powder and Particle Journal
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