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Study of the Physic-Mechanical Properties of a Typha Concrete Composites: A Possible New Material for Sustainable Construction 香蒲混凝土复合材料的物理力学性能研究:一种可能用于可持续建筑的新材料
Pub Date : 2024-05-21 DOI: 10.4028/p-bxp2lf
El Moustapha Elhaj-Maham, Babacar Diouf, El Hadji Babacar Ly, Moise Manga
Natural fibers have garnered considerable attention from researchers and academics alike due to their eco-friendly nature and sustainability. These fibers are being explored for their potential use in polymer composites. The use of natural fiber-reinforced polymer composite materials is rapidly increasing in both industrial and fundamental research applications due to their renewable, low, and biodegradable properties. In order to reduce the CO2 emissions, the building energy consumption and preserve the natural sand. The present study involved conducting an analysis of the results obtained from the experimental investigation where five mixtures of typha fiber sand, and cement (MHC0, MHC5, MHC10, MHC15 and MHC20)) were utilized to make Typha-concrete. The experimental mixtures being examined and the results indicate that the density of the samples diminishes in proportion to the incorporation of typha fiber, while the thermal conductivity is enhanced. In addition, the characteristics of lightweight structures can be attributed to the generated specimens, which have been determined by their documented compressive strength. Based on the results of RILEM's functional classification analysis, it can be concluded that Typha-concrete meets the mechanical and thermal requirements of construction materials, making it a feasible option for both structural and insulating concrete applications.
天然纤维因其环保性和可持续性而受到研究人员和学术界的广泛关注。人们正在探索这些纤维在聚合物复合材料中的潜在用途。由于天然纤维具有可再生、低成本和可生物降解的特性,因此在工业和基础研究应用中,天然纤维增强聚合物复合材料的使用正在迅速增加。为了减少二氧化碳排放、降低建筑能耗并保护天然沙土。本研究包括对实验调查所获得的结果进行分析,其中利用了五种香蒲纤维砂和水泥的混合物(MHC0、MHC5、MHC10、MHC15 和 MHC20)来制造香蒲混凝土。对实验混合物进行了检验,结果表明,样品的密度随着香蒲纤维的加入成比例地减小,而导热性能却得到了提高。此外,轻质结构的特点还可归因于所生成的试样,这些试样是根据其抗压强度文件确定的。根据 RILEM 的功能分类分析结果,可以得出结论:香蒲混凝土符合建筑材料的机械和热要求,使其成为结构和隔热混凝土应用的可行选择。
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引用次数: 0
The Effect of Bleaching Variation on Schoutenia Ovata Korth Fiber as a Composite Reinforcement 漂白变化对作为复合材料增强材料的 Schoutenia Ovata Korth 纤维的影响
Pub Date : 2024-05-21 DOI: 10.4028/p-55sktf
A. Andoko, Riduwan Prasetya
The study examined the properties of bleached Schoutenia ovata Korth Fiber (SF) for prospective application in composite reinforcement. .The characterization of SF was done using FTIR and SEM-EDS techniques to examine the morphology of SF following treatment with NaOH and various concentrations of NaClO. The treatment improved the interaction between the fiber and the composite matrix. As a result, fibers require bleaching before they may be processed further.
该研究考察了漂白 Schoutenia ovata Korth 纤维(SF)的特性,以展望其在复合材料加固中的应用。采用傅立叶变换红外光谱(FTIR)和扫描电子显微镜-电子显微镜(SEM-EDS)技术对SF进行了表征,以检查SF经NaOH和不同浓度的NaClO处理后的形态。处理改善了纤维与复合材料基体之间的相互作用。因此,纤维在进一步加工之前需要漂白。
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引用次数: 0
Optimizing Micro Friction Stir Spot Welding (mFSSW) of Aluminum Alloy AA1100 Using Neural Network Model 利用神经网络模型优化铝合金 AA1100 的微摩擦点焊 (mFSSW)
Pub Date : 2024-05-21 DOI: 10.4028/p-bbosi6
Tri Haryanto Soleh Atmaja, L. A. Safitri, P. Rupajati, A. Baskoro
This study explores the optimization of Micro Friction Stir Spot Welding (mFSSW) by investigating the influence of tool profiles on welding outcomes, using aluminum alloy AA1100 with a 0.42 mm thickness as the specimen material. Monitoring temperature and RPM during welding with thermocouples and tachometers, mechanical properties are assessed through tensile shear tests, microhardness measurements, and macrostructural observations. The findings serve as the basis for developing Neural Network models using Rapidminer software, marking a transformative development that positions Neural Networks as potent tools for optimizing welding processes, potentially leading to achieving optimal weld quality. The investigation also delves into three welding tool configurations – the two-stage pin, one-stage pin, and pinless mFSSW probes – highlighting their distinct impacts on tensile shear test values and overall welding quality. Notably, the two-stage pin configuration emphasizes the significance of larger pin diameters and controlled heat generation for enhanced weld strength, while the one-stage pin configuration underscores the pivotal role of pin diameter and elevated temperatures in improving weld quality. The pinless mFSSW probe configuration, on the other hand, emphasizes the importance of shoulder diameter and temperature control for superior tensile shear test results. Leveraging Neural Network modeling for optimization, this study advances our understanding of parameter interactions and underscores the efficacy of Neural Networks in achieving superior tensile shear test values and welding quality in mFSSW, offering valuable insights for future endeavors in the field..
本研究以厚度为 0.42 毫米的铝合金 AA1100 为试样材料,通过研究工具轮廓对焊接结果的影响,探索微摩擦搅拌点焊 (mFSSW) 的优化方法。使用热电偶和转速计监测焊接过程中的温度和转速,通过拉伸剪切试验、显微硬度测量和宏观结构观察评估机械性能。研究结果是使用 Rapidminer 软件开发神经网络模型的基础,标志着将神经网络定位为优化焊接过程的有效工具的变革性发展,有可能实现最佳焊接质量。调查还深入研究了三种焊接工具配置--两级销钉、一级销钉和无销钉 mFSSW 探头--突出了它们对拉伸剪切测试值和整体焊接质量的不同影响。值得注意的是,两级销钉结构强调了较大销钉直径和可控发热对提高焊接强度的重要性,而一级销钉结构则强调了销钉直径和高温对提高焊接质量的关键作用。另一方面,无针 mFSSW 探头配置强调了肩部直径和温度控制对获得优异拉伸剪切测试结果的重要性。这项研究利用神经网络建模进行优化,加深了我们对参数相互作用的理解,并强调了神经网络在实现优异的拉伸剪切测试值和 mFSSW 焊接质量方面的功效,为该领域未来的工作提供了宝贵的见解。
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引用次数: 0
Hardness and Microstructure of TiN Coating on Aluminum Alloy with DC Sputtering 铝合金直流溅射 TiN 涂层的硬度和微观结构
Pub Date : 2024-05-21 DOI: 10.4028/p-2clvvz
Margono Margono, D. Darmadi, T. D. Widodo, Suprapto Suprapto, T. Sujitno, Muhammad Kozin
Titanium Nitride coating has attracted much interest in increasing the hardness of aluminum alloys. This study aims to investigate the effect of Ar: N gas mixture and time on increasing the hardness of aluminum alloys using DC sputtering. Preparation of TiN thin films on aluminum alloy substrates using flowing gas mixture parameters and time. First, the layer of TiN was deposited on the sample with a gas mixture of 90Ar:10N; 80Ar:20N; 70Ar:30N; and 60Ar:40N (%) for 60 minutes. Then the optimum gas mixture that produces the highest surface hardness is used in the second process with time variations of 30, 60, 90, and 120 minutes. The results showed that the highest hardness was achieved in a gas mixture of 70Ar:30N and 60 minutes. The TiN phase formed on the aluminum surface was identified by XRD, while the surface morphology was observed by SEM. Compared with untreated samples, the hardness of treated samples increased significantly.
氮化钛涂层在提高铝合金硬度方面备受关注。本研究旨在探讨 Ar:N 混合气体和时间对使用直流溅射提高铝合金硬度的影响。利用流动混合气体参数和时间在铝合金基底上制备 TiN 薄膜。首先,在 90Ar:10N、80Ar:20N、70Ar:30N 和 60Ar:40N(%)的混合气体中将 TiN 层沉积在样品上 60 分钟。然后在第二道工序中使用产生最高表面硬度的最佳混合气体,时间分别为 30、60、90 和 120 分钟。结果表明,70Ar:30N 的混合气体和 60 分钟的时间可产生最高的硬度。铝表面形成的 TiN 相是通过 XRD 确定的,而表面形貌则是通过 SEM 观察的。与未处理的样品相比,处理后样品的硬度明显提高。
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引用次数: 0
Parameter Design of Sand Casting to Minimize Shrinkage Defects, Porosity Defects and Incomplete Defects 最小化收缩缺陷、孔隙缺陷和不完整缺陷的砂型铸造参数设计
Pub Date : 2024-05-21 DOI: 10.4028/p-ck89wq
Syah Rizal Muzaqqi, S. Suprayitno, Y. Pradana
Casting is one of the most commonly used manufacturing method for geometrically complex product. Among the casting technologies, sand casting is often found in application. Beside the advantages of the sand-casting process, it also has a drawback that is often encountered, namely product defects. Product defects can be caused by a lack of attention to sand casting parameters. This work aims to minimize those defects, including porosity defects, shrinkage defects and incomplete defects by optimizing process parameters using the Taguchi method. The identified sand-casting process parameters include gating location, riser location, molding conditions and pouring temperature with each parameter consisting of 3 levels. This research using the fractional factorial L9 (34). Data processing is carried out by analysis of mean (ANOM) to obtain plot effects. The results showed that the optimal combination of parameters that resulted in shrinkage, porosity and minimal incomplete defects were at gating location level 2, riser location level 1, mold condition level 2 and pouring temperature level 3. The results of the comparison before and after optimization were an increase of 0.77, where previously it was 1.30 to 2.07 based on normalized data.
铸造是几何形状复杂产品最常用的制造方法之一。在各种铸造技术中,砂型铸造经常被应用。除了砂型铸造工艺的优点外,它还有一个经常遇到的缺点,即产品缺陷。产品缺陷可能是由于对砂型铸造参数缺乏关注造成的。这项工作旨在通过使用田口方法优化工艺参数,最大限度地减少这些缺陷,包括气孔缺陷、收缩缺陷和不完整缺陷。确定的砂型铸造工艺参数包括浇口位置、冒口位置、成型条件和浇注温度,每个参数包含 3 个等级。本研究采用分数因子 L9 (34)。通过均值分析(ANOM)对数据进行处理,得出小区效应。结果表明,导致收缩率、孔隙率和最小不完整缺陷的最佳参数组合是浇口位置 2 级、冒口位置 1 级、模具条件 2 级和浇注温度 3 级。优化前后的比较结果是,根据归一化数据,收缩率增加了 0.77,而之前的收缩率为 1.30 至 2.07。
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引用次数: 0
Optimization of the Co-Production between the Rice Husk and the Pulp of the Cashew Apple Produced in the Natural Region of Casamance 优化卡萨芒斯自然区生产的腰果的稻壳和果肉之间的合作生产
Pub Date : 2024-05-21 DOI: 10.4028/p-k8uyif
Omar Kata Faye, P. B. Himbane, L. Ndiaye
Anaerobic digestion or anaerobic digestion is a biological process of degradation of organic matter in an anaerobic environment. It involves the degradation and stabilization of complex organic matter by a consortium of micro-organisms leading to methane-rich biogas that can be used as an alternative energy to fossil fuels. In addition, the use of biogas allows for the preservation of the environment and the sustainable development of rural areas and landlocked regions, as well as the diversification of energy resources, but also contributes to the development of agriculture through the production of organic fertilizer. In 2018, Senegal was ranked as the 15th world exporter of cashew nuts with a production of around 18,000 tons per year according to a study by PADEC (Support Program for the Development of Casamance). Four regions mainly invest in it: Kolda, Ziguinchor, Sédhiou, and Fatick. However, in the natural region of Casamance ( Kolda, Ziguinchor, and Sédhiou), each year, after the cashew nut campaign, more than 342,000 tons of cashew apples, pressed or not, are rejected without any recovery, thus degrading in the environment. In addition, rice is traditionally grown in Casamance and in some Diola circles, it had become one of the criteria of wealth, which explains why it occupied most of the cultivated areas and each year thousands of tons of rice husk are burned for elimination/reduction without any recovery. These immense annual productions of waste, without any recovery, in a context dominated by a deficit in cooking and lighting energy constitutes a form of energy resilience and motivates us to study the co-digestion of the rice husk (with a report of C/N equal to 101.317) on cashew apple pulp (having a C/N ratio of 23.201 ). The study of the co-digestion of rice husk and apple pulp at the laboratory scale with the inoculum reveals, that the co-digestion with pH correction contains 39.40% methane and 51.50% carbon dioxide after 49 days of production and 64.04% methane (CH4) and 25.86% carbon dioxide (CO2) on the 96th day. For co-digestion without adjustment, production stopped on the 49th day with a production of 23.68% methane and 45.65% carbon dioxide.
厌氧消化或厌氧分解是一种在厌氧环境中降解有机物的生物过程。它涉及微生物群对复杂有机物的降解和稳定,从而产生富含甲烷的沼气,沼气可用作化石燃料的替代能源。此外,使用沼气可以保护环境,促进农村地区和内陆地区的可持续发展,实现能源资源的多样化,还可以通过生产有机肥料促进农业发展。根据卡萨芒斯发展支持计划(PADEC)的研究,2018 年,塞内加尔以每年约 1.8 万吨的腰果产量位列世界腰果出口国第 15 位。卡萨芒斯主要有四个投资地区:科尔达(Kolda)、济金绍尔(Ziguinchor)、塞迪乌(Sédhiou)和法提克(Fatick)。然而,在卡萨芒斯的自然区(科尔达、济金绍尔和塞迪乌),每年腰果活动结束后,超过 34.2 万吨的腰果苹果(无论是否压榨)都会被丢弃,没有得到任何回收,从而造成环境退化。此外,卡萨芒斯地区传统上种植水稻,在一些迪奥拉人的圈子里,水稻已成为致富的标准之一,这也解释了为什么水稻占据了大部分耕地面积,每年有数千吨稻壳被焚烧销毁/减少,没有任何回收。在烹饪和照明能源短缺的情况下,每年产生的这些大量废弃物没有得到任何回收,这构成了一种能源复原形式,促使我们研究将稻壳(C/N 报告为 101.317)与腰果果肉(C/N 比率为 23.201)共同消化的问题。对稻壳和苹果浆在实验室规模上与接种物共同消化的研究表明,经过 pH 值校正的共同消化在生产 49 天后含有 39.40% 的甲烷和 51.50% 的二氧化碳,在第 96 天含有 64.04% 的甲烷(CH4)和 25.86% 的二氧化碳(CO2)。对于未进行调节的共消化,生产在第 49 天停止,甲烷和二氧化碳的产量分别为 23.68% 和 45.65%。
{"title":"Optimization of the Co-Production between the Rice Husk and the Pulp of the Cashew Apple Produced in the Natural Region of Casamance","authors":"Omar Kata Faye, P. B. Himbane, L. Ndiaye","doi":"10.4028/p-k8uyif","DOIUrl":"https://doi.org/10.4028/p-k8uyif","url":null,"abstract":"Anaerobic digestion or anaerobic digestion is a biological process of degradation of organic matter in an anaerobic environment. It involves the degradation and stabilization of complex organic matter by a consortium of micro-organisms leading to methane-rich biogas that can be used as an alternative energy to fossil fuels. In addition, the use of biogas allows for the preservation of the environment and the sustainable development of rural areas and landlocked regions, as well as the diversification of energy resources, but also contributes to the development of agriculture through the production of organic fertilizer. In 2018, Senegal was ranked as the 15th world exporter of cashew nuts with a production of around 18,000 tons per year according to a study by PADEC (Support Program for the Development of Casamance). Four regions mainly invest in it: Kolda, Ziguinchor, Sédhiou, and Fatick. However, in the natural region of Casamance ( Kolda, Ziguinchor, and Sédhiou), each year, after the cashew nut campaign, more than 342,000 tons of cashew apples, pressed or not, are rejected without any recovery, thus degrading in the environment. In addition, rice is traditionally grown in Casamance and in some Diola circles, it had become one of the criteria of wealth, which explains why it occupied most of the cultivated areas and each year thousands of tons of rice husk are burned for elimination/reduction without any recovery. These immense annual productions of waste, without any recovery, in a context dominated by a deficit in cooking and lighting energy constitutes a form of energy resilience and motivates us to study the co-digestion of the rice husk (with a report of C/N equal to 101.317) on cashew apple pulp (having a C/N ratio of 23.201 ). The study of the co-digestion of rice husk and apple pulp at the laboratory scale with the inoculum reveals, that the co-digestion with pH correction contains 39.40% methane and 51.50% carbon dioxide after 49 days of production and 64.04% methane (CH4) and 25.86% carbon dioxide (CO2) on the 96th day. For co-digestion without adjustment, production stopped on the 49th day with a production of 23.68% methane and 45.65% carbon dioxide.","PeriodicalId":18262,"journal":{"name":"Materials Science Forum","volume":"20 6","pages":""},"PeriodicalIF":0.0,"publicationDate":"2024-05-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141117384","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The Effect of Friction Stir Weld (FSW) Process Parameters on Tensile Strength, Macro Structure, and Hardness in Results of AA7075 Butt Joints 摩擦搅拌焊 (FSW) 工艺参数对 AA7075 对接接头拉伸强度、宏观结构和硬度结果的影响
Pub Date : 2024-05-21 DOI: 10.4028/p-elhs5v
Muhammad Fahmi Ardiansyah, L. A. Safitri, P. Rupajati, A. Baskoro
Friction Stir Welding (FSW) is an innovative technique that enhances the conventional method of joining metals. Notably ecofriendly due to its energy efficiency, FSW involves minimal energy input, reduces pollution, and saves time and costs. It finds applications in diverse sectors such as automotive, aerospace, and industry. Each material requires specific process parameters, which leads to this study focusing on identifying suitable parameters for AA7075 aluminum with a 6mm thickness. Using a tool featuring a tapered cylindrical thread pin and a flat shoulder, the study aims to investigate the influence of FSW process parameters, rotation speed, and traverse speed on the mechanical strength of butt joint connections. The study's experimental design varies these parameters and evaluates the joints through tensile strength testing, hardness testing, and macrostructural analysis. Utilizing Response Surface Methodology (RSM), the data highlights the impact of rotation and traverse speed on tensile strength. Hardness test results present variations within heat zones, analyzing the effects of the mentioned variables. The findings demonstrate minimal flash and successful surface outcomes but also identify wormholes within the stir zone (SZ). Tensile strength testing reveals a definite correlation between RPM and traverse speed with joint strength. In contrast, hardness testing indicates that these parameters do not significantly affect joint hardness. Macrostructure examination suggests RPM and traverse speed have negligible effects on the heat-affected zone. In conclusion, FSW presents a sustainable and effective welding approach with implications for multiple industries, and this research provides insights into optimizing its parameters for specific aluminum materials.
搅拌摩擦焊(FSW)是一种创新技术,它改进了传统的金属连接方法。由于其能源效率高,FSW 具有显著的生态友好性,其能源投入极低,可减少污染,节省时间和成本。它可应用于汽车、航空航天和工业等多个领域。每种材料都需要特定的工艺参数,因此本研究的重点是确定厚度为 6 毫米的 AA7075 铝的合适参数。本研究使用一种具有锥形圆柱螺纹销和平肩的工具,旨在研究 FSW 工艺参数、旋转速度和移动速度对对接连接机械强度的影响。研究的实验设计改变了这些参数,并通过拉伸强度测试、硬度测试和宏观结构分析对接头进行评估。利用响应面方法(RSM),数据突出显示了旋转和横移速度对拉伸强度的影响。硬度测试结果显示了热区内的变化,分析了上述变量的影响。测试结果表明了最小的闪光和成功的表面效果,但也发现了搅拌区(SZ)内的虫孔。拉伸强度测试显示,转速和横移速度与接头强度之间存在明确的相关性。相反,硬度测试表明,这些参数对接头硬度的影响不大。宏观结构检测表明,转速和横移速度对热影响区的影响可以忽略不计。总之,FSW 是一种可持续的有效焊接方法,对多个行业都有影响,这项研究为优化特定铝材料的参数提供了启示。
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引用次数: 0
Normal Water Effect on the Thermal and the Mechanical Properties of Jute Yarns 普通水对黄麻纱线热性能和机械性能的影响
Pub Date : 2024-05-21 DOI: 10.4028/p-8raupz
Youssef Ben Smail, Fatima Lmai, A. El Moumen, A. Imad
The production of the jute fibers and yarns in enormous amounts and their use in different fields requires an overall comprehension of the evolution of their performance during their use and before their end life. Exposing the jute yarns to the extreme environmental conditions, such as high humidity, severe weathering, severe environments, freezing environments and others can degrade the mechanical properties jute yarns. Besides, the use of these jute yarns on the appropriate applications immersed in normal water may be accelerated them to reach their end-of-life. In this work, the thermal and mechanical properties of the jute yarns immersed in normal water for different duration were evaluated. This environmental condition was selected owing to the high probability to the exposing of yarns to the immersing in normal water on outdoors which affect their performance. The thermal stability of the jute yarns was effectuated in order to explain the chemical and physical changers occurred and linked to the mechanical properties. Results show that the mechanical properties of the jute yarns degraded by along immersion in water compared to the raw one. The tensile stress and the tensile modulus are dropped by 47 % (from 52 to 28 MPa) and 46 % (from 2.28 to 1.24 GPa), respectively for the samples immersed in water along duration (9 months) compared to the raw samples. Besides, the thermal stability of the immersed samples shows that there are no significant changes except a slight high residue for the immersed ones.
黄麻纤维和纱线的生产量巨大,并被广泛应用于不同领域,因此需要全面了解其在使用过程中和报废前的性能变化。将黄麻纱暴露在极端环境条件下,如高湿度、严重风化、恶劣环境、冰冻环境等,会降低黄麻纱的机械性能。此外,将这些黄麻纱浸泡在普通水中进行适当的应用可能会加速它们的使用寿命。在这项工作中,对浸泡在普通水中不同时间的黄麻纱的热性能和机械性能进行了评估。之所以选择这种环境条件,是因为纱线在室外浸泡在普通水中很可能会影响其性能。对黄麻纱的热稳定性进行了研究,以解释所发生的化学和物理变化,并将其与机械性能联系起来。结果表明,与原黄麻纱相比,黄麻纱在水中浸泡的时间越长,其机械性能越差。与原始样品相比,浸水时间长(9 个月)的样品拉伸应力和拉伸模量分别下降了 47%(从 52 兆帕降至 28 兆帕)和 46%(从 2.28 GPa 降至 1.24 GPa)。此外,浸泡样品的热稳定性显示,除了浸泡样品的残留物略高之外,没有发生明显变化。
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引用次数: 0
Effect of Silanized Zirconium Oxide (ZrO2) Filler on Hardness of Acrylic-Based Denture Teeth 硅烷化氧化锆 (ZrO2) 填充物对丙烯酸基义齿硬度的影响
Pub Date : 2024-05-21 DOI: 10.4028/p-s4kb7u
Hubbi Hikmatu Ilma, Fahri Raihan Ashary, Fachri Kurniawan Asghar, Ardista Izdhihar Kaloka, B. Airlangga, Sumarno Sumarno
PMMA is used in dentistry as the main matrix for denture manufacture. Dentures are a substitute for natural human teeth which must have mechanical properties and are biocompatible to withstand mastication in the oral cavity. However, PMMA has poor mechanical properties, so it is necessary to add filler to the PMMA matrix. In this study zirconium oxide (ZrO2) was used as a filler because it has good mechanical properties and aesthetics. The aim of this study was to study the effect of adding ZrO2 filler on the hardness and compatibility of denture composites at concentrations ( 0%, 1%, 3%, 5%, and 7%). The bulk composite polymerization method used in the manufacture of dental composites is by mixing powdered materials in the form of PMMA, BPO as an initiator, and ZrO2 filler which has been silanized with liquid materials in the form of MMA monomer and cross-linking agent Ethylene Glycol Dimethacrylate (EGDMA). Mixing powder liquid in this method uses hand mixing in a stainless steel container until it reaches the dough phase and is packed into a mold according to ASTM for Vickers hardness tests. Heat cured polymerization technique was used for the curing process in a water bath at 74°C for 90 minutes and continued at 100°C for 30 minutes. The results obtained in this study, the addition of ZrO2 filler to a concentration of 5% showed an increase in the hardness value up to 37.6 VHN. Keywords: Denture Teeth, Composite Bulk Polymerization, Heat cured Polymerization, Zirconium Oxide
PMMA 在牙科中用作义齿制造的主要基质。假牙是天然人类牙齿的替代品,必须具有机械性能和生物相容性,以承受口腔内的咀嚼。然而,PMMA 的机械性能较差,因此有必要在 PMMA 基质中添加填料。本研究使用氧化锆(ZrO2)作为填料,因为它具有良好的机械性能和美观性。本研究的目的是研究添加 ZrO2 填料对义齿复合材料硬度和相容性的影响,其浓度分别为 0%、1%、3%、5% 和 7%。牙科复合材料生产中使用的大块复合材料聚合法是将 PMMA 形式的粉末材料、作为引发剂的 BPO 和硅烷化的 ZrO2 填料与 MMA 单体和交联剂乙二醇二甲基丙烯酸酯(EGDMA)形式的液体材料混合。在这种方法中,粉末液体的混合是在不锈钢容器中用手搅拌,直到达到面团阶段,然后按照 ASTM 标准装入模具中进行维氏硬度测试。固化过程采用热固化聚合技术,在 74°C 的水浴中固化 90 分钟,然后在 100°C 的温度下继续固化 30 分钟。研究结果表明,添加浓度为 5%的 ZrO2 填料可使硬度值提高到 37.6 VHN。关键词义齿、复合材料团聚、热固化聚合、氧化锆
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引用次数: 0
Influence of Orthophosphoric Acid Activation on the Quality of Activated Carbons 正磷酸活化对活性炭质量的影响
Pub Date : 2024-05-21 DOI: 10.4028/p-kd7gn9
Mahamane Nassirou Amadou Kiari, Affoué Tindo Sylvie Konan, Ousmaila Sanda Mamane, H. Koné, Guy Didier Fanou, Maâzou Siragi Dounounou Boukari, Maman Hamissou Ibrahim Grema, Maman Mousbahou Malam Alma, Kouassi Benjamin Yao
Activated carbon (AC) is an adsorbent material used for the removal of pollutants from wastewater. Unfortunately, these materials used by the industry are very expensive. This is why research is being conducted to produce low-cost activated carbons from natural biomass. The objective of this work is to study the effect of activation by orthophosphoric acid on the quality of activated carbons. The different techniques used for the characterization are: the Iodine number and the Methylene Blue Index. For activated carbons prepared in a single activation step, iodine number of 609.12 and methylene blue value of 102.48 mg/g were obtained. For those prepared in two activation steps, iodine number of 951.75 mg/g and methylene blue value of 115.14 mg/g were obtained.
活性炭(AC)是一种用于去除废水中污染物的吸附材料。遗憾的是,工业上使用的这些材料非常昂贵。因此,人们正在研究如何利用天然生物质生产低成本的活性炭。这项工作的目的是研究正磷酸活化对活性炭质量的影响。表征所用的不同技术包括:碘数和亚甲蓝指数。通过单一活化步骤制备的活性炭,碘值为 609.12,亚甲基蓝值为 102.48 mg/g。通过两个活化步骤制备的活性碳的碘值为 951.75 mg/g,亚甲基蓝值为 115.14 mg/g。
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Materials Science Forum
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