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Effect of SWCNT Deposition by Spraying Technique on Mechanical Properties and Electrical Conductivity of Peek Laminates 喷涂技术沉积的 SWCNT 对 Peek 层压板机械性能和导电性的影响
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-26 DOI: 10.1007/s11029-024-10210-5
M. V. Burkov, A. A. Kononova, A. V. Eremin

Hybrid composite materials reinforced with nanoscale additives provide better mechanical properties than traditional composites. Carbon-fiber-reinforced polyether ether ketone with various layups modified by 0.05-0.36 wt% of single-wall carbon nanotubes was experimentally studied. The influence of the nanotubes on the mechanical properties of the composites, found in tensile and bending tests, and on their electrical conductivity was studied and discussed. Adding 0.15 wt% of SWCNTs between layers of prepregs led to an increase in the tensile strength by 9.9% and flexural strength by 5.5%. The electrical conductivity of the unidirectional composite has not been changed significantly after the incorporation of SWCNTs, while for orthotropic layup it increases by 65%.

与传统复合材料相比,使用纳米添加剂增强的混合复合材料具有更好的机械性能。实验研究了由 0.05-0.36 wt% 的单壁碳纳米管改性的不同铺层的碳纤维增强聚醚醚酮。研究讨论了纳米管对拉伸和弯曲试验中发现的复合材料机械性能及其导电性能的影响。在预浸料层之间添加 0.15 wt% 的 SWCNT 可使拉伸强度提高 9.9%,弯曲强度提高 5.5%。加入 SWCNT 后,单向复合材料的导电性没有明显变化,而正交铺层的导电性则提高了 65%。
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引用次数: 0
Families of Stress-Strain, Relaxation, and Creep Curves Generated by a Nonlinear Model for Thixotropic Viscoelastic-Plastic Media Accounting for Structure Evolution Part 3. Creep Curves 考虑结构演变的触变粘弹性-弹性介质非线性模型生成的应力-应变、松弛和蠕变曲线族 第 3 部分.蠕变曲线
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-26 DOI: 10.1007/s11029-024-10204-3
A. V. Khokhlov, V. V. Gulin

A systematic analytical study of the mathematical properties of the previously constructed nonlinear model for shear flow of thixotropic viscoelastic-plastic media, which takes into account the mutual influence of the deformation process and structure evolution, is continued. A set of two nonlinear differential equations describing the processes of shear at a constant rate and stress relaxation is obtained. Equation set describing creep is derived; a general solution of the Cauchy problem for the set is constructed in an explicit form (the equations of the families of creep, and structuredness curves are derived). For arbitrary six material parameters and (increasing) material function that govern the model, basic properties of the families stress-strain curves at constant strain rates, stress relaxation curves and creep curves generated by the model, and the features of structuredness evolution under these types of loading are analytically studied. The dependences of these curves on time, shear rate, stress level, initial strain, and initial structuredness of the material, as well as on the material parameters and function of the model, are studied. Several indicators of the applicability of the model are found which are convenient to check with experimental data. It was examined what effects typical for viscoelastic-plastic media can be described by the model and what unusual effects (unusual properties) are generated by a change in structuredness in comparison with typical stress-strain curves, relaxation curves, and creep curves of structurally stable materials. In particular, it is proved that creep curves always increase in time and have oblique asymptote, and structuredness under constant stress is always monotonous (unlike other loading modes), but can decrease or increase depending on the relation between the stress level and initial structuredness. The same condition controls creep curves to be convex up or down: at a certain (calculated) critical load creep curves change from convexity up (under smaller loads) to convexity down, and the structuredness becomes ascending instead of descending. The analysis proved the ability of the model to describe behavior of not only liquid-like viscoelastoplastic media, but also solid-like (thickening, hardening, hardened) media: creep, relaxation, recovery, a number of typical properties of experimental relaxation curves, creep and stress-strain curves, strain rate and strain hardening, flow under constant stress and so on.

我们继续对之前构建的触变粘弹塑性介质剪切流非线性模型的数学特性进行了系统的分析研究,该模型考虑了变形过程和结构演变的相互影响。得到了描述恒定速率剪切和应力松弛过程的两个非线性微分方程组。导出了描述蠕变的方程组;以显式形式构建了方程组的考奇问题的一般解(导出了蠕变和结构度曲线的方程组)。对于支配模型的任意六个材料参数和(递增)材料函数,分析研究了恒定应变速率下的应力-应变曲线族、应力松弛曲线和模型生成的蠕变曲线的基本特性,以及在这些类型的加载下结构度演变的特征。研究了这些曲线与时间、剪切速率、应力水平、初始应变和材料初始结构度的关系,以及与材料参数和模型功能的关系。发现了模型适用性的几个指标,便于与实验数据进行核对。与结构稳定材料的典型应力-应变曲线、松弛曲线和蠕变曲线相比,研究了该模型可以描述粘弹性-塑性介质的哪些典型效应,以及结构度变化会产生哪些异常效应(异常特性)。特别是,研究证明,蠕变曲线总是随时间而增加,并具有斜渐近线,而恒定应力下的结构度总是单调的(与其他加载模式不同),但可根据应力水平和初始结构度之间的关系而减小或增大。同样的条件控制着蠕变曲线的上凸或下凸:在一定的(计算的)临界载荷下,蠕变曲线从上凸(在较小载荷下)变为下凸,结构度从下降变为上升。分析表明,该模型不仅能描述液态粘弹性介质的行为,还能描述固态(增厚、硬化、淬火)介质的行为:蠕变、松弛、恢复、实验松弛曲线的一些典型特性、蠕变和应力-应变曲线、应变速率和应变硬化、恒定应力下的流动等。
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引用次数: 0
In-Plane Free Vibration of Laterally Symmetric Functionally Graded Material Arches 横向对称功能分级材料拱的平面内自由振动
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-25 DOI: 10.1007/s11029-024-10203-4
Gweon Sik Kim, Joon Kyu Lee, Byoung Koo Lee

This study aims to analyze the in-plane free vibrations of arches comprising the laterally symmetric functionally graded materials. Emphasis is placed on the circular arch whose material properties vary laterally symmetrically about the centroidal axis by a power-law function. The differential equations governing the mode shape of the arch were derived under the boundary conditions and were numerically solved to calculate the natural frequencies using the Runge–Kutta and Regula–Falsi methods. Calculation results of this study for natural frequencies compare well with those of the finite element method. The effects of various arch parameters on natural frequencies are highlighted and discussed in detail.

本研究旨在分析由横向对称功能分级材料组成的拱的平面内自由振动。重点是材料特性以幂律函数围绕中心轴横向对称变化的圆形拱。在边界条件下导出了支配拱模态振型的微分方程,并使用 Runge-Kutta 和 Regula-Falsi 方法进行数值求解,以计算固有频率。这项研究的固有频率计算结果与有限元法的计算结果比较吻合。本研究还强调并详细讨论了各种拱形参数对自然频率的影响。
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引用次数: 0
The Effect of Fiber Waviness on the Stiffness of a Polymer Composite Material 纤维波纹对聚合物复合材料刚度的影响
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-25 DOI: 10.1007/s11029-024-10212-3
D. A. Bondarchuk, B. N. Fedulov, E. V. Lomakin

It is known that the initial fiber waviness affects the stiffness and strength of the polymer composite material. The influence of degree of waviness on stiffness characteristics under uniaxial tension and compression of a polymer composite material was investigated by using numerical modeling. A computational approach based on a special periodicity cell with different fiber waviness was developed. The hypothesis regarding the impact of manufacturing stresses, appearing during a curing process on waviness growth, was tested. The results obtained explain the mechanism that causes difference in the stiffness observed in fiber composites in the longitudinal direction under uniaxial tension and compression.

众所周知,初始纤维波纹会影响聚合物复合材料的刚度和强度。通过数值建模,研究了波纹度对聚合物复合材料单轴拉伸和压缩下刚度特性的影响。研究开发了一种基于具有不同纤维波浪度的特殊周期单元的计算方法。对固化过程中出现的制造应力对波纹增长的影响进行了假设检验。所获得的结果解释了在单轴拉伸和压缩条件下纤维复合材料纵向刚度不同的原因。
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引用次数: 0
Development of Web-Based Software for the Failure Analysis of Composite Laminae 开发基于网络的复合材料层压板失效分析软件
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-25 DOI: 10.1007/s11029-024-10213-2
E. A. W. de Menezes, T. da Costa Dias, G. M. Dick, A. O. de Rosso, M. C. Krenn, M. L. P. Tonatto, S. C. Amico

MECH-Gcomp was developed as web-based free software to aid in learning and to help researchers and industry professionals in failure analysis of composite materials. The software is already well-established for the study of micromechanics and has extended to other fields. This work focuses on one of its newest modules, related to the failure analysis of composite laminae, for which thirteen different failure criteria were implemented, along with an important tool for the construction of failure envelopes. The programming and characteristics of this module are presented and discussed. In addition, jute/polyester composites were manufactured and tested under different stress states to verify the software predictions. The root-mean-square error ranged from 0.096 to a maximum of 0.545, and most of the analyzed criteria yielded reasonable agreement compared to the experimental data. A significant variation in predictions among the criteria could be clearly observed, especially based on the produced failure envelopes for the different stress states.

MECH-Gcomp 是一款基于网络的免费软件,旨在帮助研究人员和工业专业人员学习和分析复合材料的失效。该软件已在微观力学研究中得到广泛应用,并已扩展到其他领域。这项工作的重点是其最新模块之一,与复合材料层的失效分析有关,其中实施了 13 种不同的失效标准,以及构建失效包络的重要工具。对该模块的编程和特点进行了介绍和讨论。此外,还制造了黄铜/聚酯复合材料,并在不同的应力状态下进行了测试,以验证软件的预测结果。均方根误差从 0.096 到最大 0.545 不等,与实验数据相比,大多数分析标准都取得了合理的一致。根据不同应力状态下产生的失效包络线,可以清楚地观察到不同标准的预测结果存在明显差异。
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引用次数: 0
Effect of Printing Temperature on Fatigue and Impact Performance of 3-D Printed Carbon Fiber Reinforced PLA Composites for Ankle Foot Orthotic Device 打印温度对用于踝足矫形器的 3-D 打印碳纤维增强聚乳酸复合材料的疲劳和冲击性能的影响
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-24 DOI: 10.1007/s11029-024-10209-y
Divya Pandey, Ramesh Pandey, Ashutosh Mishra, Ravi Prakash Tewari

Carbon fiber reinforced-polylactic acid (CF-PLA) composites nowadays are widely researched alternative structural materials for their potential application in prosthetic and orthotic implants. The present work firstly consolidates the findings on the application of 3D printing in biomedical and allied fields. Fatigue life and impact strength of 3D printed CF-PLA test specimens were determined. The test specimens were fabricated through the fused deposition modeling (FDM) approach at two printing temperatures. The pronounced effect of printing temperature is characterized by the significant change in fatigue life and impact strength of the FDM specimen. The fatigue life at the printing temperature of 240°C was 2.7 times greater than that at 225°C, whereas the impact strength was greater by 5.93%. The microscopy findings revealed increased diffusion and a reduced number of ridges and pores at higher printing temperature testifying that printing temperature prominently controls the durability and impact response of FDM printed parts.

如今,碳纤维增强聚乳酸(CF-PLA)复合材料因其在假肢和矫形植入物中的潜在应用而成为被广泛研究的替代结构材料。本研究首先巩固了三维打印在生物医学及相关领域的应用研究成果。本研究测定了 3D 打印 CF-PLA 试样的疲劳寿命和冲击强度。试样是在两种打印温度下通过熔融沉积成型(FDM)方法制造的。打印温度的明显影响表现在 FDM 试样的疲劳寿命和冲击强度发生了显著变化。打印温度为 240°C 时的疲劳寿命是 225°C 时的 2.7 倍,而冲击强度则提高了 5.93%。显微镜研究结果表明,在较高的印刷温度下,扩散增加,脊和孔的数量减少,这证明印刷温度在很大程度上控制着 FDM 印刷部件的耐久性和冲击响应。
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引用次数: 0
Optimization and Experimental Investigation of the Mechanical Properties of Copper/Graphene Oxide/Epoxy Hybrid Nanocomposites 铜/氧化石墨烯/环氧树脂混合纳米复合材料力学性能的优化与实验研究
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-24 DOI: 10.1007/s11029-024-10207-0
M. Mahouri, V. Parvaneh, A. Dadrasi, G. Shafiei Sabet

This study focuses on the effect of copper nanoparticles and graphene oxide nanosheets on the tensile properties and impact strength of epoxy-based hybrid nanocomposites. A mechanical mixer and an ultrasonicator were used to mix the reinforcements with the epoxy resin. Field Emission Scanning Electron Microscope (FE-SEM) was used to examine the fracture surface morphology, and tensile and impact tests were conducted to assess the mechanical properties of the nanocomposites. These properties were optimized by a genetic algorithm. The results showed that adding 0.75 wt% copper nanoparticles and 1 wt.% graphene oxide to the epoxy increased its tensile strength by 45.7 and 37.14%, respectively, compared with those of pure epoxy, and adding 0.5 wt% graphene oxide and 0.75 wt% copper nanoparticle led to a 61.76 and 32.35% increase in its fracture strength. The tensile test results indicated that the tensile strength of specimens reinforced with 0.125 wt% graphene oxide and 0.125 wt% copper nanoparticles increased by 47.51% compared with those of pure epoxy and adding 0.375 wt% graphene oxide and 0.375 wt% copper nanoparticles increased the fracture energy by 91.18%.

本研究的重点是铜纳米颗粒和氧化石墨烯纳米片对环氧基混合纳米复合材料拉伸性能和冲击强度的影响。使用机械搅拌器和超声波发生器将增强材料与环氧树脂混合。使用场发射扫描电子显微镜(FE-SEM)检查断裂表面形态,并进行拉伸和冲击试验以评估纳米复合材料的机械性能。通过遗传算法对这些性能进行了优化。结果表明,与纯环氧树脂相比,在环氧树脂中添加 0.75 wt% 的纳米铜粒子和 1 wt.% 的氧化石墨烯可使其拉伸强度分别提高 45.7% 和 37.14%,而添加 0.5 wt% 的氧化石墨烯和 0.75 wt% 的纳米铜粒子可使其断裂强度分别提高 61.76% 和 32.35%。拉伸试验结果表明,与纯环氧树脂相比,添加 0.125 wt% 氧化石墨烯和 0.125 wt% 纳米铜颗粒增强的试样的拉伸强度提高了 47.51%,添加 0.375 wt% 氧化石墨烯和 0.375 wt% 纳米铜颗粒增强的试样的断裂能提高了 91.18%。
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引用次数: 0
Experimental Investigation on the Static and Dynamic Behavior of Passive Controlled Bio Composite Manufactured Via 3D Printing Technique 通过三维打印技术制造的被动受控生物复合材料的静态和动态行为实验研究
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-24 DOI: 10.1007/s11029-024-10205-2
F. Meddeb, A. El Mahi, J. L. Rebiere, H. Daoud, M. A. Ben Souf, M. Haddar

Bio-based composites with passive control layers were investigated by means of a comprehensive set of experiments. The structure, composed of an exterior layer of PLA/Flax and an inserted rubber layer, were manufactured using 3D printing technology. Tensile tests on PLA/Flax and rubber specimens revealed that it exhibited higher stiffness, whereas rubber demonstrated superior elongation. Additionally, three-point bending tests were conducted on 3D-printed composites with varying viscoelastic layer thicknesses (VL) to assess their bending performance. However, the composite with a single 1-mm thick viscoelastic layer (V1t1) showed optimal deflection and stiffness compared to counterparts with different viscoelastic layers. Furthermore, resonance vibration experiments were performed to investigate dynamic parameters such as frequencies and modal loss factors. Based on the experiments, it was determined that V1t1 was the composite that offered the optimal compromise between mechanical and vibration behavior due to its excellent damping characteristics.

通过一系列综合实验对带有被动控制层的生物基复合材料进行了研究。该结构由聚乳酸/亚麻外层和插入的橡胶层组成,采用三维打印技术制造。对聚乳酸/亚麻和橡胶试样进行的拉伸测试表明,聚乳酸/亚麻表现出更高的刚度,而橡胶则表现出更高的伸长率。此外,还对具有不同粘弹性层厚度(VL)的三维打印复合材料进行了三点弯曲测试,以评估其弯曲性能。然而,与具有不同粘弹性层的复合材料相比,具有 1 毫米厚粘弹性层(V1t1)的复合材料显示出最佳的挠度和刚度。此外,还进行了共振振动实验,以研究频率和模态损失因子等动态参数。根据实验结果,可以确定 V1t1 是一种复合材料,由于其出色的阻尼特性,它在机械和振动行为之间提供了最佳的折衷方案。
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引用次数: 0
Preparation and Characterisation of Composites from Industrial Waste: Wood Flour and Expanded Ethylene Vinyl Acetate 利用工业废料制备复合材料并确定其特性:木粉和膨胀乙烯醋酸乙烯酯
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-22 DOI: 10.1007/s11029-024-10201-6
G. Trifeldaite-Baranauskiene, E. Stankute, A. Aniskevich, D. Zeleniakiene, K. Zukiene

The aim of the present study is to use beech wood flour (WF) and expanded ethylene vinyl acetate (EVA) copolymer industrial waste to develop a sustainable composite and its production method for further engineering use. Polyamide (PA) powder waste obtained after multiple selective laser sintering (SLS) thermal cycles was used to increase the strength and adhesion between the waste composite components. The morphological, mechanical, and thermal properties of the EVA/WF composites were characterised along with their interfacial wetting and water absorption properties. Optical and electron microscopy investigations revealed that the composites prepared have homogeneous dispersion and good interfacial adhesion between EVA and wood. The addition of SLS waste PA powder increases the strength and stiffness of the composite developed. The composite with 40 wt% WF exhibited the best water absorption, mechanical properties, and processability among the various compositions. The sustainable composite proposed can replace commercially available materials, which helps to save resources and reduce waste.

本研究的目的是利用榉木粉(WF)和发泡乙烯-醋酸乙烯(EVA)共聚物工业废料,开发一种可持续复合材料及其生产方法,供进一步工程使用。经过多次选择性激光烧结(SLS)热循环后得到的聚酰胺(PA)粉末废料被用来增加废料复合材料成分之间的强度和粘合力。对 EVA/WF 复合材料的形态、机械和热性能及其界面润湿和吸水性能进行了表征。光学和电子显微镜研究表明,制备的复合材料具有均匀的分散性,EVA 和木材之间具有良好的界面粘附性。加入 SLS 废 PA 粉末后,所制备复合材料的强度和刚度都有所提高。在各种成分中,含 40 wt% WF 的复合材料具有最佳的吸水性、机械性能和可加工性。所提出的可持续复合材料可替代市售材料,有助于节约资源和减少浪费。
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引用次数: 0
Families of Stress–Strain, Relaxation and Creep Curves Generated by a Nonlinear Model for Thixotropic Viscoelastic-Plastic Media Accounting for Structure Evolution Part 2. Relaxation and Stress-Strain Curves 考虑结构演变的触变粘弹性介质非线性模型生成的应力-应变、松弛和蠕变曲线族 第 2 部分.松弛和应力-应变曲线
IF 1.7 4区 材料科学 Q4 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-05-07 DOI: 10.1007/s11029-024-10197-z
A. V. Khokhlov, V. V. Gulin

A systematic analytical study of the mathematical properties of the previously constructed nonlinear model for shear flow of thixotropic viscoelastic-plastic media is continued. For arbitrary six material parameters and an (increasing) material function that control the model, the basic properties of the families of stress-strain curves at constant strain rates and relaxation curves generated by the model, and the features of the evolution of the structuredness under these types of loading are analytically studied. The dependences of these curves on time, shear rate, initial strain and initial structuredness of the material, as well as on the material parameters and function of the model, are studied. Several indicators of the applicability of the model are found which are convenient to check with experimental data. It was examined what effects typical for viscoelastic-plastic media can be described by the model and what unusual effects (unusual properties) are generated by a change in structuredness in comparison with typical stress-strain curves and relaxation curves of structurally stable materials. In particular, it has been proved that stress-strain curves can be both increasing functions and can have decreasing sections resembling a “yield tooth” or damped oscillations, that all stress-strain curves (SSCs) possess horizontal asymptotes (steady flow stress), monotonically dependent on shear rate, and flow stress increases with shear rate growth, that the instantaneous shear modulus, on the contrary, depends on the initial structuredness, but does not depend on shear rate. Under certain restrictions on the material parameters, the model is also capable of providing a bilinear form of stress-strain curves, which is typical for an ideal elastoplastic model, but with strain rate sensitivity. It has been established that the family of stress-strain curves does not have to be increasing either in initial structuredness or in shear rate: in a certain range of shear rates, in which the equilibrium position is a “mature” focus and pronounced oscillations of stress-strain curves are observed, it is possible to intertwine stress-strain curves with different shear rates. It is proved that for any material parameters and functions, all stress relaxation curves decrease and have a common zero asymptote as time tends to infinity. The analysis proved the ability of the model to describe behavior of not only liquid-like viscoelastoplastic media, but also solid-like (thickening, hardening, hardened) media: creep, relaxation, recovery, a number of typical properties of experimental relaxation curves, creep and stress-strain curves, strain rate and strain hardening, flow under constant stress and so on.

继续对之前构建的触变粘弹性塑性介质剪切流非线性模型的数学特性进行系统分析研究。对于控制模型的任意六个材料参数和一个(递增)材料函数,分析研究了模型产生的恒定应变速率下应力-应变曲线和松弛曲线族的基本特性,以及在这些类型的加载下结构性演变的特征。研究了这些曲线对时间、剪切速率、初始应变和材料初始结构度的依赖性,以及对材料参数和模型功能的依赖性。发现了模型适用性的几个指标,便于与实验数据进行核对。与结构稳定材料的典型应力-应变曲线和松弛曲线相比,研究了该模型可以描述粘弹性-塑性介质的哪些典型效应,以及结构度变化会产生哪些异常效应(异常特性)。特别是,研究证明应力-应变曲线既可以是递增函数,也可以具有类似 "屈服齿 "或阻尼振荡的递减截面;所有应力-应变曲线(SSC)都具有水平渐近线(稳定流动应力),与剪切速率单调相关,流动应力随剪切速率增长而增加;相反,瞬时剪切模量取决于初始结构度,但与剪切速率无关。在对材料参数有一定限制的情况下,该模型还能提供双线性形式的应力-应变曲线,这是理想弹塑性模型的典型形式,但具有应变速率敏感性。研究发现,应力-应变曲线族并不一定要在初始结构度或剪切速率上不断增加:在一定的剪切速率范围内,平衡位置是一个 "成熟 "的焦点,应力-应变曲线会出现明显的振荡,不同剪切速率下的应力-应变曲线有可能交织在一起。研究证明,对于任何材料参数和函数,当时间趋于无穷大时,所有应力松弛曲线都会减小,并有一个共同的零渐近线。分析证明,该模型不仅能描述液态粘弹性介质的行为,还能描述固态(增厚、硬化、硬化)介质的行为:蠕变、松弛、恢复、实验松弛曲线的一些典型特性、蠕变和应力-应变曲线、应变速率和应变硬化、恒定应力下的流动等。
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引用次数: 0
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Mechanics of Composite Materials
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